The hot deformation behavior of a medium-Mn steel was studied in terms of hot compression flow curves in the temperature range of 850–1050 ℃ and strain rates of 0.05–10 s-1.The thermo-mechanical analysis was carrie...The hot deformation behavior of a medium-Mn steel was studied in terms of hot compression flow curves in the temperature range of 850–1050 ℃ and strain rates of 0.05–10 s-1.The thermo-mechanical analysis was carried out and suggested that the microstructure during deformation was completely austenite which had high tendency for dynamic recrystallization(DRX).The flow behavior was characterized by significant flow softening at deformation temperatures of 950–1050 ℃ and lower strain rates of 0.05–5 s-1, which was attributed to heating during deformation, DRX and flow instability.A step-by-step calculating procedure for constitutive equations is proposed.The verification of the modified equations indicated that the developed constitutive models could accurately describe the flow softening behavior of studied steel.Additionally, according to the processing maps and microstructure analysis, it suggested that hot working of medium Mn steel should be carried out at 1050 ℃, and the strain rate of 0.05–10 s-1 resulted in significantly recrystallized microstructures in the in steel.The flow localization is mainly flow instability mechanism for experimental steel.展开更多
Low-temperature ausforming(LT-AF)prior to bainitic transformation leads to a noticeable acceleration of bainitic transformation kinetics;however,the effect of LT-AF on the retained austenite(RA)features and the result...Low-temperature ausforming(LT-AF)prior to bainitic transformation leads to a noticeable acceleration of bainitic transformation kinetics;however,the effect of LT-AF on the retained austenite(RA)features and the resulting mechanical properties is still unclear.LT-AF was applied to ultrahigh-strength bainitic steel before austempering.The deformation behavior and the resulting dislocation substructures were investigated by thermomechanical simulator and transmission electron microscopy(TEM).The planar dislocation structures produced during deformation at 350℃ accelerate the bainitic transformation kinetics during isothermal holding.The effect of LT-AF on the bainitic transformation kinetics and the features of RA was elucidated via dilatometer measurement,TEM,scanning electron microscopy,and X-ray diffraction.It is observed that LT-AF not only retains more RA content but also facilitates improved RA stability.This trend is mainly due to the large amounts of planar dislocations in RA and bainitic laths inherited from undercooled austenite caused by LT-AF,the decrease in bainitic sheaves size,and the increase in filmy RA content compared to the sample without ausforming.A large fraction of filmy RA with high stability and the refinement of bainitic sheaves obtained by LT-AF remarkably enhance the strain hardening capacity and achieve significantly better ductility compared to the directly austempered sample.展开更多
In order to further optimize welding process of Nb-Ti-Mo microalloyed steel, welding thermal cycles on coarse-grained heat-affected zone (CGHAZ) of welded joints were simulated using Gleeble 1500. The microstructure...In order to further optimize welding process of Nb-Ti-Mo microalloyed steel, welding thermal cycles on coarse-grained heat-affected zone (CGHAZ) of welded joints were simulated using Gleeble 1500. The microstructure and low-temperature impact fracture were investigated using a scanning electron microscope and a pendulum impact machine, respectively. Moreover, the relationship between cooling time ts/5 and the microstructure of CGHAZ was discussed, and the effect of microstructure on impact toughness was also studied. As cooling time increased, martensite fraction decreased from 97.8% (3 s) to 3.0% (60 s). The fraction of martensite/austenite (M/A) constituent increased from 2.2% (3 s) to 39.0% (60 s), its shape changed from granular to strip, and the maximum length increased from 2.4 μm (3 s) to 7.0 μm (60 s). As cooling time increased, the prior austenite grain size increased from 34.0 μm (3 s) to 49.0 gm (60 s), the impact absorption energy reduced from 101.8 J (5 s) to 7.2 J (60 s), and the fracture mechanism changed from quasi-cleavage fracture to cleavage fracture. The decreased toughness of CGHAZ was due to the reduction of lath martensite-content, coarsening of original austenite grain, and increase and coarsening of M/A constituent. The heat input was controlled under 7 kJ cm-1 during actual welding for these steels.展开更多
Low-carbon (0.08 wt% C) steel has been subjected to three different heat treatments to obtain dual-phase steels with different microstructures. An understanding of structure-property was established through tensile ...Low-carbon (0.08 wt% C) steel has been subjected to three different heat treatments to obtain dual-phase steels with different microstructures. An understanding of structure-property was established through tensile tests, in conjunction with scanning electron microscope and transmission electron microscope. The results show that the steel after intermediate quenching (IQ) consisting of fine and fibrous martensite exhibited the intermediate strength, highest elongation and the best comprehensive performance of mechanical properties, whereas the steel subjected to intercritical annealing (IA) produced a network martensite along ferrite grain boundaries, having the lowest strength and intermediate elongation. Besides, step quenching (SQ) resulted in a coarse and blocky ferrite-martensite microstructure showing the worst mechanical properties of the three different heat-treatment conditions. The strain-hardening behavior was studied through the modified Crussard- Jaoul model, indicating two stages of strain-hardening behavior for all three samples. The highest magnitude of strain- hardening ability was obtained by IQ annealing routes. The analysis of the fractured surface revealed that ferrite/martensite interfaces are the most susceptible for microvoid nucleation. However, martensite microcracks were also observed in SQ sample, and the microvoids are nucleated within the ferrite grain in IA sample as well. The variations in strength, elongation, strain-hardening behavior and fracture mechanism of the steel with different heat-treatment schedules were further discussed in relation to the microstructural features.展开更多
