The purpose of this study was to evaluate the antibacterial activity of a modified self-etching primer incorporating chitosan and whether this modification affected the bond strength to radicular dentin.A modified sel...The purpose of this study was to evaluate the antibacterial activity of a modified self-etching primer incorporating chitosan and whether this modification affected the bond strength to radicular dentin.A modified self-etching primer was prepared by adding chitosan solutions at 0.03%,0.06%,0.12% and 0.25%（W/W） to RealSeal selfetching primer.RealSeal primer without chitosan was used as the control.The antibacterial activity of the modified self-etching primer was evaluated using the direct contact test against Enterococcus faecalis.The bonding ability of the RealSeal system to radicular dentin was evaluated using the push-out bond strength test.The modes of failure were examined under a stereomicroscope.Data were analyzed using analysis of variance（ANOVA） and Tukey’s test,with a P-value 〈 0.05 indicating statistical significance.The results showed that the antibacterial properties of the freshly prepared and aged modified self-etching primer incorporating chitosan exhibited potent antibacterial effect against Enterococcus faecalis compared with the unmodified primer.The RealSeal system with the aged modified self-etching primer incorporating chitosan showed no significant differences in the bond strength as compared with the control（P = 0.99）.The findings suggest that modified self-etching primer incorporating chitosan is a promising antibacterial primer which does not adversely affect the bond strength of the RealSeal system to radicular dentin.展开更多
This study examined the adhesive strength of two self-adhesive methacrylate resin-based sealers（MetaSEAL and RealSeal SE） to root dentin and compared them with RealSeal and AH Plus in properties. A total of 48 extra...This study examined the adhesive strength of two self-adhesive methacrylate resin-based sealers（MetaSEAL and RealSeal SE） to root dentin and compared them with RealSeal and AH Plus in properties. A total of 48 extracted human single-rooted teeth were used to prepare the 0.9-mm thick longitudinal tooth slice（each per tooth）. Standardized simulated canal spaces of uniform dimensions were prepared in the middle of radicular dentin. After treated with 5.25% sodium hypochlorite（NaOCl） and 17% EDTA, tooth slices were allocated randomly to four groups（n=12） in terms of different sealers used： MetaSEAL, RealSeal SE, RealSeal, and AH plus groups. The simulated canal spaces were obturated with different sealers in each group. There were 10 slabs with 20 simulated canal spaces（n=20） used in each group for push-out testing. The failure modes and the ultrastructures of fractured sealer-dentin interfaces were examined. The remaining 2 slabs in each group underwent partial demineralization for observation of the ultrastructure of resin tags. The results showed that the push-out bond strength was 12.01±4.66 MPa in MetaSEAL group, significantly higher than that in the other three groups（P0.05）. Moreover, no statistically significant differences were noted in the push-out bond strength between RealSeal SE（5.43±3.68 MPa） and AH Plus（7.34±2.83 MPa） groups and between RealSeal SE and RealSeal（2.93±1.76 MPa） groups（P0.05）. Mixed failures were predominant in the fractured sealer-dentin interfaces in MetaSEAL and AH Plus groups, while adhesive failures were frequently seen in RealSeal SE and RealSeal groups. In conclusion, after complete removal of the smear layer, MetaSEAL showed superior bond ability to root dentin. The RealSeal SE is applicable in clinical practice, with its adhesive strength similar to that of AH Plus. The self-adhesive methacrylate resin-based sealer holds promise for use in endodontic treatment.展开更多
Based on the interphase layer model and the spring layer model, an improved interface model was developed to evaluate the interfacial shear strength of Titanium matrix composites(TMCs) and to analyze the effects of va...Based on the interphase layer model and the spring layer model, an improved interface model was developed to evaluate the interfacial shear strength of Titanium matrix composites(TMCs) and to analyze the effects of various parameters on the interfacial properties. The results showed that the improved interface model is more suitable for calculating the interfacial properties of SiC fiber reinforced titanium matrix composites. The interfacial shear strength of SiC/Timetal-834 predicted is 500 MPa. In addition, in order to better understand the interfacial properties of composites, some push out phenomenon were analyzed.展开更多
