Cylindrical samples of Ni-based GH4037 alloy were compressed at solid temperatures(1200,1250 and 1300℃) and semi-solid temperatures(1340,1350,1360,1370 and 1380℃) with different strain rates of 0.01,0.1 and 1 s-1.Hi...Cylindrical samples of Ni-based GH4037 alloy were compressed at solid temperatures(1200,1250 and 1300℃) and semi-solid temperatures(1340,1350,1360,1370 and 1380℃) with different strain rates of 0.01,0.1 and 1 s-1.High temperature deformation behavior and microstructure evolution of GH4037 alloy were investigated.The results indicated that flow stress decreased rapidly at semi-solid temperatures compared to that at solid temperatures.Besides,the flow stress continued to increase after reaching the initial peak stress at semi-solid temperatures when the strain rate was 1 s-1.With increasing the deformation temperature,the size of initial solid grains and recrystallized grains increased.At semi-solid temperatures,the grains were equiaxed,and liquid phase existed at the grain boundaries and inside the grains.Discontinuous dynamic recrystallization(DDRX) characterized by grain boundary bulging was the main nucleation mechanism for GH4037 alloy.展开更多
An equal channel reciprocating extrusion(ECRE)was proposed first to obtain a severe plastic deformation(SPD)of 7005 alloy.The microstructure and mechanical properties of one-pass ECREed(ECRE processed)7005 alloy were ...An equal channel reciprocating extrusion(ECRE)was proposed first to obtain a severe plastic deformation(SPD)of 7005 alloy.The microstructure and mechanical properties of one-pass ECREed(ECRE processed)7005 alloy were investigated.The results show that SPD occurring in ECRE leads to a mixed microstructure.ECREed 7005 alloy exhibits a significant improvement of ultimate tensile strength(UTS)and elongation.Mechanical properties in the region undergoing a complete ECRE process are higher than those in the region undergoing an incomplete ECRE process due to larger dislocation strengthening effect.Yield strength(YS)and UTS first decrease and then increase with an increase of extrusion temperature.The YS of 359.2 MPa,UTS of 490 MPa and elongation of 17.7%are obtained after T6 treatment.Fine-grain strengthening,dislocation strengthening and precipitation strengthening in the T6-treated ECREed sample all play important roles in improving the mechanical properties.展开更多
To shorten the preparation process of semi-solid billets,semi-solid billets of 2A14 aluminum alloy were prepared by wrought aluminum directly semi-solid isothermal treatment(WADSSIT)process.Three-dimension(3D)combined...To shorten the preparation process of semi-solid billets,semi-solid billets of 2A14 aluminum alloy were prepared by wrought aluminum directly semi-solid isothermal treatment(WADSSIT)process.Three-dimension(3D)combined microstructure evolution,namely transverse direction(TD)surface,rolling direction(RD)surface,and normal direction(ND)surface,was studied.Effects of temperature and holding time on average grain size and average shape factor were investigated.The results showed that the optimum conditions for preparation of 2A14 semi-solid billets by this process were 615℃ and 20 min(average grain size of 124μm and shape factor of 0.81).Electron backscatter diffraction(EBSD)observations indicated that the microstructure was completely recrystallized when it was heated to 600℃.Grain size was increased with the increase of temperature and grew up slowly with the holding time prolonging.Roundness was increased with increase of holding time but was not sensitive to temperature.展开更多
采用DSC测试、热镦粗实验、半固态等温处理实验、金相显微镜观察以及Image Pro Plus图像处理软件,研究了等温压缩温度、压缩量和半固态等温处理的温度、保温时间对再结晶重熔(RAP)法制备AlSi7Mg铝合金半固态坯料微观组织的影响。结果表...采用DSC测试、热镦粗实验、半固态等温处理实验、金相显微镜观察以及Image Pro Plus图像处理软件,研究了等温压缩温度、压缩量和半固态等温处理的温度、保温时间对再结晶重熔(RAP)法制备AlSi7Mg铝合金半固态坯料微观组织的影响。结果表明:等温压缩过程中温度对半固态坯料微观组织的影响不明显,而等温压缩变形量的增大有利于细化半固态坯料微观组织,最优热镦粗参数为温度240℃,变形量40%;半固态等温处理过程中,随保温温度升高,微观组织固相晶粒的尺寸逐渐增大,而随着保温时间延长,半固态组织中固相颗粒的尺寸先缓慢长大再迅速长大然后趋于不变,固相颗粒的圆整度变化较为复杂。通过RAP法制备的AlSi7Mg铝合金半固态坯料平均晶粒尺寸为64~117μm,形状因子为0.76~0.89。低于599℃时,半固态的平均晶粒尺寸的立方粗化线性关系不明显,影响晶粒粗化的机制主要有Ostwald熟化、合并长大、再结晶和熔化;在599℃时,晶粒尺寸的立方粗化线性关系较为明显,此时Ostwald熟化为晶粒粗化的主导机制。展开更多
基金Project(51575127)supported by the National Natural Science Foundation of China
文摘Cylindrical samples of Ni-based GH4037 alloy were compressed at solid temperatures(1200,1250 and 1300℃) and semi-solid temperatures(1340,1350,1360,1370 and 1380℃) with different strain rates of 0.01,0.1 and 1 s-1.High temperature deformation behavior and microstructure evolution of GH4037 alloy were investigated.The results indicated that flow stress decreased rapidly at semi-solid temperatures compared to that at solid temperatures.Besides,the flow stress continued to increase after reaching the initial peak stress at semi-solid temperatures when the strain rate was 1 s-1.With increasing the deformation temperature,the size of initial solid grains and recrystallized grains increased.At semi-solid temperatures,the grains were equiaxed,and liquid phase existed at the grain boundaries and inside the grains.Discontinuous dynamic recrystallization(DDRX) characterized by grain boundary bulging was the main nucleation mechanism for GH4037 alloy.
