The reaction precursors were synthesised by solid state reaction of H 2C 2O 4·2H 2O with NiSO 4·6H 2O and Fe(NO 3) 3·9H 2O,CuSO 4·5H 2O,at room temperature.The brown black nanomater Ni 1.5 FeCu 2.5...The reaction precursors were synthesised by solid state reaction of H 2C 2O 4·2H 2O with NiSO 4·6H 2O and Fe(NO 3) 3·9H 2O,CuSO 4·5H 2O,at room temperature.The brown black nanomater Ni 1.5 FeCu 2.5 O 5.5 with the averages of 60nm was obtained by decomposition of precursors CuC 2O 4·2H 2O,Fe 2(C 2O 4) 3·5H 2O,and NiC 2O 4·2H 2O for about 3 hour at 410℃.The composition,size,appearance and properties of the product was studied by TG,XRD,TEM and SEM.展开更多
文摘The reaction precursors were synthesised by solid state reaction of H 2C 2O 4·2H 2O with NiSO 4·6H 2O and Fe(NO 3) 3·9H 2O,CuSO 4·5H 2O,at room temperature.The brown black nanomater Ni 1.5 FeCu 2.5 O 5.5 with the averages of 60nm was obtained by decomposition of precursors CuC 2O 4·2H 2O,Fe 2(C 2O 4) 3·5H 2O,and NiC 2O 4·2H 2O for about 3 hour at 410℃.The composition,size,appearance and properties of the product was studied by TG,XRD,TEM and SEM.
