Microencapsulation of neroline inside microcapsules having a polyurethane shell based onβ-cyclodextrin(β-CD)and hexane diisocyanate was performed by interfacial polycondensation.The polyol nature ofβ-CD caused tigh...Microencapsulation of neroline inside microcapsules having a polyurethane shell based onβ-cyclodextrin(β-CD)and hexane diisocyanate was performed by interfacial polycondensation.The polyol nature ofβ-CD caused tight crosslinking of microcapsules wall.Microcapsules of neroline were characterized for their chemical composition and structure of the polyurethane shell by FTIR spectroscopy,thermogravimetric analysis,optical and electron microscopy,light scattering and electrophoresis measurements.Core content and encapsulation yield were 15%and 60%,respectively.Spherical microcapsules of mean diameter 29μm were slightly cationic with an isoelectric point of 6.3.Neroline-loaded microcapsules were fixed on cotton fabric using an impregnation technique.The functionalized fabric showed improved resistance to washing cycles in comparison with previously reported diol-based microcapsules.Such microcapsules display great potential for the long-lasting release of fragrance in the framework of cosmetotextile.展开更多
基金by the“Ministry of Higher Education and Scientific Research”of Tunisia,Laboratory of Advanced Materials and Interfaces(LAMI,LR-11-S-55)。
文摘Microencapsulation of neroline inside microcapsules having a polyurethane shell based onβ-cyclodextrin(β-CD)and hexane diisocyanate was performed by interfacial polycondensation.The polyol nature ofβ-CD caused tight crosslinking of microcapsules wall.Microcapsules of neroline were characterized for their chemical composition and structure of the polyurethane shell by FTIR spectroscopy,thermogravimetric analysis,optical and electron microscopy,light scattering and electrophoresis measurements.Core content and encapsulation yield were 15%and 60%,respectively.Spherical microcapsules of mean diameter 29μm were slightly cationic with an isoelectric point of 6.3.Neroline-loaded microcapsules were fixed on cotton fabric using an impregnation technique.The functionalized fabric showed improved resistance to washing cycles in comparison with previously reported diol-based microcapsules.Such microcapsules display great potential for the long-lasting release of fragrance in the framework of cosmetotextile.
