Formation,evolution,reconstruction of black shales and their influence on shale oil and gas resource

Black shales are important products of material cycling and energy exchange among the lithosphere,atmosphere,hydrosphere,and biosphere.They are widely distributed throughout geological history and provide essential energy and mineral resources for the development of human society.They also record the evolution process of the earth and improve the understanding of the earth.This review focuses on the diagenesis and formation mechanisms of black shales sedimentation,composition,evolution,and reconstruction,which have had a significant impact on the formation and enrichment of shale oil and gas.In terms of sedimentary environment,black shales can be classified into three types:Marine,terrestrial,and marine-terrestrial transitional facies.The formation processes include mechanisms such as eolian input,hypopycnal flow,gravity-driven and offshore bottom currents.From a geological perspective,the formation of black shales is often closely related to global or regional major geological events.The enrichment of organic matter is generally the result of the interaction and coupling of several factors such as primary productivity,water redox condition,and sedimentation rate.In terms of evolution,black shales have undergone diagenetic evolution of inorganic minerals,thermal evolution of organic matter and hydrocarbon generation,interactions between organic matter and inorganic minerals,and pore evolution.In terms of reconstruction,the effects of fold deformation,uplift and erosion,and fracturing have changed the stress state of black shale reservoirs,thereby having a significant impact on the pore structure.Fluid activity promotes the formation of veins,and have changed the material composition,stress structure,and reservoir properties of black shales.Regarding resource effects,the deposition of black shales is fundamental for shale oil and gas resources,the evolution of black shales promotes the shale oil and gas formation and storage,and the reconstruction of black shales would have caused the heterogeneous distribution of oil and gas in shales.Exploring the formation mechanisms and interactions of black shales at different scales is a key to in-depth research on shale formation and evolution,as well as the key to revealing the mechanism controlling shale oil and gas accumulation.The present records can reveal how these processes worked in geological history,and improve our understanding of the coupling mechanisms among regional geological events,black shales evolution,and shale oil and gas formation and enrichment.

Growth behavior and resource potential evaluation of gas hydrate in core fractures in Qilian Mountain permafrost area, Qinghai-Tibet Plateau

The Qilian Mountain permafrost area located in the northern of Qinghai-Tibet Plateau is a favorable place for natural gas hydrate formation and enrichment,due to its well-developed fractures and abundant gas sources.Understanding the formation and distribution of multi-component gas hydrates in fractures is crucial in accurately evaluating the hydrate reservoir resources in this area.The hydrate formation experiments were carried out using the core samples drilled from hydrate-bearing sediments in Qilian Mountain permafrost area and the multi-component gas with similar composition to natural gas hydrates in Qilian Mountain permafrost area.The formation and distribution characteristics of multi-component gas hydrates in core samples were observed in situ by X-ray Computed Tomography(X-CT)under high pressure and low temperature conditions.Results show that hydrates are mainly formed and distributed in the fractures with good connectivity.The ratios of volume of hydrates formed in fractures to the volume of fractures are about 96.8%and 60.67%in two different core samples.This indicates that the fracture surface may act as a favorable reaction site for hydrate formation in core samples.Based on the field geological data and the experimental results,it is preliminarily estimated that the inventory of methane stored in the fractured gas hydrate in Qilian Mountain permafrost area is about 8.67×1013 m3,with a resource abundance of 8.67×108 m3/km2.This study demonstrates the great resource potential of fractured gas hydrate and also provides a new way to further understand the prospect of natural gas hydrate and other oil and gas resources in Qilian Mountain permafrost area.