Different initial microstructures were obtained through combination of intercritical annealing and cold-rolling. Subsequently, steels with different microstructures of ferrite-pearlite (FP), ferrite-martensite (FM...Different initial microstructures were obtained through combination of intercritical annealing and cold-rolling. Subsequently, steels with different microstructures of ferrite-pearlite (FP), ferrite-martensite (FM) and complete martensite (M) were intercritically annealed at 780 ℃ for 5 min and water quenched to obtain ferrite-martensite microstructure. The significance of initial microstructures on ultimate microstructure, mechanical properties, strain-hardening ability and fracture behavior in dual-phase steels has been elucidated. Initial microstructures of FP, FM and M yielded different martensite morphologies, notably chain-like network structure, fine and fibrous martensite structure, respectively. Furthermore, with increasing martensite content in the initial microstructure, the average grain size of ferrite was significantly refined from about 12.3 to 2.1 μm, which results in that the ultimate tensile strength (UTS) and yield strength were increased, total elongation remained unaffected, and uniform elongation (UE) and strain-hardening ability were increased. A comparison of mechanical properties for different initial microstructures suggested that when the initial microstructure was complete martensite, the steel had excellent mechanical properties, with UTS × UE of 122.5 J cm^-3, which was 24% greater than the conventional continuously annealed steels with ferrite-pearlite initial microstructure (98.8 J cm^-3). The variation in tensile properties, strain-hardening ability and fracture mechanism of steels with different initial microstructures were discussed in relation to the ultimate microstructures.展开更多
基金financially supported by the National Natural Science Foundation of China (No.51775102)the National key research and development plan (2017YF0703001)
文摘The hot deformation behavior of a medium-Mn steel was studied in terms of hot compression flow curves in the temperature range of 850–1050 ℃ and strain rates of 0.05–10 s-1.The thermo-mechanical analysis was carried out and suggested that the microstructure during deformation was completely austenite which had high tendency for dynamic recrystallization(DRX).The flow behavior was characterized by significant flow softening at deformation temperatures of 950–1050 ℃ and lower strain rates of 0.05–5 s-1, which was attributed to heating during deformation, DRX and flow instability.A step-by-step calculating procedure for constitutive equations is proposed.The verification of the modified equations indicated that the developed constitutive models could accurately describe the flow softening behavior of studied steel.Additionally, according to the processing maps and microstructure analysis, it suggested that hot working of medium Mn steel should be carried out at 1050 ℃, and the strain rate of 0.05–10 s-1 resulted in significantly recrystallized microstructures in the in steel.The flow localization is mainly flow instability mechanism for experimental steel.
基金The financial support provided by the National Natural Science Foundation of China(No.U1808208)the Fundamental Research Funds for the Central Universities(N2107005)is gratefully acknowledged.
文摘Low-temperature ausforming(LT-AF)prior to bainitic transformation leads to a noticeable acceleration of bainitic transformation kinetics;however,the effect of LT-AF on the retained austenite(RA)features and the resulting mechanical properties is still unclear.LT-AF was applied to ultrahigh-strength bainitic steel before austempering.The deformation behavior and the resulting dislocation substructures were investigated by thermomechanical simulator and transmission electron microscopy(TEM).The planar dislocation structures produced during deformation at 350℃ accelerate the bainitic transformation kinetics during isothermal holding.The effect of LT-AF on the bainitic transformation kinetics and the features of RA was elucidated via dilatometer measurement,TEM,scanning electron microscopy,and X-ray diffraction.It is observed that LT-AF not only retains more RA content but also facilitates improved RA stability.This trend is mainly due to the large amounts of planar dislocations in RA and bainitic laths inherited from undercooled austenite caused by LT-AF,the decrease in bainitic sheaves size,and the increase in filmy RA content compared to the sample without ausforming.A large fraction of filmy RA with high stability and the refinement of bainitic sheaves obtained by LT-AF remarkably enhance the strain hardening capacity and achieve significantly better ductility compared to the directly austempered sample.