基金This work is supported by the National Natural Science Foundation of China(51875124).
文摘An equal channel reciprocating extrusion(ECRE)was proposed first to obtain a severe plastic deformation(SPD)of 7005 alloy.The microstructure and mechanical properties of one-pass ECREed(ECRE processed)7005 alloy were investigated.The results show that SPD occurring in ECRE leads to a mixed microstructure.ECREed 7005 alloy exhibits a significant improvement of ultimate tensile strength(UTS)and elongation.Mechanical properties in the region undergoing a complete ECRE process are higher than those in the region undergoing an incomplete ECRE process due to larger dislocation strengthening effect.Yield strength(YS)and UTS first decrease and then increase with an increase of extrusion temperature.The YS of 359.2 MPa,UTS of 490 MPa and elongation of 17.7%are obtained after T6 treatment.Fine-grain strengthening,dislocation strengthening and precipitation strengthening in the T6-treated ECREed sample all play important roles in improving the mechanical properties.
基金financially supported by the National Natural Science Foundation of China (No.51875124)the National Key Research and Development Project,China (No.2019YFB2006503)。
文摘To shorten the preparation process of semi-solid billets,semi-solid billets of 2A14 aluminum alloy were prepared by wrought aluminum directly semi-solid isothermal treatment(WADSSIT)process.Three-dimension(3D)combined microstructure evolution,namely transverse direction(TD)surface,rolling direction(RD)surface,and normal direction(ND)surface,was studied.Effects of temperature and holding time on average grain size and average shape factor were investigated.The results showed that the optimum conditions for preparation of 2A14 semi-solid billets by this process were 615℃ and 20 min(average grain size of 124μm and shape factor of 0.81).Electron backscatter diffraction(EBSD)observations indicated that the microstructure was completely recrystallized when it was heated to 600℃.Grain size was increased with the increase of temperature and grew up slowly with the holding time prolonging.Roundness was increased with increase of holding time but was not sensitive to temperature.
文摘采用DSC测试、热镦粗实验、半固态等温处理实验、金相显微镜观察以及Image Pro Plus图像处理软件,研究了等温压缩温度、压缩量和半固态等温处理的温度、保温时间对再结晶重熔(RAP)法制备AlSi7Mg铝合金半固态坯料微观组织的影响。结果表明:等温压缩过程中温度对半固态坯料微观组织的影响不明显,而等温压缩变形量的增大有利于细化半固态坯料微观组织,最优热镦粗参数为温度240℃,变形量40%;半固态等温处理过程中,随保温温度升高,微观组织固相晶粒的尺寸逐渐增大,而随着保温时间延长,半固态组织中固相颗粒的尺寸先缓慢长大再迅速长大然后趋于不变,固相颗粒的圆整度变化较为复杂。通过RAP法制备的AlSi7Mg铝合金半固态坯料平均晶粒尺寸为64~117μm,形状因子为0.76~0.89。低于599℃时,半固态的平均晶粒尺寸的立方粗化线性关系不明显,影响晶粒粗化的机制主要有Ostwald熟化、合并长大、再结晶和熔化;在599℃时,晶粒尺寸的立方粗化线性关系较为明显,此时Ostwald熟化为晶粒粗化的主导机制。