Tectonic evolution and accumulation characteristics of Carboniferous shale gas in Yadu-Ziyun-Luodian aulacogen, Guizhou Province, South China

The Yadu-Ziyun-Luodian aulacogen(YZLA) developed into being NW-trending in the Late Paleozoic,and was considered as an important passive continental margin aulacogen in Guizhou Province, South China. This tectonic zone is considered a large intracontinental thrust-slip tectonic unit, which has undergone a long period of development. It was ultimately determined in the Yanshanian, where the typical Upper Paleozoic marine shales were deposited. In 2021, Well QSD-1 was deployed in the Liupanshui area at the northwest margin of the aulacogen, and obtained a daily shale gas flow of 11011 m3in the Carboniferous Dawuba Formation. It thus achieved a breakthrough in the invesgation of shale gas in the Lower Carboniferous in South China, revealing relatively good gas-bearing properties and broad exploration prospects of the aulacogen. Being different from the Lower Paleozoic strata in the Sichuan Basin and the Yichang area of the Middle Yangtze, the development of the Carboniferous Dawuba Formation in the aulacogen exhibits the following characteristics:(1) The Lower Carboniferous shale is thick and widely distributed, with interbedded shale and marlstone of virous thickness;(2) The total organic carbon(TOC) content of the shale in the Dawuba Formation ranges from 1% to 5%, with an average of 2%, and the thermal maturity of organic matter(Ro) varies from 1% to 4%, with an average of2.5%, indicating good hydrocarbon generation capacity;(3) The main shale in the aulacogen was formed during the fault subsidence stage from the Middle Devonian to the Early Permian. Although the strong compression and deformation during the late Indosinian-Himalayan played a certain role in destroying the formed shale gas reservoirs, comparative analysis suggests that the area covered by the current Triassic strata has a low degree of destruction. It therefore provides good conditions for shale gas preservation,which can be regarded as a favorable area for the next exploration.

Grading Evaluation and Ranking of CO_(2) Sequestration Capacity in Place(CSCIP) in China’s Major Oil Basins:Theoretical,Effective,Practical and CCUS-EOR

Because it is necessary to focus on differences in regional oil reservoirs and determine the priority of the CCUSEOR(Carbon capture,utilization,and storage-enhanced oil recovery) deployment under China’s net-zero CO_(2) emission target,systematic and regional evaluations of CO_(2) sequestration capacity in major oil basins are needed considering the geofluid properties―carbon sequestration capacity in place(CSCIP)―where the ’in place’ indicates actual geological formation conditions underground,e.g.,formation temperature and pressure.Therefore,physical properties of geofluids at different depths with different geologic temperatures and pressure conditions are considered for the CO_(2) sequestration capacity evaluation in place,including shallow(800–2000 m),medium(2000–3500 m),deep(3500–4500 m) and ultra-deep(4500–8000 m) depth intervals.A modified evaluation model with four grading levels is proposed,combining the P-V-T equations of state(EOS) and evaluation equations of the Carbon Sequestration Leadership Forum(CSLF),including theoretical,effective,practical,and CCUS-EOR CSCIP,which is more consistent with geofluid physical properties underground,to make the grading evaluation and ranking of the CSCIP in China’s major oil basins.Then,the grading CSCIP of 29 major oil basins in China was evaluated based on the petroleum resources evaluation results of the Ministry of Natural Resources of China(MNRC) during China’s 13th Five-Year Plan period.According to the grading evaluation results,suggestions for China’s CCUS-EOR prospective regions are given as follows:shallow oil fields of the Songliao Basin in Northeast China,shallow–medium oil fields of the Bohai Bay Basin in East China,medium oil fields of the Zhungeer Basin in West China,and medium oil fields of the Ordos Basin in Central China;all are potential areas for the CCUS-EOR geological sequestration in China’s onshore oil basins.In addition,in China’s offshore oil basins,shallow–medium oil fields of the Bohai Sea and shallow oil fields of the Pearl River Mouth Basin have potential for CCUS-EOR geological sequestration.

New Progress of Oil and Gas Research in the Tonghua Area, East of the Songliao Basin

The Tonghua region in the east of the Songliao Basin is a high-risk and blank area of petroleum exploration. The unrevealed key problems including the growth of source rocks, hydrocarbon generation potential and oil and gas source and the low exploration degree have constrained the further study of petroleum geological conditions and exploration deployment. Based on outcrop and core observations, geological section survey, trench exploration, high-precision gravity and magnetism and geological survey wells, this work discussed the basic geological conditions, main hydrocarbon source rocks, hydrocarbon generation potential and the oil and gas source.