This paper presents an easily installed improved perfobond connector (PBL) designed to reduce the shearconcentration of PBL. The improvement of PBL lies in changing the straight penetrating rebar to the Z-typepenetrat...This paper presents an easily installed improved perfobond connector (PBL) designed to reduce the shearconcentration of PBL. The improvement of PBL lies in changing the straight penetrating rebar to the Z-typepenetrating rebar. To study the shear performance of improved PBL, two PBL test specimens which containstraight penetrating rebar and six improved PBL test specimens which contain Z-type penetrating rebars weredesigned and fabricated, and push-out tests of these eight test specimens were carried out to investigate andcompare the shear behavior of PBL. Additionally, Finite Element Analysis (FEA) models of the PBL specimenswere established and validated against the test results. Through FEA, the effects of concrete grade, perforatedplate’s aperture, Z-type penetrating rebar’s diameter, Z-type penetrating rebar’s bending angle, and bending lengthon shear behaviors were discussed. The results indicate that (1) Compared with PBL specimens with straightpenetrating rebars, Z-type penetrating rebar can significantly improve the shear resistance and shear stiffnessof the specimens. This enhanced performance can be mainly attributed to the increased adhesion of the transverserebar. (2) By comparing the load-slip curve, the slip of PBL test specimens which contain straight penetratingrebar increases rapidly and the bearing capacity decreases rapidly after concrete craking, while the bearingcapacity of Z-type penetrating rebar specimens decreases first and then increases gradually, showing betterductility. (3) The stress of the PBL shear connector with Z-type penetrating rebar is more uniform than thePBL shear connector with straight penetrating rebar, and the overall deformation is more uniform. (4) The higherthe concrete grade, the higher the shear bearing capacity and the better ductility of the new PBL. Increasing theaperture of the perforated plate or the diameter of the rebar has a very limited effect on the improvement of theshear capacity of PBL. Through the systematic analysis of the mechanical properties of Z-type penetrating rebarPBL specimen, the experimental reference is provided for improving the structure and design of new type PBL.展开更多
文摘The purpose of this study was to evaluate the antibacterial activity of a modified self-etching primer incorporating chitosan and whether this modification affected the bond strength to radicular dentin.A modified self-etching primer was prepared by adding chitosan solutions at 0.03%,0.06%,0.12% and 0.25%（W/W） to RealSeal selfetching primer.RealSeal primer without chitosan was used as the control.The antibacterial activity of the modified self-etching primer was evaluated using the direct contact test against Enterococcus faecalis.The bonding ability of the RealSeal system to radicular dentin was evaluated using the push-out bond strength test.The modes of failure were examined under a stereomicroscope.Data were analyzed using analysis of variance（ANOVA） and Tukey’s test,with a P-value 〈 0.05 indicating statistical significance.The results showed that the antibacterial properties of the freshly prepared and aged modified self-etching primer incorporating chitosan exhibited potent antibacterial effect against Enterococcus faecalis compared with the unmodified primer.The RealSeal system with the aged modified self-etching primer incorporating chitosan showed no significant differences in the bond strength as compared with the control（P = 0.99）.The findings suggest that modified self-etching primer incorporating chitosan is a promising antibacterial primer which does not adversely affect the bond strength of the RealSeal system to radicular dentin.
