The title compound, N′-(4-methoxybenzylidene)-2-(1%H%-1,2,4-triazol-1-yl)acetohydrazide, was synthesized and its structure was confirmed by means of IR, MS, 1H NMR and elemental analysis. The single crystal structure...The title compound, N′-(4-methoxybenzylidene)-2-(1%H%-1,2,4-triazol-1-yl)acetohydrazide, was synthesized and its structure was confirmed by means of IR, MS, 1H NMR and elemental analysis. The single crystal structure of the title compound was determined by X-ray diffraction. The preliminary biological test shows that the synthesized compound has a low antifungal activity.展开更多
A field experiment was conducted to investigate the variations in denitrification losses and N2O emissions from 4 different types of nitrogen fertilizers (urea, ammonium nitrate, ammonium bicarbonate, and calcium nitr...A field experiment was conducted to investigate the variations in denitrification losses and N2O emissions from 4 different types of nitrogen fertilizers (urea, ammonium nitrate, ammonium bicarbonate, and calcium nitrate) applied to the maize- fluvo-aquic soil system in the North China Plain by the method of intact soil core incubation and acetylene inhibition, and the responses of nitrogen fertilizers to maize grain yields. Results show that the denitrification loss from different nitrogen fertilizers ranged from 0.38-1.20 kg N ha-1, with no significant differences among different fertilizer treatments, and the N2O emission from 0.05-0.95 kg N ha-1, with a significant difference (P<0.05) among the treatments. The highest emission was from the treatment of ammonium nitrate, while the lowest from calcium nitrate. The nitrogen fertilizers increased the maize grain yield by 9.7-19.8% compared to control. But there were no significant differences in yield increase among the 4 types of nitrogen fertilizers. In comparison, urea had the best effect, whereas calcium nitrate had the least effect on increasing maize yield. The maize yield was 5.7% higher when urea was separately applied at 2 times than when it was applied at a time. In this case, however, the denitrification loss and the N2O emission were also increased by 4.05 and 1.84 kg N ha-1, respectively.展开更多
The title compound, 2-(methoxybenzoyl)-N-phenyl-2-(1,2,4-triazol-1-yl)thioacetamide was synthesized by several reactions from 4-methoxyacetophenone, triazole and phenyl isothiocyanate. The structure was identified by ...The title compound, 2-(methoxybenzoyl)-N-phenyl-2-(1,2,4-triazol-1-yl)thioacetamide was synthesized by several reactions from 4-methoxyacetophenone, triazole and phenyl isothiocyanate. The structure was identified by elemental analysis, ~ 1H NMR, MS and IR. The single crystal structure of 2-(methoxybenzoyl)-N-phenyl-2-(1,2,4-triazol-1-yl)thioacetamide was determined with X-ray diffraction. The preliminary bioassays show that the title compound exhibits weak antifungal activities and plant-growth regulatory activity.展开更多
文摘The title compound, N′-(4-methoxybenzylidene)-2-(1%H%-1,2,4-triazol-1-yl)acetohydrazide, was synthesized and its structure was confirmed by means of IR, MS, 1H NMR and elemental analysis. The single crystal structure of the title compound was determined by X-ray diffraction. The preliminary biological test shows that the synthesized compound has a low antifungal activity.
基金The work was supported by the National Natural Sci-ence Foundation of China(49901010).
文摘A field experiment was conducted to investigate the variations in denitrification losses and N2O emissions from 4 different types of nitrogen fertilizers (urea, ammonium nitrate, ammonium bicarbonate, and calcium nitrate) applied to the maize- fluvo-aquic soil system in the North China Plain by the method of intact soil core incubation and acetylene inhibition, and the responses of nitrogen fertilizers to maize grain yields. Results show that the denitrification loss from different nitrogen fertilizers ranged from 0.38-1.20 kg N ha-1, with no significant differences among different fertilizer treatments, and the N2O emission from 0.05-0.95 kg N ha-1, with a significant difference (P<0.05) among the treatments. The highest emission was from the treatment of ammonium nitrate, while the lowest from calcium nitrate. The nitrogen fertilizers increased the maize grain yield by 9.7-19.8% compared to control. But there were no significant differences in yield increase among the 4 types of nitrogen fertilizers. In comparison, urea had the best effect, whereas calcium nitrate had the least effect on increasing maize yield. The maize yield was 5.7% higher when urea was separately applied at 2 times than when it was applied at a time. In this case, however, the denitrification loss and the N2O emission were also increased by 4.05 and 1.84 kg N ha-1, respectively.
文摘The title compound, 2-(methoxybenzoyl)-N-phenyl-2-(1,2,4-triazol-1-yl)thioacetamide was synthesized by several reactions from 4-methoxyacetophenone, triazole and phenyl isothiocyanate. The structure was identified by elemental analysis, ~ 1H NMR, MS and IR. The single crystal structure of 2-(methoxybenzoyl)-N-phenyl-2-(1,2,4-triazol-1-yl)thioacetamide was determined with X-ray diffraction. The preliminary bioassays show that the title compound exhibits weak antifungal activities and plant-growth regulatory activity.