Discovery of Oil and Gas Shows in the Lower Cretaceous of the Hongmiaozi Basin, Southeastern Songlibao Peripheral Basin

Objective The Hongmiaozi Basin in the southeastern part of the Songliao peripheral basin is a new oil and gas exploration area with a very low exploration level.This basin covers an area of 795 km;.It is adjacent to the Liuhe Basin and Tonghua Basin in the north,and to the Huanren Basin in the south.In order to identify the basic oil and gas geological characteristics,the deep structures and the

Geological conditions and reservoir characteristics of various shales in major shalehosted regions of China

China is home to shales of three facies:Marine shale,continental shale,and marine-continental transitional shale.Different types of shale gas are associated with significantly different formation conditions and major controlling factors.This study compared the geological characteristics of various shales and analyzed the influences of different parameters on the formation and accumulation of shale gas.In general,shales in China’s several regions exhibit high total organic carbon(TOC)contents,which lays a sound material basis for shale gas generation.Marine strata generally show high degrees of thermal evolution.In contrast,continental shales manifest low degrees of thermal evolution,necessitating focusing on areas with relatively high degrees of thermal evolution in the process of shale gas surveys for these shales.The shales of the Wufeng and Silurian formations constitute the most favorable shale gas reservoirs since they exhibit the highest porosity among the three types of shales.These shales are followed by those in the Niutitang and Longtan formations.In contrast,the shales of the Doushantuo,Yanchang,and Qingshankou formations manifest low porosities.Furthermore,the shales of the Wufeng and Longmaxi formations exhibit high brittle mineral contents.Despite a low siliceous mineral content,the shales of the Doushantuo Formation feature a high carbonate mineral content,which can increase the shales’brittleness to some extent.For marine-continental transitional shales,where thin interbeds of tight sandstone with unequal thicknesses are generally found,it is recommended that fracturing combined with drainage of multiple sets of lithologic strata should be employed to enhance their shale gas production.

Paleoenvironmental Evolution and Organic Matter Enrichment Genesis of the Late Turonian Black Shale in the Southern Songliao Basin,NE China

The Upper Cretaceous Qingshankou Formation black shales,deposited in the late Turonian(LTB shales),are the main source rocks of the Songliao Basin.The origins of organic matter enrichment of the shales is a contentious subject fuelling many ongoing debates.This study investigates the genesis of the organic matter-rich shale by using molecular geochemistry.The LTB shales can be divided into three sections.The SectionⅠshales were deposited in saline,stratified and anoxic water conditions,which are related to seawater incursion events.At least three episodic and periodic seawater incursion events were recognized during SectionⅠshale deposition.The SectionⅡshales deposited in brackish to fresh and deep lake-level conditions with high primary productivity,which are related to lake-level transgression.The SectionⅢshales were deposited under fresh and slightly oxidized water conditions,which are related to lake-level regression.Two organic matter enrichment models for the LTB shales are identified,that is,the seawater incursion model and the maximum lake-level transgression sedimentation model,which act on different shale sections,both playing significant roles in the enrichment of organic matter.

Analysis and prediction of glacier evolution trend(2020-2100)in Northern Xinjiang

Glaciers,as“solid reservoirs”,are precious resources in arid areas.The study of glaciers is of great significance to the sustainable development and management of agriculture and the economy in northern Xinjiang.The area of glacier distribution on the 1963 topographic map data,1975 MSS data,2000 ETM data,2008 CBERS-2 data,2014 and 2018 ETM+were collected as secondary data.According to the remote sensing survey,the glacier areas in Northern Xinjiang are identified during 1963-2018.Based on the evolution of glacier area in the past 55 years,and using two scenarios,the average annual decrease area of a region during the whole 1963-2018 and the period with the minimum reduction area,the glacier areas of Southern Tianshan Mountains,Western Tianshan Mountains,Eastern Tianshan Mountains,the Sawuer Mountains and Altai Mountains in Northern Xinjiang,and the whole northern Xinjiang in 2030,2040,2050,and 2100 are examined and predicted.In 2100,the glacier area in Northern Xinjiang may decrease by 43%-59%.

