调整双季铵盐表面活性剂与单季铵盐表面活性剂的使用量,通过协同晶化的方式合成了高结晶度、高介孔容的薄层ZSM-5沸石。利用XRD、XRF、SEM、TEM、NH3-TPD、低温氮气物理吸脱附以及27Al MAS NMR对沸石样品进行表征,并评价其甲醇制丙烯反...调整双季铵盐表面活性剂与单季铵盐表面活性剂的使用量,通过协同晶化的方式合成了高结晶度、高介孔容的薄层ZSM-5沸石。利用XRD、XRF、SEM、TEM、NH3-TPD、低温氮气物理吸脱附以及27Al MAS NMR对沸石样品进行表征,并评价其甲醇制丙烯反应(MTP)催化性能。结果表明,薄层沸石的b轴厚度随着双季铵盐表面活性剂使用量的减少而增加,适量的单季铵盐表面活性剂的加入可以起到协同晶化的作用,能够有效稳定胶束,从而调控沸石的形貌。优化2种季铵盐表面活性剂的使用量所得薄层ZSM-5沸石的比表面积和介孔孔容都有所增加,在甲醇制丙烯反应中的活性稳定性也得到较大改善。此外,协同晶化的方式减少了双季铵盐表面活性剂的使用,有利于降低薄层ZSM-5沸石的合成成本。展开更多
BOOM处理器采用的Store指令回查策略虽然解决了访存指令乱序执行引发的数据冲突问题,但是该策略会导致流水线的大量冲刷,降低了处理器的性能。对此,提出了一种访存指令的相关性预测方法。该方法取消了Load指令访存前的查询操作,增加了L...BOOM处理器采用的Store指令回查策略虽然解决了访存指令乱序执行引发的数据冲突问题,但是该策略会导致流水线的大量冲刷,降低了处理器的性能。对此,提出了一种访存指令的相关性预测方法。该方法取消了Load指令访存前的查询操作,增加了Load指令相关性预测表,只有预测为无相关性的Load指令才可以乱序执行。这种方法在保证程序逻辑正确的前提下避免了大量冲刷流水线。测试程序采用SPEC CPU 2006下的7个子程序,实验结果表明,改进后的处理器执行程序的性能平均提升了3.5%。展开更多
The larch wood was treated by microwave irradiation under different radiant intensity and treating duration. The microwave-treated wood specimens together with the un-treated for comparison were impregnated by water i...The larch wood was treated by microwave irradiation under different radiant intensity and treating duration. The microwave-treated wood specimens together with the un-treated for comparison were impregnated by water in pressure vessel and then tested for permeability, mechanical properties and microstructure change by SEM to study the modification performance of microwave treatment on larch wood. The results showed that under suitable conditions of microwave treatment the permeability of larch wood was improved without noticeable decreasing of the modulus of rupture （MOR） and the modulus of elasticity （MOE）. The radial parenchyma and some pit membrane were ruptured, and tiny cracks were formed in the cell walls. The formation of tiny cracks in the cell walls serves as man-made channels of gas and liquid and this contribute to improve the permeability of the wood.展开更多
Two zero-phonon lines with wide linewidth on R_(1)^(- ) and unknown colour centres have been observed in the magnesium-doped lithium fluoride crystals coloured by electron beam bombardment at 200 K in the measured tem...Two zero-phonon lines with wide linewidth on R_(1)^(- ) and unknown colour centres have been observed in the magnesium-doped lithium fluoride crystals coloured by electron beam bombardment at 200 K in the measured temperature range of 10-77 K. The R_(1)^(- )zero-phonon line can be nearly completely bleached using the normal spectrophotometer light at 10K. An obvious spectral burning hole in the absorption profile of the R_(1)^(- ) zero-phonon line of colour centres in the coloured lithium fluoride crystals has been obtained by using the spectrophotometer light adjusted to narrower bandwidth at 10K. The optical bleaching of the zero-phonon line can be partially recovered by annealing the crystals to room temperature for a short time period or irradiating the crystals with ultraviolet light above 40 K, and nearly complete restoration can be obtained after the ultraviolet light irradiation and storage in the dark for a long time at room temperature.展开更多
文摘调整双季铵盐表面活性剂与单季铵盐表面活性剂的使用量,通过协同晶化的方式合成了高结晶度、高介孔容的薄层ZSM-5沸石。利用XRD、XRF、SEM、TEM、NH3-TPD、低温氮气物理吸脱附以及27Al MAS NMR对沸石样品进行表征,并评价其甲醇制丙烯反应(MTP)催化性能。结果表明,薄层沸石的b轴厚度随着双季铵盐表面活性剂使用量的减少而增加,适量的单季铵盐表面活性剂的加入可以起到协同晶化的作用,能够有效稳定胶束,从而调控沸石的形貌。优化2种季铵盐表面活性剂的使用量所得薄层ZSM-5沸石的比表面积和介孔孔容都有所增加,在甲醇制丙烯反应中的活性稳定性也得到较大改善。此外,协同晶化的方式减少了双季铵盐表面活性剂的使用,有利于降低薄层ZSM-5沸石的合成成本。
文摘BOOM处理器采用的Store指令回查策略虽然解决了访存指令乱序执行引发的数据冲突问题,但是该策略会导致流水线的大量冲刷,降低了处理器的性能。对此,提出了一种访存指令的相关性预测方法。该方法取消了Load指令访存前的查询操作,增加了Load指令相关性预测表,只有预测为无相关性的Load指令才可以乱序执行。这种方法在保证程序逻辑正确的前提下避免了大量冲刷流水线。测试程序采用SPEC CPU 2006下的7个子程序,实验结果表明,改进后的处理器执行程序的性能平均提升了3.5%。
基金This paper was supported by Science Fund for Distin-guished Young Scholars, Heilongjiang Province (No. JC04-01)
文摘The larch wood was treated by microwave irradiation under different radiant intensity and treating duration. The microwave-treated wood specimens together with the un-treated for comparison were impregnated by water in pressure vessel and then tested for permeability, mechanical properties and microstructure change by SEM to study the modification performance of microwave treatment on larch wood. The results showed that under suitable conditions of microwave treatment the permeability of larch wood was improved without noticeable decreasing of the modulus of rupture （MOR） and the modulus of elasticity （MOE）. The radial parenchyma and some pit membrane were ruptured, and tiny cracks were formed in the cell walls. The formation of tiny cracks in the cell walls serves as man-made channels of gas and liquid and this contribute to improve the permeability of the wood.
基金Supported partially by the National Natural Science Foundation of China under Grant No.69178028。
文摘Two zero-phonon lines with wide linewidth on R_(1)^(- ) and unknown colour centres have been observed in the magnesium-doped lithium fluoride crystals coloured by electron beam bombardment at 200 K in the measured temperature range of 10-77 K. The R_(1)^(- )zero-phonon line can be nearly completely bleached using the normal spectrophotometer light at 10K. An obvious spectral burning hole in the absorption profile of the R_(1)^(- ) zero-phonon line of colour centres in the coloured lithium fluoride crystals has been obtained by using the spectrophotometer light adjusted to narrower bandwidth at 10K. The optical bleaching of the zero-phonon line can be partially recovered by annealing the crystals to room temperature for a short time period or irradiating the crystals with ultraviolet light above 40 K, and nearly complete restoration can be obtained after the ultraviolet light irradiation and storage in the dark for a long time at room temperature.
