[Objectives]The paper was to establish the quality standard of Shenqi Qiangjing granules and to conduct routine inspection of granular dosage forms.[Methods]The particle size,moisture,loss on drying,dissolubility,cont...[Objectives]The paper was to establish the quality standard of Shenqi Qiangjing granules and to conduct routine inspection of granular dosage forms.[Methods]The particle size,moisture,loss on drying,dissolubility,content uniformity and microbial limit of Shenqi Qiangjing granules were detected.Radix Astragali,Herba Epimedii,Radix Dipsaci and Fructus Schisandrae Chinensis were qualitatively identified by thin layer chromatography(TLC).[Results]The particle size,moisture,loss on drying,dissolubility,content uniformity and microbial limit of Shenqi Qiangjing granules were all in line with the relevant regulations of Pharmacopoeia of the People's Republic of China(2020 edition).Radix Astragali,Herba Epimedii,Radix Dipsaci and Fructus Schisandrae Chinensis had clear fluorescent spots in TLC assay,and no such spots were found in negative control.[Conclusions]The method has the advantages of simple operation,accurate and reliable results,strong specificity and good repeatability,and can effectively control the quality of Shenqi Qiangjing granules.展开更多
提出了一种基于传导冷却的紧凑型中能段电子束离子阱杂质光谱研究平台的系统设计方案,用于未来聚变堆上金属杂质原子光谱研究。系统设计主要包括磁场计算、内电极设计、光谱仪设计及其他辅助系统设计。通过使用COMSOL仿真软件对磁场和...提出了一种基于传导冷却的紧凑型中能段电子束离子阱杂质光谱研究平台的系统设计方案,用于未来聚变堆上金属杂质原子光谱研究。系统设计主要包括磁场计算、内电极设计、光谱仪设计及其他辅助系统设计。通过使用COMSOL仿真软件对磁场和电子束进行了辅助设计,仿真结果显示,合适的设计参数可以使电子束离子阱(Electron Beam Ion Trap,EBIT)漂移管中心得到1.0 T的均匀磁场强度,电子束可以在漂移管中被约束并通过漂移管到达收集极,此设计可为进一步工程设计提供设计参数参考。展开更多
The dominant wavelength range of edge impurity emissions moves from the visible range to the vacuum ultraviolet(VUV)range,as heating power increasing in the Experimental Advanced Superconducting Tokamak(EAST).The meas...The dominant wavelength range of edge impurity emissions moves from the visible range to the vacuum ultraviolet(VUV)range,as heating power increasing in the Experimental Advanced Superconducting Tokamak(EAST).The measurement provided by the existing visible spectroscopies in EAST is not sufficient for impurity transport studies for high-parameters plasmas.Therefore,in this study,a VUV spectroscopy is newly developed to measure edge impurity emissions in EAST.One Seya-Namioka VUV spectrometer(McPherson 234/302)is used in the system,equipped with a concave-corrected holographic grating with groove density of 600 grooves mm-1.Impurity line emissions can be observed in the wavelength range ofλ=50-700 nm,covering VUV,near ultraviolet and visible ranges.The observed vertical range is Z=-350-350 mm.The minimum sampling time can be set to 5 ms under full vertical binning(FVB)mode.VUV spectroscopy has been used to measure the edge impurity emission for the 2019 EAST experimental campaign.Impurity spectra are identified for several impurity species,i.e.,lithium(Li),carbon(C),oxygen(O),and iron(Fe).Several candidates for tungsten(W)lines are also measured but their clear identification is very difficult due to a strong overlap with Fe lines.Time evolutions of impurity carbon emissions of CⅡat 134.5 nm and CⅢat 97.7 nm are analyzed to prove the system capability of time-resolved measurement.The measurements of the VUV spectroscopy are very helpful for edge impurity transport study in the high-parameters plasma in EAST.展开更多
基金Supported by Guangxi Key Research and Development Project(GK AB2203-5073)Guangxi TCM Appropriate Technology Development and Promotion Project(GZSY22-18)Research Project of Guangxi Administration of Traditional Chinese Medicine(GXZYZ20210209,GXZYA20220180).
