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Lantana camara berry for the synthesis of silver nanoparticles 被引量:1
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作者 Brajesh Kumar kumari smita +1 位作者 Luis Cumbal Alexis Debut 《Asian Pacific Journal of Tropical Biomedicine》 SCIE CAS 2015年第3期192-195,共4页
Objective:To synthesize the silver nunoparticles(AgNPs) by reduction of silver ions into nano silver,using ripened berry extract of Lantana camara and evaluate its antioxidant activity against 1.1-diphenyl-2- picrylhy... Objective:To synthesize the silver nunoparticles(AgNPs) by reduction of silver ions into nano silver,using ripened berry extract of Lantana camara and evaluate its antioxidant activity against 1.1-diphenyl-2- picrylhydrazyl.Methods:The prepared AgNPs were characterized by visual,UV-visible spectrophotometer.dynamic light scattering and transmission electron microscopy with selected area electron diffraction.Results:Transmission electron microscopy and dynamic light scattering analysis confirmed the AgNPs are spherical and 75.2 nm average sized.Selected area electron diffraction analysis supports that the obtained nanoparticles were in crystalline form.In addition,the antioxidant efficacy of prepared AgNPs was found to be higher than berry extract against 1.1-diphenyl-2-picrylhydrazyl.Conclusions:From the results obtained it is suggested that surface modified AgNPs at lower concentration,showed higher antioxidant activity than berry extract against 1,1-diphenyl-2-picrylhydrazyl and could be used effectively in future ethno pharmacological concerns. 展开更多
关键词 Green synthesis LANTANA camara SILVER nanoparticles Transmission electron MICROSCOPY DPPH·
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Extracellular green synthesis of silver nanoparticles using Amazonian fruit Araza(Eugenia stipitata McVaugh)
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作者 Brajesh KUMAR kumari smita +1 位作者 Alexis DEBUT Luis CUMBAL 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2016年第9期2363-2371,共9页
An eco-friendly method for the extracellular synthesis of silver nanoparticles(AgNPs) using aqueous Araza fruit extract and their antioxidant activity was investigated. It was observed that UV–Vis absorption peak i... An eco-friendly method for the extracellular synthesis of silver nanoparticles(AgNPs) using aqueous Araza fruit extract and their antioxidant activity was investigated. It was observed that UV–Vis absorption peak is dependent on various parameters such as pH, temperature, and change of time. The initial appearance of the yellow color with intense surface plasmon bands at 430-450 nm, then transmission electron microscopy, scanning electron microscopy and X-ray diffraction analysis revealed the formation of 15-45 nm sized, spherical and crystalline Ag NPs. Fourier transform infrared spectroscopy depicted that malic acid, citric acid, and carotenoids of Araza fruit involved in the synthesis of Ag NPs. In addition, the surface modified AgNPs(77.42%, 1mL) showed nearly double antioxidant efficiency than Araza fruit extract(35.30%, 1 mL) against 1, 1-diphenyl-2-picrylhydrazyl. The present study highlights the possibility of using the Araza fruit to synthesize AgNPs, which could be used effectively in the present and future antioxidant agent. 展开更多
关键词 extracellular synthesis silver nanoparticles ANTIOXIDANT ECO-FRIENDLINESS
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Capuli cherry-mediated green synthesis of silver nanoparticles under white solar and blue LED light 被引量:2
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作者 Brajesh Kumar Yolancla Angulo +2 位作者 kumari smita Luis Cumbal Alexis Debut 《Particuology》 SCIE EI CAS CSCD 2016年第1期123-128,共6页
In this article, the Capuli (Prunus serotina Ehrh. var. Capuli) cherry extract was used for the synthesis of silver nanoparticles (AgNPs) in the presence of white/visible solar and blue light-emitting diode (LED... In this article, the Capuli (Prunus serotina Ehrh. var. Capuli) cherry extract was used for the synthesis of silver nanoparticles (AgNPs) in the presence of white/visible solar and blue light-emitting diode (LED) light. For the characterization of the extract and the AgNPs, Fourier transform infrared spectroscopy and ultraviolet-visible spectroscopy were employed, along with hydrodynamic particle size analysis, trans- mission electron microscopy and X-ray diffraction. The Ag nanospheres obtained using white light were 40-100 nm in diameter and exhibited an absorption peak at λmax= 445 nm, whereas those obtained using blue LED light were 20-80 nm in diameter with an absorption peak at λmax= 425 nm. Thermal analysis revealed that the content of biomolecules surrounding the AgNPs was about 55-65%, and it was also found that blue LED light AgNPs (56.28%, 0.05 mM) had a higher antioxidant efficacy than the white solar light AgNPs (33.42%, 0.05 mM) against l,l-diphenyl-2-picrylhydrazyl. The results indicate that obtaining AgNPs using a blue LED light may prove to be a simple, cost-effective and easily reproducible method for creating future nanopharmaceuticals. 展开更多
关键词 Silver nanoparticles Capuli LED light Fourier transform infrared spectroscopy Transmission electron microscopy Antioxidant
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