This article explored the influence of molding density of TiO<sub>2</sub> varistor-ceramic on densification of ceramic body and grain growth. By the main phase and second phase analysis of TiO<sub>2&...This article explored the influence of molding density of TiO<sub>2</sub> varistor-ceramic on densification of ceramic body and grain growth. By the main phase and second phase analysis of TiO<sub>2</sub> varistor-ceramic through XRD and EDAX, the effects of the second phrase on TiO<sub>2</sub> varistor-ceramic were studied. Grain size and its distribution were observed through scanning electron microscope and the density of porcelain body was measured. The effects of grain size, distribution and density of ceramic body on electrical property of TiO<sub>2</sub> varistor-ceramic were the focus issue for analysis. The increased molding density would improve the densifying of magnetic body to some extent and promote grain growth.展开更多
In this paper, the changes of surface morphology, microstructure, hardness and corrosion resistance of industrial pure zirconium before and after surface modification by high current pulsed electron beam were discusse...In this paper, the changes of surface morphology, microstructure, hardness and corrosion resistance of industrial pure zirconium before and after surface modification by high current pulsed electron beam were discussed. The microstructure evolution and surface morphologies of the samples were characterized by using X-ray diffraction (XRD), optical microscopy (OM), scanning electron microscopy (SEM). The experimental results show that sample by high current pulsed electron beam treatment surface melting, martensitic phase transformation occurred, and volcanic crater morphology and fine microstructure in the remelted layer surface;with the increase of number of pulses, after processing the microhardness of the samples also with the increase, 15-pulsed sample microhardness than the original sample increased by 30.9%. Corrosion resistance of samples was studied with the impedance diagram and polarization curve. The electrochemical results show that corrosion resistance of samples by high current pulsed electron beam treatment presents different degrees of change, the 5-pulsed sample in 1 mol HNO<sub>3</sub> solution corrosion of the best, and 15-pulsed sample corrosion resistance is even lower than the original sample. Grain refinement, martensite transformation, dislocation and deformation twins are the main reasons for improving the micro hardness and corrosion resistance of the samples.展开更多
In this work,surface modification of a Mg-4Sm-2Al-0.5Mn alloy with high current pulse electron beam(HCPEB)under different number of pulses were investigated.The evolution in microstructure,composition and phase compon...In this work,surface modification of a Mg-4Sm-2Al-0.5Mn alloy with high current pulse electron beam(HCPEB)under different number of pulses were investigated.The evolution in microstructure,composition and phase components and properties in the surface layer before and after HCPEB treatment were characterized.It was found that the Al 11 Sm 3 and Al 2 Sm phases in the surface layer were gradually dissolved during HCPEB treatment,leading to the formation of a chemical homogeneous melted layers.Besides,deformation bands were formed in the treated layer due to the thermal stress generated during treatment.After 15 pulses treatment,the surface hardness increases to the maximum value of about 62.2 HV,about 61.2%higher than that of the untreated state.Electrochemical results show that the 15 pulses treated sample presents the best corrosion resistance in the 3.5wt%NaCl water solution by showing the highest corrosion potential(E_(corr))of-1.339V SEC and the lowest corrosion current density(I_(corr))of 1.48×10^(-6)A·cm^(-2).The results prove that the surface properties of the Mg-4Sm-2Al-0.5Mn alloy can be significantly improved by the HCPEB treatments under proper conditions.展开更多
In this paper, Al/Ni/TiC powders were mixed on the surface of A380 aluminum alloy, by selecting appropriate laser parameters;the cladding layer with good adhesion to the substrate was obtained. The microstructure and ...In this paper, Al/Ni/TiC powders were mixed on the surface of A380 aluminum alloy, by selecting appropriate laser parameters;the cladding layer with good adhesion to the substrate was obtained. The microstructure and properties of the cladding layer under different laser parameters were analyzed. The results show that: the phase composition of the cladding layer is mainly composed of TiC, Al, Ni, C and Ti phases. The hardness of the cladding region is up to 173.3 HV, which is about 2.9 times the matrix (–59.1 HV). The corrosion voltage (–1.8 V) of the cladding layer shifted significantly from the corrosion potential (–1.18 V), the corrosion current density increased, the resistance value decreased and the diameter of the capacitor arc decreased;all these phenomena indicate that the corrosion resistance of the cladding layer is decreased.展开更多
It is proved that for given integer k≥2, almost all k-hypertournaments are strong and in almost all k-hypertournaments, every pair of vertices lies on a 3-cycle.
