Qualification of polarization can be realized either on a macroscopic scale as an average property by P-E hysteresis measurements or on a nano/micro scale by piezoelectric force microscopy,transmission electron micros...Qualification of polarization can be realized either on a macroscopic scale as an average property by P-E hysteresis measurements or on a nano/micro scale by piezoelectric force microscopy,transmission electron microscopy,scanning electron microscopy,and so on.However,visualization and qualification of polarization distribution in the micron to millimeter scale is still a challenge.Polarizing light microscopy(PLM)is often used in the study of ferroelectric domain structures mainly for domain patterns.A phe-nomenon called“chromatic polarization”has been observed in transparent ferroelectric crystals by using a crossed-PLM system viewed with white light,which contains rich information about local polariza-tion distribution.In this study,an automatic full-angle light intensity detection(AFALID)algorithm com-bined with colorimetry is developed to analyze the distribution of nonuniform local spontaneous polar-ization distribution in transparent ferroelectric single crystals.Temperature-dependent spontaneous po-larizations from the color analysis for PMN-0.36PT single crystals with single tetragonal domain state are in good coincidence with those extracted from temperature-dependent hysteresis loops and pyroelectric current measurements.We further apply this method to quantify the nonuniform domain distributions with nano-indentations.This non-contact and non-destructive characterization can provide fast and au-tomatic detection of polarization distributions in ferroelectric materials.展开更多
In this paper,0.36Pb(Ni_(1/3)Nb_(2/3))O_(3)-0.24PbZrO3-0.40PbTiO_(3)(PNN-PZT)ceramic was prepared,and texture engineering was performed on this PNN-PZT ceramic to improve its electromechanical properties and temperatu...In this paper,0.36Pb(Ni_(1/3)Nb_(2/3))O_(3)-0.24PbZrO3-0.40PbTiO_(3)(PNN-PZT)ceramic was prepared,and texture engineering was performed on this PNN-PZT ceramic to improve its electromechanical properties and temperature stability.Single element ultra-sonic transducers were prepared using PNN-PZT,PNN-PZT textured ceramics,and their performance were evaluated and com-pared using a PZT-5H ceramic based transducer as the benchmark.It is shown that the sensitivity and bandwidth of the PNN-PZT textured ceramic-based transducer are much superior to regular PNN-PZT ceramic and PZT-5H ceramic based transducers.展开更多
基金This work is financially supported by the National Key Re-search and Development Program of China(No.2021YFF0501001)the Heilongjiang Provincial Natural Science Foundation of China(No.LH2020A006)the Open Fund of Key Laboratory for In-telligent Nano Materials and Devices of the Ministry of Education NJ2022002(No.INMD-2022M08).
文摘Qualification of polarization can be realized either on a macroscopic scale as an average property by P-E hysteresis measurements or on a nano/micro scale by piezoelectric force microscopy,transmission electron microscopy,scanning electron microscopy,and so on.However,visualization and qualification of polarization distribution in the micron to millimeter scale is still a challenge.Polarizing light microscopy(PLM)is often used in the study of ferroelectric domain structures mainly for domain patterns.A phe-nomenon called“chromatic polarization”has been observed in transparent ferroelectric crystals by using a crossed-PLM system viewed with white light,which contains rich information about local polariza-tion distribution.In this study,an automatic full-angle light intensity detection(AFALID)algorithm com-bined with colorimetry is developed to analyze the distribution of nonuniform local spontaneous polar-ization distribution in transparent ferroelectric single crystals.Temperature-dependent spontaneous po-larizations from the color analysis for PMN-0.36PT single crystals with single tetragonal domain state are in good coincidence with those extracted from temperature-dependent hysteresis loops and pyroelectric current measurements.We further apply this method to quantify the nonuniform domain distributions with nano-indentations.This non-contact and non-destructive characterization can provide fast and au-tomatic detection of polarization distributions in ferroelectric materials.
基金This work was supported by the National Natural Science Foundation of China(Grant No.51975160).
文摘In this paper,0.36Pb(Ni_(1/3)Nb_(2/3))O_(3)-0.24PbZrO3-0.40PbTiO_(3)(PNN-PZT)ceramic was prepared,and texture engineering was performed on this PNN-PZT ceramic to improve its electromechanical properties and temperature stability.Single element ultra-sonic transducers were prepared using PNN-PZT,PNN-PZT textured ceramics,and their performance were evaluated and com-pared using a PZT-5H ceramic based transducer as the benchmark.It is shown that the sensitivity and bandwidth of the PNN-PZT textured ceramic-based transducer are much superior to regular PNN-PZT ceramic and PZT-5H ceramic based transducers.
