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Pressure Generation above 35 GPa in a Walker-Type Large-Volume Press 被引量:4
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作者 尚宇琛 沈方韧 +11 位作者 侯旭远 陈璐瑶 胡阔 李鑫 刘然 陶强 朱品文 刘兆东 姚明光 周强 崔田 刘冰冰 《Chinese Physics Letters》 SCIE CAS CSCD 2020年第8期25-30,共6页
Pressure generation to a higher pressure range in a large-volume press(LVP)denotes our ability to explore more functional materials and deeper Earth's interior.Pressure generated by normal tungsten carbide(WC)anvi... Pressure generation to a higher pressure range in a large-volume press(LVP)denotes our ability to explore more functional materials and deeper Earth's interior.Pressure generated by normal tungsten carbide(WC)anvils in a commercial way is mostly limited to 25 GPa in LVPs due to the limitation of their hardness and design of cell assemblies.We adopt three newly developed WC anvils for ultrahigh pressure generation in a Walker-type LVP with a maximum press load of 1000 ton.The hardest ZK01F WC anvils exhibit the highest efficiency of pressure generation than ZK10F and ZK20F WC anvils,which is related to their performances of plastic deformations.Pressure up to 35 GPa at room temperature is achieved at a relatively low press load of 4.5 MN by adopting the hardest ZK01F WC anvils with three tapering surfaces in conjunction with an optimized cell assembly,while pressure above 35 GPa at 1700 K is achieved at a higher press load of 7.5 MN.Temperature above 2000 K can be generated by our cell assemblies at pressure below 30 GPa.We adopt such high-pressure and high-temperature techniques to fabricate several high-quality and well-sintered polycrystalline minerals for practical use.The present development of high-pressure techniques expands the pressure and temperature ranges in Walker-type LVPs and has wide applications in physics,materials,chemistry,and Earth science. 展开更多
关键词 CARBIDE INTERIOR POLYCRYSTALLINE
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高压下新型超硬非晶碳材料合成研究进展
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作者 尚宇琛 张盈 +1 位作者 姚明光 刘冰冰 《硅酸盐学报》 EI CAS CSCD 北大核心 2023年第4期1078-1090,共13页
非晶碳材料随着其内部sp^(3)杂化键成分的不断增加,展现出更加优异的力学、光学和热学性质.高压作为一种极端物理条件,可以有效促进材料中碳原子由sp^(2)向sp^(3)发生成键转变.本文介绍了近年来高压下新型超硬非晶碳材料合成与研究中取... 非晶碳材料随着其内部sp^(3)杂化键成分的不断增加,展现出更加优异的力学、光学和热学性质.高压作为一种极端物理条件,可以有效促进材料中碳原子由sp^(2)向sp^(3)发生成键转变.本文介绍了近年来高压下新型超硬非晶碳材料合成与研究中取得的一些成果和进展,主要利用富勒烯、玻璃碳等碳前驱体,研究其在高压、高温高压以及剪切应变下制备超硬非晶碳,及其结构转变机理.这些结果深化了对共价非晶材料微观结构转变以及其结构与性能之间关联的认识,基于此,对未来极端条件下超硬sp3非晶碳材料的合成做出了展望. 展开更多
关键词 非晶碳材料 高温高压 富勒烯 玻璃碳 超硬
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