基金This work was financially supported by the National Natural Science Foundation of China (No. 51775102), Open Research Fund from the State Key Laboratory of Roiling and Automation, Northeastern University (No. 2016005) and Project Funded by China Postdoctoral Science Foundation (No. 2016M601877).
文摘In order to further optimize welding process of Nb-Ti-Mo microalloyed steel, welding thermal cycles on coarse-grained heat-affected zone (CGHAZ) of welded joints were simulated using Gleeble 1500. The microstructure and low-temperature impact fracture were investigated using a scanning electron microscope and a pendulum impact machine, respectively. Moreover, the relationship between cooling time ts/5 and the microstructure of CGHAZ was discussed, and the effect of microstructure on impact toughness was also studied. As cooling time increased, martensite fraction decreased from 97.8% (3 s) to 3.0% (60 s). The fraction of martensite/austenite (M/A) constituent increased from 2.2% (3 s) to 39.0% (60 s), its shape changed from granular to strip, and the maximum length increased from 2.4 μm (3 s) to 7.0 μm (60 s). As cooling time increased, the prior austenite grain size increased from 34.0 μm (3 s) to 49.0 gm (60 s), the impact absorption energy reduced from 101.8 J (5 s) to 7.2 J (60 s), and the fracture mechanism changed from quasi-cleavage fracture to cleavage fracture. The decreased toughness of CGHAZ was due to the reduction of lath martensite-content, coarsening of original austenite grain, and increase and coarsening of M/A constituent. The heat input was controlled under 7 kJ cm-1 during actual welding for these steels.
基金financially supported by the National Key Project of Scientific and Technical Supporting Programs of China (No. 2011CB606306-2)the National Natural Science Foundation of China (Grant No. 51204048)
文摘Low-carbon (0.08 wt% C) steel has been subjected to three different heat treatments to obtain dual-phase steels with different microstructures. An understanding of structure-property was established through tensile tests, in conjunction with scanning electron microscope and transmission electron microscope. The results show that the steel after intermediate quenching (IQ) consisting of fine and fibrous martensite exhibited the intermediate strength, highest elongation and the best comprehensive performance of mechanical properties, whereas the steel subjected to intercritical annealing (IA) produced a network martensite along ferrite grain boundaries, having the lowest strength and intermediate elongation. Besides, step quenching (SQ) resulted in a coarse and blocky ferrite-martensite microstructure showing the worst mechanical properties of the three different heat-treatment conditions. The strain-hardening behavior was studied through the modified Crussard- Jaoul model, indicating two stages of strain-hardening behavior for all three samples. The highest magnitude of strain- hardening ability was obtained by IQ annealing routes. The analysis of the fractured surface revealed that ferrite/martensite interfaces are the most susceptible for microvoid nucleation. However, martensite microcracks were also observed in SQ sample, and the microvoids are nucleated within the ferrite grain in IA sample as well. The variations in strength, elongation, strain-hardening behavior and fracture mechanism of the steel with different heat-treatment schedules were further discussed in relation to the microstructural features.
文摘Different initial microstructures were obtained through combination of intercritical annealing and cold-rolling. Subsequently, steels with different microstructures of ferrite-pearlite (FP), ferrite-martensite (FM) and complete martensite (M) were intercritically annealed at 780 ℃ for 5 min and water quenched to obtain ferrite-martensite microstructure. The significance of initial microstructures on ultimate microstructure, mechanical properties, strain-hardening ability and fracture behavior in dual-phase steels has been elucidated. Initial microstructures of FP, FM and M yielded different martensite morphologies, notably chain-like network structure, fine and fibrous martensite structure, respectively. Furthermore, with increasing martensite content in the initial microstructure, the average grain size of ferrite was significantly refined from about 12.3 to 2.1 μm, which results in that the ultimate tensile strength (UTS) and yield strength were increased, total elongation remained unaffected, and uniform elongation (UE) and strain-hardening ability were increased. A comparison of mechanical properties for different initial microstructures suggested that when the initial microstructure was complete martensite, the steel had excellent mechanical properties, with UTS × UE of 122.5 J cm^-3, which was 24% greater than the conventional continuously annealed steels with ferrite-pearlite initial microstructure (98.8 J cm^-3). The variation in tensile properties, strain-hardening ability and fracture mechanism of steels with different initial microstructures were discussed in relation to the ultimate microstructures.