Exploration and research progress of shale gas in China

There are three types of shale gas resources in China.The resources are present in large amounts and are widely distributed.Marine facies,transitional facies and continental facies resources each account for a third.Based on resource distributions,there are many wells penetrated into the Sinian,Cambrian, Ordovieian,Silurian,Devonian,Carboniferous and Permian strata of the Yangtze plate and its periphery, the North China Craton and the Tarim Basin.Many years of exploration have indicated that the marine Silurian Longmaxi shale gas is widely distributed in south China and has been industrialized in its production in the Siehuan basin.The shale gas from the Cambrian Niutitang Formation and the Sinian Doushantuo Formation are important discoveries in Yichang,Hub ei and Zhenba,Shanxi.There are also shale gas resources found within transitional facies and continental facies in different areas in China.The "two element enrichment theory"has been summarized during the exploration process of Silurian marine shale gas in the Sichuan Basin.In addition,horizontal drilling and fracturing technologies up to 3500 m in depth have been developed.Based on the understanding of shale gas accumulation in a complex tectonic zone outside the Sichnan basin,a preliminary summary of the formation of the "converse fault syneline control reservoir"and "paleo uplift control reservoir"model has been constructed.The dominant theory of "Trinity"shale gas enrichment and the high yield of the "deep water Lu Pengxiang sedimentary facies belt, structural preservation conditions and overpressure"is summarized.Guided by the above theories.Anyel well in Guizhou and Eyangyel well in Hubei were drilled."Four storey"oil and shale "gas is found in the Permian Qixia group,the Silurian Shiniulan Formation,the Longmaxi Formation and the Ordovician Baota Formation in Anyel well.Good shale gas has been gound in the Cambrian Niutitang formation inian Doushantuo formation in Eyangye lwell.This paper aims to summarize and review the main progress,theoretical technology and problems of shale gas exploration and development in recent years in China,and predicts the future exploration and development direction for shale gas and possible exploration areas.

"Source-Diagenesis-Accumulation" enrichment and accumulation regularity of marine shale gas in southern China

After the breakthrough of shale gas exploration and development in the Ordovician Wufeng Formation (Fm.) and Silurian Longmaxi Fm. of Chongqing Jiaoshiba area,Changning-Weiyuan area,etc. in Sichuan basin,a series of discovery and breakthrough were obtained by China Geological Survey in the Cambrian Niutitang Fm. and Sinian Doushantuo Fm. shale of the areas with complicated structure outside Sichuan basin. Based on the understanding of the law of shale gas enrichment in Longmaxi Fm. in the basin,this paper puts forward three elements of the formation and enrichment of shale gas,which are the “Source”,the “Diagenesis ” and the “Accumulation ”,after deeply studying the law shale gas enrichment and accumulation in Sinian-Cambrian reservoir of the complex structure area outside the basin. The “Source”means the sedimentary environment and petrological characteristics of organic shale.The “Diagenesis ”means the basin tectonic subsidence and hydrocarbon generation and expulsion process of organic matter.The “Accumulation” means the tectonic uplift and shale gas preservation. It is proposed that the Sinian-Cambrian and Ordovician-Silurian black shale series in the middle and upper Yangtze region of southern China were both formed in the deep-water shelf environment of rift trough and foreland basin respectively.The dessert intervals were formed in the strong reduction environment under transgressive system tract.The shale lithology belongs to calcium-siliceous and charcoal-siliceous respectively. Based on the summary of structural evolution in Yangtze area,the correlation of structural burial depth with shale diagenesis and the coupling evolution of organic matter with pore structure are discussed. Combining with structural styles,the preservation conditions of shale gas are discussed. Five types of shale gas reservoir control models are further described. Two types of future exploration directions,which are reverse fault syncline and paleo-uplift margin in complex structural area outside the basin,are proposed.

