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微波辐射下一步合成2-芳基-4,5-二苯基咪唑衍生物 被引量:3
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作者 周建峰 陆惠锋 +2 位作者 顾惠丹 朱玉兰 屠树江 《应用化学》 CAS CSCD 北大核心 2005年第8期918-919,共2页
A series of 2-aryl-4,5-diphenylimidazoles were synthesized by one-step condensation reaction of (aromatic) aldehyde, diphenyl diketone and ammonium acetate(molar ratio 112) in acetic acid under microwave irradiati... A series of 2-aryl-4,5-diphenylimidazoles were synthesized by one-step condensation reaction of (aromatic) aldehyde, diphenyl diketone and ammonium acetate(molar ratio 112) in acetic acid under microwave irradiation. Products were characterized by mp, IR, (1H NMR), MS and elemental analysis, and their melting points are identical to those of the known compounds reported in the literature. The reaction time was 411 min and the yield 70%98%. Its a low energy (consumption), environmentally benign, and easy process. 展开更多
关键词 芳基咪唑 二苯基二(甲)酮 芳醛 微波辐射 合成
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微波辐射下双亚苄基环己酮衍生物的合成 被引量:1
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作者 许世道 陈芳 +1 位作者 周建峰 陆惠锋 《合成化学》 CAS CSCD 2004年第6期526-528,共3页
芳醛与环己酮在碳酸钠水溶液中 ,用微波辐射相转移催化法合成了α ,α′ 双亚苄基环己酮 ( 3a~ 3j) ,其中 3c ,3i和 3j为新化合物。
关键词 α α′-双亚苄己酮 芳醛 环己酮 微波辐射 相转移催化
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