The addition Of Pb enhances the hightemperature stability as well as theproportion of the high Tphase in Bi-Sr-Ca-Cu-O superconductor.The sample A with nominal composi-tion of BiSrCaCuOwas synthesized bySolid state re...The addition Of Pb enhances the hightemperature stability as well as theproportion of the high Tphase in Bi-Sr-Ca-Cu-O superconductor.The sample A with nominal composi-tion of BiSrCaCuOwas synthesized bySolid state reaction.It was sintered in airat 1153K for 24h,followed by annealingat 773K for 24h and furnace-cooling.The sample B with a nominal compositionof BiPbSrCaCuOwas prepared bymixing PbO with the powder ofBiSrCaCuOwhich had been prefired at1113K for 24h,pressing,sintering at展开更多
文摘The addition Of Pb enhances the hightemperature stability as well as theproportion of the high Tphase in Bi-Sr-Ca-Cu-O superconductor.The sample A with nominal composi-tion of BiSrCaCuOwas synthesized bySolid state reaction.It was sintered in airat 1153K for 24h,followed by annealingat 773K for 24h and furnace-cooling.The sample B with a nominal compositionof BiPbSrCaCuOwas prepared bymixing PbO with the powder ofBiSrCaCuOwhich had been prefired at1113K for 24h,pressing,sintering at