The evolution of the Huangling uplift and its control on the accumulation and preservation of shale gas

There are plenty of Sinian and Cambrian potential shale gas resources in South China,which is characterized by high thermal evolution degrees,poor drilling performances and only occurs in local areas.Taking the principle “high to find low” is the key issue to achieving a breakthrough in older shale.China Geological Survey drilled in the periphery of the Proterozoic basement,i.e.the Huangling anticline,in the western Hubei,and Hannan paleocontinent in the southern Shanxi.It received high-quality gas-bearing shale with relatively low Ro in the in Lower Cambrian Niutitang formation and Sinian Doushantuo formation.Based on geological conditions of shale gas reservoirs in the Huangling anticline,this paper puts forward the new model named “Control over reservoirs by periphery of basement” about shale gas accumulation,suggesting that the shale deposited in a deepwater continental shelf in the periphery of the basement is characterized by shallow burial,a short burial time,stable tectonics,relatively low thermal evolution degrees,and shale gas reservoirs in a good condition.The shale of the Sinian-Cambrian strata deposited in deepwater continental shelves in the periphery of Chuanzhong paleo-uplift in Sichuan,Hannan paleocontinent in the southern Shanxi,Huangling anticline in western Hubei and Jiangnang-Xuefeng paleo-uplift in Hunan and Guizhou province have good shale gas exploration potential.

Distribution characteristics, exploration and development, geological theories research progress and exploration directions of shale gas in China

The shale gas resources in China have great potential and the geological resources of shale gas is over 100×10^(12)m^(3),which includes about 20×10^(12)m^(3) of recoverable resources.Organic-rich shales can be divided into three types according to their sedimentary environments,namely marine,marine-continental transitional,and continental shales,which are distributed in 13 stratigraphic systems from the Mesoproterozoic to the Cenozoic.The Sichuan Basin and its surrounding areas have the highest geological resources of shale gas,and the commercial development of shale gas has been achieved in the Upper Ordovician Wufeng Formation-Lower Silurian Longmaxi Formation in these areas,with a shale gas production of up to 20×10^(9)m^(3) in 2020.China has seen rapid shale gas exploration and development over the last five years,successively achieving breakthroughs and important findings in many areas and strata.The details are as follows.(1)Large-scale development of middle-shallow shale gas(burial depth:less than 3500 m)has been realized,with the productivity having rapidly increased;(2)breakthroughs have been constantly made in the development of deep shale gas(burial depth:3500-4500 m),and the ultradeep shale gas(burial depth:greater than 4500 m)is under testing;(3)breakthroughs have been made in the development of normal-pressure shale gas,and the assessment of the shale gas in complex tectonic areas is being accelerated;(4)shale gas has been frequently discovered in new areas and new strata,exhibiting a great prospect.Based on the exploration and development practice,three aspects of consensus have been gradually reached on the research progress in the geological theories of shale gas achieved in China.(1)in terms of deep-water fine-grained sediments,organic-rich shales are the base for the formation of shale gas;(2)in terms of high-quality reservoirs,the development of micro-nano organic matter-hosted pores serves as the core of shale gas accumulation;(3)in terms of preservation conditions,weak structural transformation,a moderate degree of thermal evolution,and a high pressure coefficient are the key to shale gas enrichment.As a type of important low-carbon fossil energy,shale gas will play an increasingly important role in achieving the strategic goals of peak carbon dioxide emissions and carbon neutrality.Based on the in-depth study of shale gas geological conditions and current exploration progress,three important directions for shale gas exploration in China in the next five years are put forward.

