Plasma electrolytic oxidation(PEO) processes were carried out to produce ceramic layers on 6061 aluminum substrates in four kinds of electrolytes such as silicate and aluminate solution with and without sodium fluoros...Plasma electrolytic oxidation(PEO) processes were carried out to produce ceramic layers on 6061 aluminum substrates in four kinds of electrolytes such as silicate and aluminate solution with and without sodium fluorosilicate.The PEO processes were carried out under a hybrid voltage(260 V DC combined with 200 V,60 Hz AC amplitude) at room temperature for 5 min.The composition,microstructure and element distribution analyses of the PEO-treated layers were carried out by XRD and SEM & EDS.The effect of the electrolyte contents on the growth mechanism,element distribution and properties of oxide layers were studied.It is obvious that the layers generated in aluminate solutions show smoother surfaces than those in silicate solutions.Moreover,an addition of fluorine ion can effectively control the layer porosity;therefore,it can enhance the properties of the layers.展开更多
Nano-particles have several interesting properties which are not shown in bulk materials because of their high ratio of surface area to volume. FeCo alloy nano-particles with soft magnetic properties are demanded for ...Nano-particles have several interesting properties which are not shown in bulk materials because of their high ratio of surface area to volume. FeCo alloy nano-particles with soft magnetic properties are demanded for various applications such as optics, eletronics and magnetics. Through the polyol method, highly purified particles with mono-dispersibility in various sizes can be produced and used as high-tech functional materials. In this study, the magnetic characteristics of FeCo alloy with Ag seed added in the production process of mono-dispersed nano-particles through the polyol method were investigated.展开更多
基金Korea Research Foundation Grant (KRF-2006-005-J02703)
文摘Plasma electrolytic oxidation(PEO) processes were carried out to produce ceramic layers on 6061 aluminum substrates in four kinds of electrolytes such as silicate and aluminate solution with and without sodium fluorosilicate.The PEO processes were carried out under a hybrid voltage(260 V DC combined with 200 V,60 Hz AC amplitude) at room temperature for 5 min.The composition,microstructure and element distribution analyses of the PEO-treated layers were carried out by XRD and SEM & EDS.The effect of the electrolyte contents on the growth mechanism,element distribution and properties of oxide layers were studied.It is obvious that the layers generated in aluminate solutions show smoother surfaces than those in silicate solutions.Moreover,an addition of fluorine ion can effectively control the layer porosity;therefore,it can enhance the properties of the layers.
基金supported by the MKE(The Min-istry of Knowledge Economy),Korea,the ITRC(Information Technology Research Center) Support program supervised by the NIPA(National IT Industry Promotion Agency),No.NIPA-2010-C1090-1021-0015
文摘Nano-particles have several interesting properties which are not shown in bulk materials because of their high ratio of surface area to volume. FeCo alloy nano-particles with soft magnetic properties are demanded for various applications such as optics, eletronics and magnetics. Through the polyol method, highly purified particles with mono-dispersibility in various sizes can be produced and used as high-tech functional materials. In this study, the magnetic characteristics of FeCo alloy with Ag seed added in the production process of mono-dispersed nano-particles through the polyol method were investigated.