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Crystal and Molecular Structure of Di-chloro-bis(р-methylphenylbutylsulfide) Palladium(Ⅱ)
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作者 guo song-shan Cui Li +1 位作者 Wang Hang-Zhang Qian Pu(Department of Chemistry, University of Suzhou, Suzhou 215006)Yu Kai-Bei(Chengdu Center of Analysis and Determination, Academic Sinica, Chengdu, 610041) 《Chinese Journal of Structural Chemistry》 SCIE CAS CSCD 1994年第1期16-18,共3页
Pd (p-CH3C6H4SC4H9)2Cl2C(22)H(32)CL2S2Pd , MR= 537. 92, space group P21/c, a=10. 336(2) , b=8. 657(1) ,c=14. 452(2) A, β=105. 19(1)°, V = 1247. 9(3) A3, Z=2 , Dc= 1. 43 g/cm ̄(-3), MoKα radiation,μ=11. 16 cm-1... Pd (p-CH3C6H4SC4H9)2Cl2C(22)H(32)CL2S2Pd , MR= 537. 92, space group P21/c, a=10. 336(2) , b=8. 657(1) ,c=14. 452(2) A, β=105. 19(1)°, V = 1247. 9(3) A3, Z=2 , Dc= 1. 43 g/cm ̄(-3), MoKα radiation,μ=11. 16 cm-1,F(000) = 552 , R= 0. 030 for 2417 reflections with I】3a(Ⅰ) .Pd (Ⅱ) is coordinated by two chloride atoms and two sulfur atoms of organic ligands, forming a transsquare planar with Pd-S of 2. 316(1) and Pd-Cl of 2. 303(1) A. 展开更多
关键词 crystal structure palladium complex chloro-methylphenylbutyl-sulfide-palladium
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