A Volumetric Model for Evaluating Tight Sandstone Gas Reserves in the Permian Sulige Gas Field,Ordos Basin,Central China

To accurately measure and evaluate reserves is critical for ensuring successful production of unconventional oil and gas. This work proposes a volumetric model to evaluate the tight sandstone gas reserves of the Permian Sulige gas field in the Ordos Basin. The reserves can be determined by four major parameters of reservoir cutoffs, net pay, gas-bearing area and compression factor Z, which are controlled by reservoir characteristics and sedimentation. Well logging, seismic analysis, core analysis and gas testing, as well as thin section identification and SEM analysis were used to analyze the pore evolution and pore-throat structure. The porosity and permeability cutoffs are determined by distribution function curve,empirical statistics and intersection plot. Net pay and gas-bearing area are determined based on the cutoffs, gas testing and sand body distribution, and the compression factor Z is obtained by gas component. The results demonstrate that the reservoir in the Sulige gas field is characterized by ultralow porosity and permeability, and the cutoffs of porosity and permeability are 5% and 0.15×10^(–3) μm^2, respectively. The net pay and gas-bearing area are mainly affected by the sedimentary facies, sand body types and distribution. The gas component is dominated by methane which accounts for more than 90%, and the compression factor Z of H_8(P_2h_8) and S_1(P_1s_1) are 0.98 and 0.985, respectively. The distributary channels stacked and overlapped, forming a wide and thick sand body with good developed intergranular pores and intercrystalline pores. The upper part of channel sand with good porosity and permeability can be sweet spot for gas exploration. The complete set of calculation systems proposed for tight gas reserve calculation has proved to be effective based on application and feedback. This model provides a new concept and consideration for reserve prediction and calculation in other areas.

The influence factors of gas-bearing and geological characteristics of Niutitang Formation shale in the southern margin of Xuefeng Mountain ancient uplift: A case of Well Huangdi 1

In order to evaluate the geological characteristics and gas-bearing factors of Niutitang Formation within the Lower Cambrian of northern Guizhou,the Huangping area located at the southern edge of the ancient uplift belt of Xuefeng Mountain was selected as the target area,and Well Huangdi 1 was drilled for the geological survey of shale gas.Through geological background analysis and well logging and laboratory analysis such as organic geochemical test,gas content analysis,isothermal adsorption,and specific surface area experiments on Well Huangdi 1,the results show that the Niutitang Formation is a deep-water shelf,trough-like folds and thrust fault.The thickness of black shale is 119.95 m,of which carbonaceous shale is 89.6 m.The average value of organic carbon content is 3.55%,kerogen vitrinite reflectance value is 2.37% and kerogen type is sapropel-type.The brittle mineral content is 51%(quartz 38%),clay mineral content is 38.3%.The value of porosity and permeability are 0.5%and 0.0014 mD,which the reservoir of the Niutitang Formation belongs to low permeability with characteristics of ultra-low porosity.The gas content is 0.09‒1.31 m^3/t with a high-value area and a second high-value area.By comparing with the geological parameters of adjacent wells in the adjacent area,the accumulation model of“sediment control zone,Ro control zone,structure controlling reservoir”in the study area is proposed.Therefore,deep-water shelf-slope facies,Ro is between high maturity-early stage of overmaturity and well-preserved zones in the Niutitang Formation in this area are favorable direction for the next step of shale gas exploration.

Tectonic evolution of the Huangling dome and its control effect on shale gas preservation in the north margin of the Yangtze Block, South China

Significant breakthroughs of shale gas exploration have been made in Lower Cambrian and Sinian shale in the north margin of the Yangtze Block,South China.The drill wells with industrial gas flow located in the southern margin of the Huangling dome.Base on the geological survey,2D seismic,geochronological and drill wells data,the tectonic evolution history of Huangling dome was studied,and its control effect on the preservation condition of shale gas was discussed.The result shows that the Huangling dome might undergo four tectonic stages:(1)About 800 Ma,granite intrusion in the Huangling dome basement,primarily of granites replaced metamorphism rocks;(2)800-200 Ma,no significant tectonic movement with slowly buried history;(3)From 200 Ma,multi-phase uplift and the sedimentary rocks was eroded in the core of the Huangling dome.Shale gas in the Cambrian and Sinian strata was well preserved in the margin of the Huangling dome as the following reasons:(1)The Sinian shale was buried about 7.8 km indepth during Middle Jurassic,source rocks have a suitable thermal maturity for shale gas;(2)The rigid basement of the Huangling dome was mainly composed by homogeneity granite,without intensive deformation.As the main challenges of the widely distributed Lower Cambrian and Sinian shale are highmaturity and intensive deformation,a geological unit with a dome probably is a favorable zone for the old age shale gas.Therefore,it indicates that the adjacent zone of the Xuefengshan,Shennongjia and Hannan are the geological units with a dome and probably have potentials for the exploration of shale in the Lower Cambrian and Sinian.

