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Fe_2O_3-TiO_2纳米复合颗粒的激光控制合成研究
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作者 陈岁元 张一坤 +1 位作者 daniel wellburn 刘常升 《东北大学学报(自然科学版)》 EI CAS CSCD 北大核心 2013年第2期205-208,共4页
以微米级的5%Fe2O3粉末和95%TiO2粉末(以质量分数计)形成混合靶材,利用脉冲激光气相蒸发-液相收集控制合成新方法制备Fe2O3-TiO2复合纳米颗粒.采用透射电子显微镜(TEM)、X射线衍射(XRD)、红外光谱、UV光谱检测等测试技术,对实验制备的... 以微米级的5%Fe2O3粉末和95%TiO2粉末(以质量分数计)形成混合靶材,利用脉冲激光气相蒸发-液相收集控制合成新方法制备Fe2O3-TiO2复合纳米颗粒.采用透射电子显微镜(TEM)、X射线衍射(XRD)、红外光谱、UV光谱检测等测试技术,对实验制备的样品的形貌、组织结构、光吸收性能及合成机理等进行了系统研究.结果表明:用气相蒸发-液相收集激光法制备的Fe2O3-TiO2纳米颗粒外观呈球形,平均粒径约为40 nm,颗粒呈链状连接趋势;Fe2O3的复合改善了TiO2纳米颗粒的磁性.对样品在800~200 nm区间进行光谱分析,发现Fe2O3复合TiO2后,样品光谱发生红移,改善了TiO2纳米颗粒的光催化性能. 展开更多
关键词 脉冲激光 Fe2O3-TiO2复合纳米颗粒 合成 光谱红移
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Fabrication of wear-resistant layers with lamellar eutectic structure by laser surface alloying using the in situ reaction between Cr and B_4C 被引量:1
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作者 You-zheng Sun Jin-bao Li +1 位作者 daniel wellburn Chang-sheng Liu 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2016年第11期1294-1301,共8页
To improve the wear resistance of Cr5 steel, wear-resistant layers with lamellar eutectic microstructure were fabricated by laser surface alloying(LSA), which is dependent on the in situ reaction between Cr and B_4C... To improve the wear resistance of Cr5 steel, wear-resistant layers with lamellar eutectic microstructure were fabricated by laser surface alloying(LSA), which is dependent on the in situ reaction between Cr and B_4C. Our results indicated that the hypoeutectic structures of the LSA layers were divided into interdendritic eutectic structures and dendrites. The area fraction of the eutectic structures increased with increasing laser scanning speed, which improved the hardness and wear resistance of the LSA layers. The average hardness of the LSA layer prepared at a scanning speed of 8 mm/s was HV_(0.2) 883.9, which was 1.8 times greater than that of the traditional quenched layer(approximately HV 480). After sliding for 659.4 m, the specimen prepared at a scanning speed of 8 mm/s exhibited a volume loss of 0.0323 mm^3, which was only 29.5% of the volume loss of the traditional quenched specimen. 展开更多
关键词 eutectic wear resistance laser alloying hardness
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