An N38SH-grade magnet with low oxygen content was used to study the evolution of magnetic properties upon post-sin-tering annealing. Phase transformation of as-sintered magnet was investigated by differential scanning...An N38SH-grade magnet with low oxygen content was used to study the evolution of magnetic properties upon post-sin-tering annealing. Phase transformation of as-sintered magnet was investigated by differential scanning calorimetry (DSC). Three low temperature eutectic transition points were detected. Little change could be found when annealed below the lowest eutectic transition point. A wide annealing temperature range (460–560 oC) between the lowest and highest eutectic transition point was available for this magnet to achieve a relatively high coercivity (~1671 kA/m) at a relatively low Dy content (~3 wt.%). However, squareness fac-tor (SF) of the demagnetizing curve and its temperature stability were found to decrease after annealing above the highest eutectic transition point. This was attributed to the change of Cu content in the Nd-rich phase under different annealing temperatures.展开更多
基金Project supported by the National Natural Science Foundation of China(51171111)
文摘An N38SH-grade magnet with low oxygen content was used to study the evolution of magnetic properties upon post-sin-tering annealing. Phase transformation of as-sintered magnet was investigated by differential scanning calorimetry (DSC). Three low temperature eutectic transition points were detected. Little change could be found when annealed below the lowest eutectic transition point. A wide annealing temperature range (460–560 oC) between the lowest and highest eutectic transition point was available for this magnet to achieve a relatively high coercivity (~1671 kA/m) at a relatively low Dy content (~3 wt.%). However, squareness fac-tor (SF) of the demagnetizing curve and its temperature stability were found to decrease after annealing above the highest eutectic transition point. This was attributed to the change of Cu content in the Nd-rich phase under different annealing temperatures.