Geological characteristics and co-exploration and co-production methods of Upper Permian Longtan coal measure gas in Yangmeishu Syncline, Western Guizhou Province, China

Coal measure gas(also known as coal-bearing unconventional gas)is the key field and development direction of unconventional natural gas in recent years.The exploration and evaluation of coal measure gas(coalbed methane,coal shale gas and coal measure tight sandstone gas)from single coalbed methane has greatly expanded the field and space of resource evaluation,which is of positive significance for realizing the comprehensive utilization of coal resources,maximizing the benefits and promoting the innovation of oil and gas geological theory and technological advances in exploration and development.For the first time,in Yangmeishu Syncline of Western Guizhou Province,the public welfare coalbed methane geological survey project of China Geological Survey has been carried out a systematic geological survey of coal measure gas for the Upper Permian Longtan Formation,identified the geological conditions of coal measure gas and found high quality resources.The total geological resource quantity of coalbed methane and coal shale gas is 51.423×109 m3 and the geological resource abundance is up to 566×106 m3/km2.In this area,the coal measures are characterized by many layers of minable coal seams,large total thickness,thin to the medium thickness of the single layer,good gas-bearing property of coal seams and coal measure mudstone and sandstone,good reservoir physical property and high-pressure coefficient.According to the principle of combination of high quality and similarity of key parameters of the coal reservoir,the most favorable intervals are No.5-2,No.7 and No.13-2 coal seam in Well YMC1.And the pilot tests are carried out on coal seams and roof silty mudstone,such as staged perforation,increasing hydraulic fracturing scale and"three gas"production.The high and stable industrial gas flow with a daily gas output of more than 4000 m3 has been obtained,which has realized the breakthrough in the geological survey of coal measure gas in Southwest China.Based on the above investigation results,the geological characteristics of coal measure gas in the multi-thin-coal-seam-developed area and the coexploration and co-production methods,such as the optimization method of favorable intervals,the highefficiency fracturing and reservoir reconstruction method of coal measures,and the"three gas"drainage and production system,are systematically summarized in this paper.It will provide a reference for efficient exploration and development of coal measure gas in similar geological conditions in China.

Accumulation and exploration of continental shale gas resources of Cretaceous Shahezi Formation in Lishu fault depression,Songliao Basin,NE China

Distribution characteristics,organic matter development characteristics,gas-bearing characteristics,reservoir characteristics,and preservation conditions of the Shahezi Formation shale of Lower Cretaceous in the Lishu fault depression,Songliao Basin,NE China,are analyzed using organic geochemical,whole rock,and SEM analysis data,and CO_(2)and N_(2) adsorption and high-pressure mercury injection experiment data in combination with the tectonic and sedimentation evolution of the region to reveal the geological conditions for enrichment and resource potential of continental shale gas.The organic-rich shale in the Lower Cretaceous of the Lishu fault depression is mainly developed in the lower submember of the second member of the Shahezi Formation(K_(1)sh_(2)^(1) Fm.)and is thick and stable in distribution.The shale has high TOC,mainly types II_(1) and II_(2) organic matter,and is in the mature to the over-mature stage.The volcanic activity,salinization,and reduction of the water environment are conducive to the formation of the organic-rich shale.The shale reservoirs have mainly clay mineral intergranular pores,organic matter pores,carbonate mineral dissolution pores,and foliated microfractures as storage space.The pores are in the mesopore range of 10–50 nm,and the microfractures are mostly 5–10μm wide.Massive argillaceous rocks of lowland and highstand domains are deposited above and below the gas-bearing shale separately in the lower submember of the K_(1)sh_(2)^(1) Fm.,act as the natural roof and floor in the process of shale gas accumulation and preservation,and control the shale gas enrichment.Based on the above understandings,the first shale gas exploration well in Shahezi Formation was drilled in the Lishu fault depression of Songliao Basin.After fracturing,the well tested a daily gas production of 7.6×10^(4) m^(3),marking a breakthrough in continental shale gas exploration in the Shahezi Formation(K1 sh Fm.)of the Lishu fault depression in Songliao Basin.The exploration practice has reference significance for the exploration of continental shale gas in the Lower Cretaceous of Songliao Basin and its periphery.