Laser surface melting has been applied on a commercially pure Mg. The microstructure and texture modifications encountered in the surface layers were carefully investigated by using electron backscattered diffraction ...Laser surface melting has been applied on a commercially pure Mg. The microstructure and texture modifications encountered in the surface layers were carefully investigated by using electron backscattered diffraction (EBSD) technique. Due to the melting followed by rapid solidification and cooling, a layer having graded microstructures and texture formed. At the bottom of the melted layer, the solidified Mg grains have an elongated shape with a 〈0001 〉 basal fibre texture nearly parallel to sample normal direction, while equiaxed grains were observed in the top melted layer having a much weaker basal fibre texture. Solidification twinning and deformation twinning were found in the vicinity of the melt/substrate interface where the Mg grains grow larger due to the heating. In addition, no epitaxial type grain growth was observed at the melt/substrate interface.展开更多
文摘This article explored the influence of molding density of TiO<sub>2</sub> varistor-ceramic on densification of ceramic body and grain growth. By the main phase and second phase analysis of TiO<sub>2</sub> varistor-ceramic through XRD and EDAX, the effects of the second phrase on TiO<sub>2</sub> varistor-ceramic were studied. Grain size and its distribution were observed through scanning electron microscope and the density of porcelain body was measured. The effects of grain size, distribution and density of ceramic body on electrical property of TiO<sub>2</sub> varistor-ceramic were the focus issue for analysis. The increased molding density would improve the densifying of magnetic body to some extent and promote grain growth.
文摘In this paper, the changes of surface morphology, microstructure, hardness and corrosion resistance of industrial pure zirconium before and after surface modification by high current pulsed electron beam were discussed. The microstructure evolution and surface morphologies of the samples were characterized by using X-ray diffraction (XRD), optical microscopy (OM), scanning electron microscopy (SEM). The experimental results show that sample by high current pulsed electron beam treatment surface melting, martensitic phase transformation occurred, and volcanic crater morphology and fine microstructure in the remelted layer surface;with the increase of number of pulses, after processing the microhardness of the samples also with the increase, 15-pulsed sample microhardness than the original sample increased by 30.9%. Corrosion resistance of samples was studied with the impedance diagram and polarization curve. The electrochemical results show that corrosion resistance of samples by high current pulsed electron beam treatment presents different degrees of change, the 5-pulsed sample in 1 mol HNO<sub>3</sub> solution corrosion of the best, and 15-pulsed sample corrosion resistance is even lower than the original sample. Grain refinement, martensite transformation, dislocation and deformation twins are the main reasons for improving the micro hardness and corrosion resistance of the samples.
基金This work was supported by the National Natural Science Foundations of China(No.51271121,51471109).
文摘In this work,surface modification of a Mg-4Sm-2Al-0.5Mn alloy with high current pulse electron beam(HCPEB)under different number of pulses were investigated.The evolution in microstructure,composition and phase components and properties in the surface layer before and after HCPEB treatment were characterized.It was found that the Al 11 Sm 3 and Al 2 Sm phases in the surface layer were gradually dissolved during HCPEB treatment,leading to the formation of a chemical homogeneous melted layers.Besides,deformation bands were formed in the treated layer due to the thermal stress generated during treatment.After 15 pulses treatment,the surface hardness increases to the maximum value of about 62.2 HV,about 61.2%higher than that of the untreated state.Electrochemical results show that the 15 pulses treated sample presents the best corrosion resistance in the 3.5wt%NaCl water solution by showing the highest corrosion potential(E_(corr))of-1.339V SEC and the lowest corrosion current density(I_(corr))of 1.48×10^(-6)A·cm^(-2).The results prove that the surface properties of the Mg-4Sm-2Al-0.5Mn alloy can be significantly improved by the HCPEB treatments under proper conditions.
文摘In this paper, Al/Ni/TiC powders were mixed on the surface of A380 aluminum alloy, by selecting appropriate laser parameters;the cladding layer with good adhesion to the substrate was obtained. The microstructure and properties of the cladding layer under different laser parameters were analyzed. The results show that: the phase composition of the cladding layer is mainly composed of TiC, Al, Ni, C and Ti phases. The hardness of the cladding region is up to 173.3 HV, which is about 2.9 times the matrix (–59.1 HV). The corrosion voltage (–1.8 V) of the cladding layer shifted significantly from the corrosion potential (–1.18 V), the corrosion current density increased, the resistance value decreased and the diameter of the capacitor arc decreased;all these phenomena indicate that the corrosion resistance of the cladding layer is decreased.
文摘It is proved that for given integer k≥2, almost all k-hypertournaments are strong and in almost all k-hypertournaments, every pair of vertices lies on a 3-cycle.
基金support of the Top Discipline Plan for Mechanical Engineering of Shanghai Municipal Education Commission (YLJX12-2)partially supported by the Special Foundation of the Shanghai Science and Technology Committee for Nano-Materials Research (No. 1052nm05000)the National Natural Science Foundation of China (Nos. 51101096, 51271121 and 51002093)
文摘Laser surface melting has been applied on a commercially pure Mg. The microstructure and texture modifications encountered in the surface layers were carefully investigated by using electron backscattered diffraction (EBSD) technique. Due to the melting followed by rapid solidification and cooling, a layer having graded microstructures and texture formed. At the bottom of the melted layer, the solidified Mg grains have an elongated shape with a 〈0001 〉 basal fibre texture nearly parallel to sample normal direction, while equiaxed grains were observed in the top melted layer having a much weaker basal fibre texture. Solidification twinning and deformation twinning were found in the vicinity of the melt/substrate interface where the Mg grains grow larger due to the heating. In addition, no epitaxial type grain growth was observed at the melt/substrate interface.