Flower-like microstructured nickel was synthesized by a facile mixed-solvent thermal process. The structure, morphology, and magnetic properties of the reaction products were investigated, respectively, by X-ray diffr...Flower-like microstructured nickel was synthesized by a facile mixed-solvent thermal process. The structure, morphology, and magnetic properties of the reaction products were investigated, respectively, by X-ray diffraction （XRD）, scanning electron microscopy （SEM）, and vibrating sample magnetometry （VSM）. The results showed that the products consisted of a face-centered cubic （fcc） structure with lattice constant of u=3.524A. The average diameter of flower-like microstructured nickel was about 5 um and the thickness of a single flake was about 100nm. Magnetic measurement showed that these powders exhibited ferromagnetic characteristics.展开更多
基金provided by the National Natural Science Foundation of China (11164027)the Project of regional scientific research program of Xinjiang, China(06018805)
文摘Flower-like microstructured nickel was synthesized by a facile mixed-solvent thermal process. The structure, morphology, and magnetic properties of the reaction products were investigated, respectively, by X-ray diffraction （XRD）, scanning electron microscopy （SEM）, and vibrating sample magnetometry （VSM）. The results showed that the products consisted of a face-centered cubic （fcc） structure with lattice constant of u=3.524A. The average diameter of flower-like microstructured nickel was about 5 um and the thickness of a single flake was about 100nm. Magnetic measurement showed that these powders exhibited ferromagnetic characteristics.