A natural gas hydrate-oil-gas system in the Qilian Mountain permafrost area, northeast of Qinghai-Tibet Plateau

Natural gas hydrate,oil and gas were all found together in the Qilian Mountain permafrost area,northeast of Qinghai-Tibet Plateau,China.They are closely associated with each other in space,but whether they are in any genetic relations are unknown yet.In this paper,a hydrocarbon gas-generation series,gas-fluid migration series and hydrocarbon gas-accumulation series are analyzed to probe the spatial,temporal and genetic relationships among natural natural gas hydrate,oil and gas.The subsequent results show that natural gas hydrate,oil and gas actually form a natural gas hydrate-oil-gas system.Based on the Middle Jurassic and the Upper Triassic hydrocarbon gas-generation series,it is divided into four major sub-systems in the study area:(1)A conventional Upper Triassic gas-bearing sub-system with peak hydrocarbon gas-generation in the late Middle Jurassic;(2)a conventional Middle Jurassic oil-bearing sub-system with low to mature hydrocarbon gas-generation in the late Middle Jurassic;(3)a natural gas hydrate sub-system with main gas source from the Upper Triassic gas-bearing sub-system and minor gas source from the Middle Jurassic oil-bearing sub-system as well as little gas source from the Middle Jurassic coal-bed gas and the microbial gas;(4)a shallower gas sub-system with microbial alteration of the main gas source from the Upper Triassic gas-bearing sub-system.This natural gas hydrate-oil-gas system and its sub-systems are not only theoretical but also practical,and thus they will play an important role in the further exploration of natural gas hydrate,oil and gas,even other energy resources in the study area.

A review and research on comprehensive characterization of microscopic shale gas reservoir space

In this paper,substantial domestic and foreign research results of microscopic shale reservoir space were systemically reviewed,the research history consisting of simple observation and qualitative classification,quantitative research,the combination of qualitative and quantitative research successively as well as the characteristics of each research stage were summarized.In addition,the current problems existing in the characterization methods of shale reservoir space were also analyzed.Furthermore,based on massive actual detection of typical core samples obtained from more than 50 global shale gas wells and relevant practical experience,a comprehensive characterization method of combining qualitative with the semiquantitative characterization was put forward.In detail,the indicators of the qualitative characterization include pore combination type and organic-matter microscopic morphology type,while the core elements of the semi-quantitative characterization include the percentage of the organic-matter area and the plane porosity of the pores of different types.Based on the reference of the naming and classification of rocks,the three-end-member diagram method was used to characterize microscopic shale reservoir space.This is achieved by plotting the three end-member diagram of 3 kinds of first-order critical reservoir spaces,i.e.,organic-matter pores,matrix pores,and micro-fractures,in order to intuitively present the features of the microscopic pore combination.Meanwhile,statistic histograms of organic-matter microscopic morphology type and the plane porosity of different types of pores were adopted to characterize the development degree of second-order pores quantitatively.By this comprehensive characterization method,the importance of both pore combination and the microscopic morphology of organic matter were emphasized,revealing the control of organic-matter microscopic morphology over the organic-matter pores.What is more,high-resolution FE-SEM was adopted to obtain semi-quantitative statistics results.In this way,the features of pore development and pore combination were quantified,not only reflecting the types and storage capacity of the microscopic shale reservoir space,but also presenting the hydrocarbongenerating potential of organic matter in shale.Therefore,the results of this research are capable of providing in-depth microscopic information for the assessment and exploration and development of shale gas resources.