A SiO2@PPy core/shell structure was synthesized by performing the polymerization of pyrrole monomers around SiO2 spheres.For the first time,the SiC hollow spheres with a high surface area was prepared from the SiO2@PP...A SiO2@PPy core/shell structure was synthesized by performing the polymerization of pyrrole monomers around SiO2 spheres.For the first time,the SiC hollow spheres with a high surface area was prepared from the SiO2@PPy with a core/shell structure by using a carbothermal reduction reaction technique.The preparation process and the structures of the products were characterized with XRD,TEM,SEM,N2 adsorption-desorption isotherms and XPS.The results indicate that β-SiC hollow spheres with a specific surface area of 101.3 m2/g could be prepared from the SiO2@PPy with a core/shell structure.展开更多
文摘A SiO2@PPy core/shell structure was synthesized by performing the polymerization of pyrrole monomers around SiO2 spheres.For the first time,the SiC hollow spheres with a high surface area was prepared from the SiO2@PPy with a core/shell structure by using a carbothermal reduction reaction technique.The preparation process and the structures of the products were characterized with XRD,TEM,SEM,N2 adsorption-desorption isotherms and XPS.The results indicate that β-SiC hollow spheres with a specific surface area of 101.3 m2/g could be prepared from the SiO2@PPy with a core/shell structure.
基金National Natural Science Foundation of China(51572172,51602332)Equipment Research Program(6140721050215)One-Hundred Talent Plan of Chinese Academy of Sciences
