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四氢黄连碱中间体的合成
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作者 欧文涛 李旺 +6 位作者 王李平 庞易英 杨陈阳 郭文彬 张雪松 黄双平 王晓季 《江西科技师范大学学报》 2019年第6期67-70,共4页
以高原儿茶酸为起始原料,经甲基化、溴化、偶联反应、酯水解、缩合酰化,五步反应得到目标化合物四氢黄连碱中间体,总收率64%。利用核磁共振对各中间体及目标化合物的化学结构进行了表征。
关键词 四氢黄连碱 高原儿茶酸 中间体
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Room temperature H_2S micro-sensors with anti-humidity properties fabricated from NiO-In_2O_3 composite nanofibers 被引量:1
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作者 YUE XueJun HONG TianSheng +1 位作者 YANG Zhou huang shuangping 《Science China(Technological Sciences)》 SCIE EI CAS 2013年第3期821-826,共6页
NiO-In2O3 composite nanofibers are synthesized via electrospinning and calcining techniques. Micro-sensors are fabricated by sputtering Pt electrodes on Si chips to form sensor substrates, and then spinning the NiO-In... NiO-In2O3 composite nanofibers are synthesized via electrospinning and calcining techniques. Micro-sensors are fabricated by sputtering Pt electrodes on Si chips to form sensor substrates, and then spinning the NiO-In2O3 composite nanofibers onto the sensor substrate surface. The as-fabricated micro-sensors exhibit excellent H2S sensing properties at room temperature. The sensi- tivity of the micro-sensors is up to 6 when the sensors are exposed to 3 μL/L HzS, and the corresponding response and recovery times are 14 and 22 s, respectively. The micro-sensors also exhibit high selectivity and good stability. Especially, the micro-sensors can operate at various humidity conditions. The sensitivity of the micro-sensors is 3.8 to 3 μL/L HzS at 75% relative humidity. These characteristics make the micro-sensors good candidates for practical H2S sensors with high performance. 展开更多
关键词 gas sensors NANOFIBERS micro-sensors metal oxide semiconductors NANOMATERIALS
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