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镧对铽荧光增强效应测定药物加替沙星胶囊中的加替沙星含量
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作者 赵悦辉 李烨 +7 位作者 谭博 马丽丽 王冠乔 李刚 宋冬雪 AbdullahAbdu Ahmed 郑极慧 吕玉光 《药物资讯》 2012年第2期15-20,共6页
探讨第四代喹诺酮类药物加替沙星与稀土离子铽离子形成的配合物的荧光特性。应用荧光分光光度计测定药物加替沙星与稀土离子铽离子形成的配合物的荧光强度,通过加入表面活性剂、加入共发光离子La3+、改变溶液的pH等增敏方法选择最佳条... 探讨第四代喹诺酮类药物加替沙星与稀土离子铽离子形成的配合物的荧光特性。应用荧光分光光度计测定药物加替沙星与稀土离子铽离子形成的配合物的荧光强度,通过加入表面活性剂、加入共发光离子La3+、改变溶液的pH等增敏方法选择最佳条件。镧对该体系具有较强的荧光增强效应,最佳的pH值为7.5,选用0.1 mol·L–1 NH4Cl-HCl效果最佳,加替沙星的最佳浓度为1.0*10–6 mol·L–1。对荧光新体系的荧光增强作用的机理进行了初步探讨,最终建立了Tb3+-La3+-GFLX-SDS新体系,上述研究对于稀土元素分析、生物和药物分析都具有潜在的应用价值,为稀土和喹诺酮类药物配合物的相关研究提供了一定的理论和实验基础,可以用于测定人工合成样品和制剂的含量,该方法选择性好,灵敏度高,结果令人满意。 展开更多
关键词 稀土离子 喹诺酮类 加替沙星 荧光分光光度法
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Long-distance ranging with high precision using a soliton microcomb 被引量:11
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作者 JINDONG WANG ZHIZHOU LU +9 位作者 WEIQIANG WANG FUMIN ZHANG JIAWEI CHEN YANG WANG jihui zheng SAI T.CHU WEI ZHAO BRENT E.LITTLE XINGHUA QU WENFU ZHANG 《Photonics Research》 SCIE EI CAS CSCD 2020年第12期1964-1972,共9页
Laser-based light detection and ranging(lidar)plays a significant role in both scientific and industrial areas.However,it is difficult for existing lidars to achieve high speed,high precision,and long distance simulta... Laser-based light detection and ranging(lidar)plays a significant role in both scientific and industrial areas.However,it is difficult for existing lidars to achieve high speed,high precision,and long distance simultaneously.Here,we demonstrate a high-performance lidar based on a chip-scaled soliton microcomb(SMC)that can realize all three specialties simultaneously.Aided by the excellent properties of ultrahigh repetition rate and the smooth envelope of the SMC,traditional optical frequency comb(OFC)-based dispersive interferometry is heavily improved and the measuring dead zone induced by the mismatch between the repetition rate of the OFC and resolution of the optical spectrum analyzer is totally eliminated.Combined with an auxiliary dual-frequency phase-modulated laser range finder,the none-dead-zone measurable range ambiguity is extended up to 1500 m.The proposed SMC lidar is experimentally implemented in both indoor and outdoor environment.In the outdoor baseline field,real-time,high-speed(up to 35 k Hz)measurement of a long distance of^1179 m is achieved with a minimum Allan deviation of 5.6μm at an average time of 0.2 ms(27 nm at an average time of 1.8 s after high-pass filtering).The present SMC lidar approaches a compact,fast,high-precision,and none-dead zone long-distance ranging system,aimed at emerging applications of frontier basic scientific research and advances in industrial manufacturing. 展开更多
关键词 LIDAR SOLITON HIGH
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