AlCoCrFeNi_(2.1)eutectic high entropy alloy(EHEA)and AlCoCrFeNi_(2.1)-x NbC(x=2.5wt%,5.0wt%,7.5wt%,and 10wt%)high entropy alloy(HEAs)were prepared by mechanical alloying(MA).The effects of milling time and NbC content...AlCoCrFeNi_(2.1)eutectic high entropy alloy(EHEA)and AlCoCrFeNi_(2.1)-x NbC(x=2.5wt%,5.0wt%,7.5wt%,and 10wt%)high entropy alloy(HEAs)were prepared by mechanical alloying(MA).The effects of milling time and NbC content on the alloying behavior and grain size of the AlCoCrFeNi_(2.1)EHEA were investigated.The experimental results show that the AlCoCrFeNi_(2.1)EHEA primarily consists of order BCC(B2)and face-centered-cubic(FCC)phases,while the AlCoCrFeNi_(2.1)-x NbC(x=2.5wt%,5.0wt%,7.5wt%,and 10wt%)HEAs are composed of B2,FCC,and NbC phases.With the increase of milling time,the powder goes through three stages,irregularity,cold welding fracture and spheroidization.The particle size of AlCoCrFeNi_(2.1)EHEA powder shows a trend of first increasing and then decreasing.Therein,the particle size presents a normal distribution during 0-50 h alloying.With the addition of NbC,the AlCoCrFeNi_(2.1)-x NbC HEAs powders are significantly refined.And the degree of grain refinement gradually increases with the increase of NbC content.展开更多
基金Funded by the Natural Science Foundation of Shandong Province (Nos.ZR2020QE019)the National Natural Science Foundation of China (Nos.51901116)the China Postdoctoral Science Fund (2021M692724)。
文摘AlCoCrFeNi_(2.1)eutectic high entropy alloy(EHEA)and AlCoCrFeNi_(2.1)-x NbC(x=2.5wt%,5.0wt%,7.5wt%,and 10wt%)high entropy alloy(HEAs)were prepared by mechanical alloying(MA).The effects of milling time and NbC content on the alloying behavior and grain size of the AlCoCrFeNi_(2.1)EHEA were investigated.The experimental results show that the AlCoCrFeNi_(2.1)EHEA primarily consists of order BCC(B2)and face-centered-cubic(FCC)phases,while the AlCoCrFeNi_(2.1)-x NbC(x=2.5wt%,5.0wt%,7.5wt%,and 10wt%)HEAs are composed of B2,FCC,and NbC phases.With the increase of milling time,the powder goes through three stages,irregularity,cold welding fracture and spheroidization.The particle size of AlCoCrFeNi_(2.1)EHEA powder shows a trend of first increasing and then decreasing.Therein,the particle size presents a normal distribution during 0-50 h alloying.With the addition of NbC,the AlCoCrFeNi_(2.1)-x NbC HEAs powders are significantly refined.And the degree of grain refinement gradually increases with the increase of NbC content.