文摘[Objectives]The paper was to establish the quality standard of Shenqi Qiangjing granules and to conduct routine inspection of granular dosage forms.[Methods]The particle size,moisture,loss on drying,dissolubility,content uniformity and microbial limit of Shenqi Qiangjing granules were detected.Radix Astragali,Herba Epimedii,Radix Dipsaci and Fructus Schisandrae Chinensis were qualitatively identified by thin layer chromatography(TLC).[Results]The particle size,moisture,loss on drying,dissolubility,content uniformity and microbial limit of Shenqi Qiangjing granules were all in line with the relevant regulations of Pharmacopoeia of the People's Republic of China(2020 edition).Radix Astragali,Herba Epimedii,Radix Dipsaci and Fructus Schisandrae Chinensis had clear fluorescent spots in TLC assay,and no such spots were found in negative control.[Conclusions]The method has the advantages of simple operation,accurate and reliable results,strong specificity and good repeatability,and can effectively control the quality of Shenqi Qiangjing granules.
文摘提出了一种基于传导冷却的紧凑型中能段电子束离子阱杂质光谱研究平台的系统设计方案,用于未来聚变堆上金属杂质原子光谱研究。系统设计主要包括磁场计算、内电极设计、光谱仪设计及其他辅助系统设计。通过使用COMSOL仿真软件对磁场和电子束进行了辅助设计,仿真结果显示,合适的设计参数可以使电子束离子阱(Electron Beam Ion Trap,EBIT)漂移管中心得到1.0 T的均匀磁场强度,电子束可以在漂移管中被约束并通过漂移管到达收集极,此设计可为进一步工程设计提供设计参数参考。
基金the National Magnetic Confinement Fusion Science Program of China(Nos.2017YFE0301300 and 2018YFE0301100)National Natural Science Foundation of China(Nos.11805231,11705151)+4 种基金ASIPP Science and Research Grant(No.DSJJ-17-03)Key Program of Research and Development of Hefei Science Center(No.2017HSC-KPRD002)Anhui Provincial Natural Sci-ence Foundation(Nos.1808085QA14 and 1908085J01)Instrument Developing Project of the Chinese Academy of Sciences(No.YJKYYQ20180013)Collaborative Innovation Program of Hefei Science Center,CAS(No.2019HSC-CIP005).
文摘The dominant wavelength range of edge impurity emissions moves from the visible range to the vacuum ultraviolet(VUV)range,as heating power increasing in the Experimental Advanced Superconducting Tokamak(EAST).The measurement provided by the existing visible spectroscopies in EAST is not sufficient for impurity transport studies for high-parameters plasmas.Therefore,in this study,a VUV spectroscopy is newly developed to measure edge impurity emissions in EAST.One Seya-Namioka VUV spectrometer(McPherson 234/302)is used in the system,equipped with a concave-corrected holographic grating with groove density of 600 grooves mm-1.Impurity line emissions can be observed in the wavelength range ofλ=50-700 nm,covering VUV,near ultraviolet and visible ranges.The observed vertical range is Z=-350-350 mm.The minimum sampling time can be set to 5 ms under full vertical binning(FVB)mode.VUV spectroscopy has been used to measure the edge impurity emission for the 2019 EAST experimental campaign.Impurity spectra are identified for several impurity species,i.e.,lithium(Li),carbon(C),oxygen(O),and iron(Fe).Several candidates for tungsten(W)lines are also measured but their clear identification is very difficult due to a strong overlap with Fe lines.Time evolutions of impurity carbon emissions of CⅡat 134.5 nm and CⅢat 97.7 nm are analyzed to prove the system capability of time-resolved measurement.The measurements of the VUV spectroscopy are very helpful for edge impurity transport study in the high-parameters plasma in EAST.
