In this paper, the characteristics of separating xylitol, arabinitol and sorbitol with uniformly loaded columns containing 2,5,7 and 9wt% XE-60 and gradient loaded columns are compared in detail. The suspended chain c...In this paper, the characteristics of separating xylitol, arabinitol and sorbitol with uniformly loaded columns containing 2,5,7 and 9wt% XE-60 and gradient loaded columns are compared in detail. The suspended chain curve formulaY=en (x-a/2) +e-n (x-a/2) is suggested for calculation of amount of different coated packing in the gradient loaded column, where selector coefficient n=l.l, a is average liquid loading amount, x is individual liquid loading amount. The gradient loaded column can not only satisfactorily separate isomers of xylitol and arabinitol, but also shorten retention time of sorbitol obviously.展开更多
文摘In this paper, the characteristics of separating xylitol, arabinitol and sorbitol with uniformly loaded columns containing 2,5,7 and 9wt% XE-60 and gradient loaded columns are compared in detail. The suspended chain curve formulaY=en (x-a/2) +e-n (x-a/2) is suggested for calculation of amount of different coated packing in the gradient loaded column, where selector coefficient n=l.l, a is average liquid loading amount, x is individual liquid loading amount. The gradient loaded column can not only satisfactorily separate isomers of xylitol and arabinitol, but also shorten retention time of sorbitol obviously.
