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Structural and Photoluminescence Characterization of GaN Film Grown on Si(111)Substrate
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作者 YE Zhi-zhen ZHANG Hao-xiang +1 位作者 lu huan-ming ZHAO Bing-hui 《Chinese Physics Letters》 SCIE CAS CSCD 1999年第4期293-294,共2页
GaN epilayer grown on Si(111)substrate by a novel vacuum reaction method rather than metal organic chemical vapor deposition or molecule beam epitaxy is reported.Scanning electron micrograph shows that surface of GaN ... GaN epilayer grown on Si(111)substrate by a novel vacuum reaction method rather than metal organic chemical vapor deposition or molecule beam epitaxy is reported.Scanning electron micrograph shows that surface of GaN film is flat and crack-free.A pronounced GaN(0002)peak appears in the x-ray diffraction pattern.The full width at half-maximum(FWHM)of the double-crystal x-ray rocking curve for(0002)diffraction from the GaN epilayer is 30arcmin.The photoluminescence spectrum shows that the GaN epilayer emits light at the wavelength of 365nm with an FWHM of 8nm(74.6meV). 展开更多
关键词 SI(111) GAN VACUUM
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飞行时间质谱仪固体样品自动进样系统研制 被引量:1
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作者 刘蔓 韩莹莹 +2 位作者 朱丽辉 卢焕明 李勇 《分析测试学报》 CAS CSCD 北大核心 2019年第11期1310-1314,共5页
以常规型飞行时间质谱仪为基础,通过配置移动平台、样品杆、工业相机、LED灯源、工业显示屏等部件,研制了一套飞行时间质谱仪用固体样品自动进样系统,实现了固体有机样品的直接进样分析。该装置具有一定的普适性,可为相关实验室设备升... 以常规型飞行时间质谱仪为基础,通过配置移动平台、样品杆、工业相机、LED灯源、工业显示屏等部件,研制了一套飞行时间质谱仪用固体样品自动进样系统,实现了固体有机样品的直接进样分析。该装置具有一定的普适性,可为相关实验室设备升级改造提供借鉴和参考。该装置可进行难溶未知有机化合物的结构剖析,实现目标物的快速筛查,且操作人员可实时观测锥孔处样品状态并可软件操控进样位置,实现人机分离的自动化测试。 展开更多
关键词 飞行时间质谱仪 固体样品 自动进样系统 仪器研制
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高温与电子束辐照共同作用下SiO_(x)材料的结构演化研究 被引量:2
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作者 梁芮 陈国新 +5 位作者 黄钦 王楠 唐发俊 张志佳 卢焕明 康建立 《电子显微学报》 CAS CSCD 北大核心 2021年第4期367-372,共6页
本文利用透射电子显微镜原位加热技术研究了高温下SiO_(x)材料的结构演化行为,并通过EELS谱分析了SiO_(x)材料结构的化学组成变化。研究结果表明:在高温作用下,电子束辐照对SiO_(x)材料的相分离过程起到了促进作用;高密度电子束辐照是Si... 本文利用透射电子显微镜原位加热技术研究了高温下SiO_(x)材料的结构演化行为,并通过EELS谱分析了SiO_(x)材料结构的化学组成变化。研究结果表明:在高温作用下,电子束辐照对SiO_(x)材料的相分离过程起到了促进作用;高密度电子束辐照是SiO_(x)材料中产生孔状结构的主要原因;SiO_(x)材料在高温和电子束辐照作用下,会快速形成纳米硅镶嵌在多孔二氧化硅薄膜中的特殊结构。 展开更多
关键词 SiO_(x)材料 电子束辐照 原位TEM加热
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X射线光电子能谱测定固体粉末样品的制备方法比较 被引量:3
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作者 苗利静 江柯敏 +3 位作者 朱丽辉 卢焕明 李勇 吴越 《分析测试技术与仪器》 CAS 2020年第1期56-60,共5页
样品制备方法对X射线光电子能谱测试结果具有较大影响,以导电样品锂电材料和不导电样品奶粉为测试对象,探讨了不同制样方法对两者测试效果的影响.试验结果表明,导电样品锂电材料使用导电胶铜片制样效果较好,而不导电样品奶粉使用导电胶... 样品制备方法对X射线光电子能谱测试结果具有较大影响,以导电样品锂电材料和不导电样品奶粉为测试对象,探讨了不同制样方法对两者测试效果的影响.试验结果表明,导电样品锂电材料使用导电胶铜片制样效果较好,而不导电样品奶粉使用导电胶压片或3M胶带压片效果较好. 展开更多
关键词 X射线光电子能谱 锂电材料 奶粉 压片 铜片制样
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Growth and Characterization of High Quality Si_(1-x-y)Ge_(x)C_(y) Alloy Grown by Ultra-High Vacuum Chemical Vapor Deposition
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作者 QI Zhen HUANG Jing-yun +4 位作者 YE Zhi-zhen lu huan-ming CHEN Wei-hua ZHAO Bing-hui WANG Lei 《Chinese Physics Letters》 SCIE CAS CSCD 1999年第10期750-752,共3页
High quality Si_(1-x-y)Ge_(x)C_(y) alloy with 2.2%C is grown at a relatively high temperature(760℃)on Si(100)using ultra-high vacuum/chemical vapor deposition(UHV/CVD)system.The samples are investigated with high res... High quality Si_(1-x-y)Ge_(x)C_(y) alloy with 2.2%C is grown at a relatively high temperature(760℃)on Si(100)using ultra-high vacuum/chemical vapor deposition(UHV/CVD)system.The samples are investigated with high resolution cross-sectioned transmission electron microscope and x-ray diffraction.Compared with Si_(1-x)Ge_(x) alloys,Si_(1-x-y)Ge_(x)C_(y) alloys with small amounts of Chave much less strain and larger critical layer thickness.The quality of interface is edso improved.Relatively flat growing profiles of the film are confirmed by secondary ion mass spectroscopy.Fourier transform infrared spectroscopy is also used to testify that the carbon atoms are on the substitutional sites.It is proved that the UHV/CVD system is an efficient method of growing Si_(1-x-y)Ge_(x)C_(y) alloys. 展开更多
关键词 spectroscopy. diffraction. ALLOYS
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SiGe Epitaxy with Graded Buffer by Ultrahigh Vacuum Chemical Vapor Deposition
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作者 HUANG Jing-yun YE Zhi-zhen +5 位作者 lu huan-ming JIANG Xiao-bo WU Hui-zhen ZHAO Bing-hui WANG Lei QUE Duan-lin 《Chinese Physics Letters》 SCIE CAS CSCD 1998年第9期692-694,共3页
A SiGe/Si epilayer with a linear-step-graded buffer was grown by ultrahigh vacuum chemical vapor deposition technique at a relatively high growth temperature(780℃)and a relatively high growth rate.Almost linear Ge co... A SiGe/Si epilayer with a linear-step-graded buffer was grown by ultrahigh vacuum chemical vapor deposition technique at a relatively high growth temperature(780℃)and a relatively high growth rate.Almost linear Ge content variation was realized in the buffer layer due to the Ge segregation to the growing surface during epitaxial growth.Double crystal x-ray diffraction and Raman spectroscopy show that the upper layer is fully relaxed.However,the measured results show that the density of dislocation in the composition graded structure is much lower than that in single-step epilayer structures. 展开更多
关键词 SIGE/SI EPITAXY SIGE
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