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剧烈-温和阳极氧化结合法快速制备有序阳极氧化铝膜的研究 被引量:3
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作者 郝爱文 黄丽清 +4 位作者 程龙 李新 张薇薇 单冬至 冯雪红 《无机材料学报》 SCIE EI CAS CSCD 北大核心 2014年第6期645-649,共5页
本研究采用剧烈–温和阳极氧化(hard anodization-mild anodization,HA-MA)结合快速制备高度有序多孔阳极氧化铝(porous anodic alumina,PAA)膜的方法,即先利用HA在铝表面快速形成有序凹坑阵列,然后再对表面留有有序凹坑的铝基进行温和... 本研究采用剧烈–温和阳极氧化(hard anodization-mild anodization,HA-MA)结合快速制备高度有序多孔阳极氧化铝(porous anodic alumina,PAA)膜的方法,即先利用HA在铝表面快速形成有序凹坑阵列,然后再对表面留有有序凹坑的铝基进行温和阳极氧化,制备出有序PAA膜。研究了剧烈阳极氧化时氧化电压、氧化时间对所制备PAA膜有序度的影响。研究结果表明,HA-MA结合法制备PAA膜的优化HA参数为:0.3 mol/L硫酸、80 V、10 min。HA-MA结合法所制备PAA膜的有序性和机械稳定性与二步温和阳极氧化法的相近,但形成有序PAA膜所需的时间为4.5 h,约为温和阳极氧化法的1/4,极大地提高了高度有序PAA膜的制备效率。 展开更多
关键词 多孔阳极氧化铝 温和阳极氧化法 剧烈阳极氧化法 剧烈-温和阳极氧化结合法
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低频带通与带阻自由切换的频率选择表面 被引量:4
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作者 徐阳 高劲松 +2 位作者 徐念喜 单冬至 宋乃涛 《光学精密工程》 EI CAS CSCD 北大核心 2018年第1期142-149,共8页
为了在不同时域下获得兼具带通与带阻空间滤波功能的低频频率选择表面(FSS),提出了一种带通与带阻型FSS可自由切换的设计方法,即在基于卷曲技术设计的小型化FSS表面上贴装电控PIN二极管,并利用"场-路"协同仿真的方法进行建模... 为了在不同时域下获得兼具带通与带阻空间滤波功能的低频频率选择表面(FSS),提出了一种带通与带阻型FSS可自由切换的设计方法,即在基于卷曲技术设计的小型化FSS表面上贴装电控PIN二极管,并利用"场-路"协同仿真的方法进行建模与计算。其中,卷曲图案既是滤波结构,也是馈电导线。当PIN二极管导通时,卷曲图案缝隙处产生的电容C1与金属贴片电感L1构成并联LC回路,FSS表现为带通滤波功能;反之,焊盘处缝隙及反偏PIN二极管产生的电容C2与金属贴片电感L2串联,FSS切换为带阻滤波功能。采用印刷线路板及表面贴装工艺制作出了400 mm×400mm试验样件并采用自由空间法进行测试,仿真与测试结果表明:在2.45GHz处,当PIN二极管导通时,FSS表现为强透射性能,反之则表现出强反射效果。这种基于电控PIN二极管开关所实现的带通与带阻型FSS自由切换方法在通信、电磁屏蔽及雷达隐身等领域具有广阔的应用前景。 展开更多
关键词 频率选择表面 “场-路”协同仿真 PIN二极管 电桥网络
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银三角纳米粒子的制备及其稳定性的研究
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作者 冯雪红 冯选旗 +10 位作者 黄丽清 徐忠峰 王军 张薇薇 刘悠 李新 程龙 耶红刚 翟立朋 单冬至 高萌 《光子学报》 EI CAS CSCD 北大核心 2014年第6期68-71,共4页
室温下,通过控制银种子胶体pH值,采用光诱导法制备出银三角纳米粒子,并对其表面增强喇曼散射活性和时间稳定性进行了实验研究.对比分析了新制备样品与在暗室中存放5个月样品的透射电子显微镜照片、紫外-可见吸收光谱和表面增强喇曼光谱... 室温下,通过控制银种子胶体pH值,采用光诱导法制备出银三角纳米粒子,并对其表面增强喇曼散射活性和时间稳定性进行了实验研究.对比分析了新制备样品与在暗室中存放5个月样品的透射电子显微镜照片、紫外-可见吸收光谱和表面增强喇曼光谱.结果表明:所制备的银三角纳米粒子在室温暗室中存放5个月后其几何形状、尺寸以及相应吸收峰的位置基本不变,具有较好的时间稳定性,对罗丹明6G探针分子仍具有较好的表面增强喇曼效应. 展开更多
关键词 纳米材料 等离子共振 光化学方法 银三角纳米粒子 吸收谱 表面增强喇曼光谱 时间稳定性
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Perforated nanocap array: Facile fabrication process and efficient surface enhanced Raman scattering with fluorescence suppression
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作者 王军 黄丽清 +7 位作者 童慧敏 翟立鹏 袁林 赵丽华 张薇薇 单冬至 郝爱文 冯雪红 《Chinese Physics B》 SCIE EI CAS CSCD 2013年第4期415-419,共5页
Recently, individual reduced-symmetry metal nanostructures and their plasmonic properties have been studied extensively. However, little attention has been paid to the approach to fabricating ordered reduced-symmetry ... Recently, individual reduced-symmetry metal nanostructures and their plasmonic properties have been studied extensively. However, little attention has been paid to the approach to fabricating ordered reduced-symmetry metal nanostructure arrays. In this paper, a novel perforated silver nanocap array with high surface-enhanced Raman scattering (SERS) activity and fluorescence suppression is reported. The array is fabricated by electron beam evaporating Ag onto the perforated barrier layer side of a hard anodization (HA) anodic aluminum oxide (AAO) template. The morphology and optical property of the perforated silver nanocap array are characterized by an atomic force microscope (AFM), a scanning electron microscope (SEM), and absorption spectra. The results of SERS measurements reveal that the perforated silver nanocap array offers high SERS activity and fluorescence suppression compared with an imperforated silver nanocap array. 展开更多
