A one-pot synthesis of a series of 5-oxo-5,6,7,8-tetrahydro-4H-benzo-[b]-pyran derivatives via three-component coupling reactions of aldehydes, dimedone and malononitrilein room temperature ionic liquids (RTILs) wit...A one-pot synthesis of a series of 5-oxo-5,6,7,8-tetrahydro-4H-benzo-[b]-pyran derivatives via three-component coupling reactions of aldehydes, dimedone and malononitrilein room temperature ionic liquids (RTILs) without any catalyst has been reported. In the meantime, the reuse of ionic liquids and the effect of different ionic liquids as solvent on the reaction have also been investigated.展开更多
基金Project supported by the National Natural Science Foundation of China (Nos. 20172039, 20472062) and Jiangsu Provincial Key Laboratory of Fine Petrochemical Technology (No. KF0402).
文摘A one-pot synthesis of a series of 5-oxo-5,6,7,8-tetrahydro-4H-benzo-[b]-pyran derivatives via three-component coupling reactions of aldehydes, dimedone and malononitrilein room temperature ionic liquids (RTILs) without any catalyst has been reported. In the meantime, the reuse of ionic liquids and the effect of different ionic liquids as solvent on the reaction have also been investigated.