文摘This study examined the adhesive strength of two self-adhesive methacrylate resin-based sealers（MetaSEAL and RealSeal SE） to root dentin and compared them with RealSeal and AH Plus in properties. A total of 48 extracted human single-rooted teeth were used to prepare the 0.9-mm thick longitudinal tooth slice（each per tooth）. Standardized simulated canal spaces of uniform dimensions were prepared in the middle of radicular dentin. After treated with 5.25% sodium hypochlorite（NaOCl） and 17% EDTA, tooth slices were allocated randomly to four groups（n=12） in terms of different sealers used： MetaSEAL, RealSeal SE, RealSeal, and AH plus groups. The simulated canal spaces were obturated with different sealers in each group. There were 10 slabs with 20 simulated canal spaces（n=20） used in each group for push-out testing. The failure modes and the ultrastructures of fractured sealer-dentin interfaces were examined. The remaining 2 slabs in each group underwent partial demineralization for observation of the ultrastructure of resin tags. The results showed that the push-out bond strength was 12.01±4.66 MPa in MetaSEAL group, significantly higher than that in the other three groups（P0.05）. Moreover, no statistically significant differences were noted in the push-out bond strength between RealSeal SE（5.43±3.68 MPa） and AH Plus（7.34±2.83 MPa） groups and between RealSeal SE and RealSeal（2.93±1.76 MPa） groups（P0.05）. Mixed failures were predominant in the fractured sealer-dentin interfaces in MetaSEAL and AH Plus groups, while adhesive failures were frequently seen in RealSeal SE and RealSeal groups. In conclusion, after complete removal of the smear layer, MetaSEAL showed superior bond ability to root dentin. The RealSeal SE is applicable in clinical practice, with its adhesive strength similar to that of AH Plus. The self-adhesive methacrylate resin-based sealer holds promise for use in endodontic treatment.
基金Supported by the Natural Science Foundation of Chinathe Aviation Science Foundation of Chinathe Doctoral Innovation Foundation of Northwestern Polytechnical University
文摘Based on the interphase layer model and the spring layer model, an improved interface model was developed to evaluate the interfacial shear strength of Titanium matrix composites(TMCs) and to analyze the effects of various parameters on the interfacial properties. The results showed that the improved interface model is more suitable for calculating the interfacial properties of SiC fiber reinforced titanium matrix composites. The interfacial shear strength of SiC/Timetal-834 predicted is 500 MPa. In addition, in order to better understand the interfacial properties of composites, some push out phenomenon were analyzed.
文摘This paper presents an easily installed improved perfobond connector (PBL) designed to reduce the shearconcentration of PBL. The improvement of PBL lies in changing the straight penetrating rebar to the Z-typepenetrating rebar. To study the shear performance of improved PBL, two PBL test specimens which containstraight penetrating rebar and six improved PBL test specimens which contain Z-type penetrating rebars weredesigned and fabricated, and push-out tests of these eight test specimens were carried out to investigate andcompare the shear behavior of PBL. Additionally, Finite Element Analysis (FEA) models of the PBL specimenswere established and validated against the test results. Through FEA, the effects of concrete grade, perforatedplate’s aperture, Z-type penetrating rebar’s diameter, Z-type penetrating rebar’s bending angle, and bending lengthon shear behaviors were discussed. The results indicate that (1) Compared with PBL specimens with straightpenetrating rebars, Z-type penetrating rebar can significantly improve the shear resistance and shear stiffnessof the specimens. This enhanced performance can be mainly attributed to the increased adhesion of the transverserebar. (2) By comparing the load-slip curve, the slip of PBL test specimens which contain straight penetratingrebar increases rapidly and the bearing capacity decreases rapidly after concrete craking, while the bearingcapacity of Z-type penetrating rebar specimens decreases first and then increases gradually, showing betterductility. (3) The stress of the PBL shear connector with Z-type penetrating rebar is more uniform than thePBL shear connector with straight penetrating rebar, and the overall deformation is more uniform. (4) The higherthe concrete grade, the higher the shear bearing capacity and the better ductility of the new PBL. Increasing theaperture of the perforated plate or the diameter of the rebar has a very limited effect on the improvement of theshear capacity of PBL. Through the systematic analysis of the mechanical properties of Z-type penetrating rebarPBL specimen, the experimental reference is provided for improving the structure and design of new type PBL.
