Micrometer NbC_x-C three-dimensional netted fibers were synthesized by thecarbothermal method under 0.1 MPa of N_2 ambient atmosphere at a relatively low temperature. Rawmaterials were commercial powders of Nb_2O_5 (9...Micrometer NbC_x-C three-dimensional netted fibers were synthesized by thecarbothermal method under 0.1 MPa of N_2 ambient atmosphere at a relatively low temperature. Rawmaterials were commercial powders of Nb_2O_5 (99.95 percent), reactive carbon (99.99 percent), NaCl(99.95 percent) and sucrose (99.94 percent). The relationship of the fabrication processing with thecomposition, crystal structure and morphology of fibers was investigated. The formation mechanismwas also proposed and discussed.展开更多
基金The authors gratefully acknowledge financial support from Key Technologies R&D Program Foundation of China(02BA312B07)the National Natural Science Foundation of China(No.20303011)Natural Science Foundation of Shandong Province(Y 2001 B08).
基金This work was financially supported by the National Nature Science Foundation of China(No.59425007, No.59432033).
文摘Micrometer NbC_x-C three-dimensional netted fibers were synthesized by thecarbothermal method under 0.1 MPa of N_2 ambient atmosphere at a relatively low temperature. Rawmaterials were commercial powders of Nb_2O_5 (99.95 percent), reactive carbon (99.99 percent), NaCl(99.95 percent) and sucrose (99.94 percent). The relationship of the fabrication processing with thecomposition, crystal structure and morphology of fibers was investigated. The formation mechanismwas also proposed and discussed.
