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低聚倍半硅氧烷基铁络合物阻燃剂的合成及改性环氧树脂 被引量:6
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作者 曾碧榕 陈锦梅 +4 位作者 胡蓉 刘新瑜 陈国荣 郑薇 戴李宗 《高分子材料科学与工程》 EI CAS CSCD 北大核心 2019年第6期1-9,共9页
采用Kabachnik-Fields反应合成出含有邻苯二酚功能团、磷杂菲基团和笼型倍半硅氧烷结构基元的新型配体POSS-DOPO-Catechol(PDC),再与Fe^3+配位络合形成低聚倍半硅氧烷基铁络合物Fe(PDC)3,进一步加入双酚A型环氧树脂(EP)进行固化制备出EP... 采用Kabachnik-Fields反应合成出含有邻苯二酚功能团、磷杂菲基团和笼型倍半硅氧烷结构基元的新型配体POSS-DOPO-Catechol(PDC),再与Fe^3+配位络合形成低聚倍半硅氧烷基铁络合物Fe(PDC)3,进一步加入双酚A型环氧树脂(EP)进行固化制备出EP/Fe(PDC)3复合材料。利用红外、质谱和核磁共振表征配体及络合物的化学结构;通过差示扫描量热分析、热重分析、氧指数测定、微形量热、动态力学实验等方法研究铁络合物Fe(PDC)3的引入对环氧树脂固化温度、热性能、阻燃性能、力学性能及介电性能的影响。结果表明,添加Fe(PDC)3可以降低环氧树脂的固化温度、热释放速率及总热释放量,提高残炭量、氧指数,这是由于铁络合物可以有效促进材料在高温下形成稳定性良好的致密炭层,起到隔氧隔热作用,从而在燃烧过程中阻止材料进一步燃烧。 展开更多
关键词 低聚倍半硅氧烷衍生物 铁络合物 环氧树脂 阻燃
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Response of Different Varieties of Red Cartridge Kiwifruit to Temperature and Precipitation in Growth Stages
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作者 Lijuan LIU Liangyu PENG +3 位作者 Zaixiang CHI Bo LI jinmei chen Tianfu HUANG 《Meteorological and Environmental Research》 CAS 2022年第2期75-77,共3页
The responses of Hongyang,Donghong and Jinhong varieties to temperature and precipitation were analyzed by observing the growth stages of different kiwifruit varieties in Longhe red cartridge kiwifruit base of Liuzhi ... The responses of Hongyang,Donghong and Jinhong varieties to temperature and precipitation were analyzed by observing the growth stages of different kiwifruit varieties in Longhe red cartridge kiwifruit base of Liuzhi Special Zone of Guizhou Province in 2021 and combining with the meteorological data of temperature and precipitation in the base in the same period.The results showed that Hongyang,Donghong and Jinhong all sprouted on February 1,and had the same response to temperature and precipitation.From germination to leaf spreading stage,Hongyang and Donghong had the same response to precipitation,while Donghong and Jinhong had the same response to temperature,but Jinhong needed 32.5 mm precipitation to meet its growth and development.From leaf spreading stage to budding stage,Hongyang and Donghong had similar responses to temperature and precipitation,while Jinhong needed average daily temperature of 16.5℃and precipitation of 2.1 mm.The responses of the three varieties from budding to flowering to temperature and precipitation were consistent.From flowering to fruiting,Hongyang needed 19.9℃temperature and the least precipitation,while Jinhong needed the lowest temperature and the maximum precipitation.Donghong's response to temperature and precipitation was between Hongyang and Jinhong.During the period from fruit setting to fruit ripening and picking,Hongyang needed the least temperature and precipitation,while Donghong and Jinhong had the same response to temperature and precipitation.In the key period of fruit expansion of the three kiwifruit varieties in 2021,temperature and precipitation were the most suitable for fruit expansion.In short,red cartridge kiwifruit has a good response to temperature and precipitation in different growth stages,and it requires 201 d for Hongyang variety from germination to maturity and picking,211 d for Donghong variety and 218 d for Jinhong variety. 展开更多
关键词 TEMPERATURE PRECIPITATION Growth stage RESPONSE Red cartridge kiwifruit
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