关键词 reduced-symmetry structures perforated nanocap array surface-enhanced Raman scattering anodic aluminum oxide
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Highly efficient optics/microwave beam splitter based on frequency selective surface
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作者 Qiao Sun Nianxi Xu +6 位作者 Haigui Yang Dongzhi Shan Yang Tang Xin Chen Tongtong Wang Jinsong Gao Yu Cai 《Chinese Optics Letters》 SCIE EI CAS 2024年第6期136-141,共6页
The development of hybrid optics/microwave communication systems puts forward a new requirement for beam splitters to efficiently transmit microwave signals and simultaneously reflect optical signals. Owing to mechani... The development of hybrid optics/microwave communication systems puts forward a new requirement for beam splitters to efficiently transmit microwave signals and simultaneously reflect optical signals. Owing to mechanical constraints, the physical thickness of beam splitters is of the order of tens of millimeters. The corresponding electrical thickness has the same order of magnitude as microwave wavelengths, and the resulting multi-beam interference effect significantly reduces the microwave transmittance, impacting the beam splitting quality.This study presents a new optics/microwave beam splitter based on the ability of the frequency selective surface(FSS) to shape the resonant curve. A beam splitter sample,whose physical thickness and substrate material are 20 mm and quartz glass, respectively, is designed, simulated, fabricated, and characterized to validate the feasibility of this strategy. The measured results show that the minimum microwave transmittance between 35 and 36.5 GHz with an incidence angle of 45° under TE polarization is 86.43%, and the mean value of the reflectance spectra from 450 to 900 nm and that from 7.7 to 10.5 μm both exceed 96%. This FSS-based optics/microwave beam splitter is expected to play a key role in hybrid optics/microwave communication systems. 展开更多
关键词 beam splitter multi-beam interference frequency selective surface high transmission
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A simple fabrication method of germanium-based metasurfaces
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作者 Dongzhi Shan Jinsong Gao +9 位作者 Nianxi Xu Naitao Song Hongda Wei Qiang Li Yi Zhao Hai Liu Qiao Sun Xiaonan Jiang Chao Li Zhiyu Zhang 《Chinese Optics Letters》 SCIE EI CAS 2024年第7期117-120,共4页
In this work,a simple fabrication method of germanium-based metasurfaces is proposed,where the deposited Al_(2)O_(3) layer with high selectivity is chosen as the hard mask and retained after the dry etching process.Th... In this work,a simple fabrication method of germanium-based metasurfaces is proposed,where the deposited Al_(2)O_(3) layer with high selectivity is chosen as the hard mask and retained after the dry etching process.The simulation and experimental characterization results verify the feasibility of the fabrication method.The experimental study on the fabrication methods of germanium-based metasurfaces is very significant as the meta-atoms with a higher refractive index can achieve 0 to 2πtransmission phase variation with a smaller period under the same thickness-to-period ratio,which is consistent with the requirement of the period miniaturization in some cases. 展开更多
关键词 metasurfaces period miniaturization refractive index.
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