Dislocation structures in polycrystalline Ni 3Al alloy doped with palladium deformed at room temperature have been investigated by transmission electron microscopy. The structure consists mainly of dislocations dissoc...Dislocation structures in polycrystalline Ni 3Al alloy doped with palladium deformed at room temperature have been investigated by transmission electron microscopy. The structure consists mainly of dislocations dissociated into a /2〈011〉 super partials bounding an anti phase boundary (APB). Dislocations dissociated into a /3〈112〉 super Shockley partials bounding a superlattice intrinsic stacking fault (SISF) are also common debris. The majority of the SISFs are truncated loops, i.e. the partials bounding the SISF are of similar Burgers vector. These faulted loops are generated from APB coupled dislocations, according to a mechanism for formation of SISFs proposed by Suzuki et al , and recently modified by Chiba et al . The APB energies for {111} and {010} slip planes are measured to be 144±20 mJ/m 2 and 102±11 mJ/m 2 respectively, and the SISF energy has been estimated to be 12 mJ/m 2 in this alloy. It is concluded that the dislocation structure in Ni 74.5 Pd 2Al 23.5 alloy deformed at room temperature is similar to that in binary Ni 3Al, and the difference in fault energies between these two alloys is small. Thus, it seems unlikely that the enhancement of ductility of Ni 74.5 Pd 2Al 23.5 results from only such a small decrease of the ordering energy of the alloy. SISF bounding dislocations also have no apparent influence on the ductilization of Ni 74.5 Pd 2Al 23.5 alloy.展开更多
Brittle pro-eutectoid cementite that forms along prior-austenite in hypereutectoid steels is deleterious to mechanical properties. The optimum process parameters which suppress the formation of pro-eutectoid cementite...Brittle pro-eutectoid cementite that forms along prior-austenite in hypereutectoid steels is deleterious to mechanical properties. The optimum process parameters which suppress the formation of pro-eutectoid cementite in hypereutectoid steels with carbon content in the range of 0.8%-1.3% in mass fraction, were investigated. Pro-eutectoid cementite formation is effectively hindered by increasing the deformation temperature and decreasing the amount of strain. Transformation at lower temperatures close to the nose of the cooling-transformation diagram also reduces the tendency of the formation of pro-eutectoid cementite. Control of prior-austenite grain size and grain boundary conditions is important. Due to larger number of nucleation sites, finer prior-austenite grain size results in the acceleration of transformation to pro-eutectoid cementite. However, large prior-austenite and straight boundaries lead to less nucleation sites of pro-eutectoid cementite. The cooling rate and carbon content should be reduced as much as possible. The transformation temperature below 660 °C and the strain of 0.5 at deformation temperature of 850 °C are suggested.展开更多
Proton resonant states in 22Mg have been investigated by the resonant elastic scattering of 21Na+p. The 21Na beam with a mean energy of 4.00 MeV/u was separated by the CNS radioactive ion beam separator(CRIB) and bomb...Proton resonant states in 22Mg have been investigated by the resonant elastic scattering of 21Na+p. The 21Na beam with a mean energy of 4.00 MeV/u was separated by the CNS radioactive ion beam separator(CRIB) and bombarded a thick(CH2)n target. The energy spectra of recoiled protons were measured at scattering angles of θcm ≈172° and 146°,respectively. A new state at 7.06 MeV has been observed clearly and another new one at 7.28 MeV is tentatively identified due to its low statistics. The proton resonant parameters were deduced from an R-matrix analysis of the differential cross section data. The astrophysical resonant reaction rate for the 18Ne(α,p)21Na reaction has been estimated,and it is about five times larger than that assumed before.展开更多
文摘Dislocation structures in polycrystalline Ni 3Al alloy doped with palladium deformed at room temperature have been investigated by transmission electron microscopy. The structure consists mainly of dislocations dissociated into a /2〈011〉 super partials bounding an anti phase boundary (APB). Dislocations dissociated into a /3〈112〉 super Shockley partials bounding a superlattice intrinsic stacking fault (SISF) are also common debris. The majority of the SISFs are truncated loops, i.e. the partials bounding the SISF are of similar Burgers vector. These faulted loops are generated from APB coupled dislocations, according to a mechanism for formation of SISFs proposed by Suzuki et al , and recently modified by Chiba et al . The APB energies for {111} and {010} slip planes are measured to be 144±20 mJ/m 2 and 102±11 mJ/m 2 respectively, and the SISF energy has been estimated to be 12 mJ/m 2 in this alloy. It is concluded that the dislocation structure in Ni 74.5 Pd 2Al 23.5 alloy deformed at room temperature is similar to that in binary Ni 3Al, and the difference in fault energies between these two alloys is small. Thus, it seems unlikely that the enhancement of ductility of Ni 74.5 Pd 2Al 23.5 results from only such a small decrease of the ordering energy of the alloy. SISF bounding dislocations also have no apparent influence on the ductilization of Ni 74.5 Pd 2Al 23.5 alloy.
基金Project(51222405)supported by the National Science Foundation for Outstanding Young Scholars of ChinaProject(51034002)supported by the National Natural Science Foundation of China+1 种基金Project(132002)supported by the Fok Ying Tong Education Foundation,ChinaProject(N120502001)supported by the Basic Scientific Research Operation of Center University of China
文摘Brittle pro-eutectoid cementite that forms along prior-austenite in hypereutectoid steels is deleterious to mechanical properties. The optimum process parameters which suppress the formation of pro-eutectoid cementite in hypereutectoid steels with carbon content in the range of 0.8%-1.3% in mass fraction, were investigated. Pro-eutectoid cementite formation is effectively hindered by increasing the deformation temperature and decreasing the amount of strain. Transformation at lower temperatures close to the nose of the cooling-transformation diagram also reduces the tendency of the formation of pro-eutectoid cementite. Control of prior-austenite grain size and grain boundary conditions is important. Due to larger number of nucleation sites, finer prior-austenite grain size results in the acceleration of transformation to pro-eutectoid cementite. However, large prior-austenite and straight boundaries lead to less nucleation sites of pro-eutectoid cementite. The cooling rate and carbon content should be reduced as much as possible. The transformation temperature below 660 °C and the strain of 0.5 at deformation temperature of 850 °C are suggested.
基金Japanese Ministry of Education, Culture,Sports,and Technology,Japan(13440071,14740156)Grants-in-Aids for JSPS,Japan(1604055)
文摘Proton resonant states in 22Mg have been investigated by the resonant elastic scattering of 21Na+p. The 21Na beam with a mean energy of 4.00 MeV/u was separated by the CNS radioactive ion beam separator(CRIB) and bombarded a thick(CH2)n target. The energy spectra of recoiled protons were measured at scattering angles of θcm ≈172° and 146°,respectively. A new state at 7.06 MeV has been observed clearly and another new one at 7.28 MeV is tentatively identified due to its low statistics. The proton resonant parameters were deduced from an R-matrix analysis of the differential cross section data. The astrophysical resonant reaction rate for the 18Ne(α,p)21Na reaction has been estimated,and it is about five times larger than that assumed before.
