Hierarchical porous Co_(3)O_(4)spheres were synthesized by a solvothermal method followed by high-temperature calcination.XRD,SEM,TEM and electrochemical tests were used to study the structure and performance of the h...Hierarchical porous Co_(3)O_(4)spheres were synthesized by a solvothermal method followed by high-temperature calcination.XRD,SEM,TEM and electrochemical tests were used to study the structure and performance of the hierarchical porous Co_(3)O_(4)spheres.The results show that the Co_(3)O_(4)synthesized at a calcination temperature of 700°C(Co_(3)O_(4)-700)is micro-sized spheres(1-2μm)consisting of plentiful nanoparticles(50-200 nm)and numerous pores(~100 nm).Due to its numerous porous morphology,the Co_(3)O_(4)-700 anode exhibits the highest cycling performance with excellent reversible discharge and charge specific capacities of 745 and 755 m A·h/g at the current density of 100 m A/g after 100 charge-discharge cycles,respectively.展开更多
利用"黑白衬度"金相和彩色金相技术研究五种铁碳合金(热轧态37Mn5、中温回火65Mn、铸态QT400-18L、热轧态P92超超临界钢和退火态20钢)和一种钛合金(热锻后淬火)的金相组织。研究结果表明,"黑白衬度"金相仅能用来观...利用"黑白衬度"金相和彩色金相技术研究五种铁碳合金(热轧态37Mn5、中温回火65Mn、铸态QT400-18L、热轧态P92超超临界钢和退火态20钢)和一种钛合金(热锻后淬火)的金相组织。研究结果表明,"黑白衬度"金相仅能用来观察传统碳钢和低合金钢的金相组织,试剂一(40 m L水+1 m L稀硝酸+0.5 g钼酸钠)、试剂二(盐酸(35%)+蒸馏水=1:5体积比(共100 m L)+0.5~1 g的焦亚硫酸钾)和热染法三种彩色金相方法能够清晰地观察球墨铸铁材料QT400-18L的铁素体基体晶界,且三种方法在操作性方面均较容易实现。热染法也可用来观察工业上批量化生产的碳钢和低合金钢的金相组织。展开更多
基金funded by the Natural Science Foundation of Hunan Province,China(No.2020JJ4729)。
文摘Hierarchical porous Co_(3)O_(4)spheres were synthesized by a solvothermal method followed by high-temperature calcination.XRD,SEM,TEM and electrochemical tests were used to study the structure and performance of the hierarchical porous Co_(3)O_(4)spheres.The results show that the Co_(3)O_(4)synthesized at a calcination temperature of 700°C(Co_(3)O_(4)-700)is micro-sized spheres(1-2μm)consisting of plentiful nanoparticles(50-200 nm)and numerous pores(~100 nm).Due to its numerous porous morphology,the Co_(3)O_(4)-700 anode exhibits the highest cycling performance with excellent reversible discharge and charge specific capacities of 745 and 755 m A·h/g at the current density of 100 m A/g after 100 charge-discharge cycles,respectively.
文摘利用"黑白衬度"金相和彩色金相技术研究五种铁碳合金(热轧态37Mn5、中温回火65Mn、铸态QT400-18L、热轧态P92超超临界钢和退火态20钢)和一种钛合金(热锻后淬火)的金相组织。研究结果表明,"黑白衬度"金相仅能用来观察传统碳钢和低合金钢的金相组织,试剂一(40 m L水+1 m L稀硝酸+0.5 g钼酸钠)、试剂二(盐酸(35%)+蒸馏水=1:5体积比(共100 m L)+0.5~1 g的焦亚硫酸钾)和热染法三种彩色金相方法能够清晰地观察球墨铸铁材料QT400-18L的铁素体基体晶界,且三种方法在操作性方面均较容易实现。热染法也可用来观察工业上批量化生产的碳钢和低合金钢的金相组织。
