The nanosized binary mixed oxides of Zn/Sn had been prepared by the fractional homogeneous precipitation route using urea as the latent precipitant under boiling reflux condition The samples prepared with the differen...The nanosized binary mixed oxides of Zn/Sn had been prepared by the fractional homogeneous precipitation route using urea as the latent precipitant under boiling reflux condition The samples prepared with the different initial concentrations of urea or calcined at different temperatures had been investigated by X-ray diffration （XRD） or transmission electron microscopy （TEM）. The calcination temperature had obvious effect on the phase composition and the crystal size of the samples attained, and the precipitant concentration also had obvious effect on the oxide particles size and the production rate of ZnO.展开更多
基金Acknowledgments： This work was supported by the National Natural Science Foundation of China （No. 20673042）, the Natural Science Foundation of Anhui Provincial Education Committee （No. K12007B014）, the Natural Science Foundation of Anhui Province （No. 070415211）, China Postdoctoral Science Foundation （No. 2004036511）, the Laboratory Open Foundation of Green Materials Chemistry （No. KLSF（I）09）, and the Laboratory Open Foundation of Guangdong Public Laboratory of Environmental Science and Technology. The authors thank Mr. LUO S. M., Mr. CHEN D. Z., and Mr. TAO Q. for their assistance.
文摘The nanosized binary mixed oxides of Zn/Sn had been prepared by the fractional homogeneous precipitation route using urea as the latent precipitant under boiling reflux condition The samples prepared with the different initial concentrations of urea or calcined at different temperatures had been investigated by X-ray diffration （XRD） or transmission electron microscopy （TEM）. The calcination temperature had obvious effect on the phase composition and the crystal size of the samples attained, and the precipitant concentration also had obvious effect on the oxide particles size and the production rate of ZnO.
