Iron powders were mixed with graphite powders by 1-15 wt pct to produce block samples using powder metallurgy technique. The powders were blended in a three dimensional blender for 20 min and compacted in a die under ...Iron powders were mixed with graphite powders by 1-15 wt pct to produce block samples using powder metallurgy technique. The powders were blended in a three dimensional blender for 20 min and compacted in a die under 500 MPa by using a one directional press. Sinterability and mechanical properties of the samples with different carbon content were investigated. Sintering process was carried out on a belt furnace with flame curtain in dissociated ammonia atmosphere. Block samples produced were suitable for ASTM B-312 transverse rupture strength test apparatus and were tested with 0.050 kN/s velocity in a press under 100 g load. It was found that graphite amount up to 2 wt pct increased the contact area of particles and acted as a lubricant to affect the sintering behaviour positively. The results indicated that the samples containing up to 5 wt pct showed good sintering behaviour and also good hardness due to an increase in pearlite amount. However, the samples containing higher amount of graphite （more than 5 wt pct） affected the sintering behaviour negatively due to the settlement of free graphite around the Fe powders, which resulted in a decrease in the hardness and transverse rupture strength.展开更多
Friction-wear properties of the ZrSiO4 reinforced samples were measured and compared with those of plain bronze based ones. For this purpose, density, hardness, friction coefficient wear behaviour of the samples were ...Friction-wear properties of the ZrSiO4 reinforced samples were measured and compared with those of plain bronze based ones. For this purpose, density, hardness, friction coefficient wear behaviour of the samples were tested. Microstructures of samples before and after sintering and worn surfaces were also investigated by scanning electron microscopy （SEM）, and the wear types were determined. The optimum friction-wear behaviour was obtained in the sample compacted at 500 MPa and sintered at 820℃. Density of the final samples decreased with increasing the amount of reinforcing elements （ZrSiO4） before pre-sintering. However after sintering, there is no change in density of the samples including reinforcing elements （ZrSiO4）. With increasing friction surface temperature, a reduction in the friction coefficient of the samples was observed. However, the highest reductions in the friction coefficients were observed in the as-received samples containing 0. 5% reinforced ZrSiO4. The SEM images of the sample indicated that while bronze-based break lining material without ZrSiO4 showed abrasive wear behaviour, increasing the amount of ZrSiO4 resulted a change in abrasive to adhesive wear mechanism. All samples exhibited friction-wear values, which were within the values shown in SAE-J661 standard. With increasing the amount of reinforcing ZrSiO4, wear resistance of the samples was increased. However samples reinforced with 5% and 6% ZrSiO4 showed the best results.展开更多
This study intends to determine the pressability and sinterability of AZ91 powder production by gas atomisation method and that of the produced powder for partial production.Therefore,first,a gas atomisation unit has ...This study intends to determine the pressability and sinterability of AZ91 powder production by gas atomisation method and that of the produced powder for partial production.Therefore,first,a gas atomisation unit has been designed and manufactured in the laboratories of the Karabiik University,Department of Manufacturing Engineering.Atomised powder production has been achieved at a temperature of 795℃,with nozzle diameters of 2 and 4 mm and four different gas pressures(5,15,25,35 bars).Argon gas has been used for atomisation and as a protective gas atmosphere.Scanning electron microscope(SEM)is used to determine the shape of the produced AZ91 powder,and a laser particle size analyzer is used to analyze the powder size.Additionally,a microhardness(HV0.025)measurement has been conducted to determine the hardness of the produced powders.To achieve a homogeneous distribution,the produced powders are mixed in a three-dimensional moving turbulator for 30 min.Mixed powders have been pressed at 300,400,500 and 600 MPa and have been sintered at 500℃,550℃and 600℃.Additionally,the density values have been determined before and after sintering of the materials.SEM images have been obtained from the fractured surfaces of the samples before and after sintering.XRD and EDX analyses have been performed to determine the chemical composition.Further,microhardness(HV0.5)is obtained from the pressure surfaces of the samples to determine the effects of the pressing pressure and the sintering temperature on the hardness.As a result of the experimental studies,it has been observed that the powder size decreases with the increase in gas pressure and that the powder shape generally changes from ligament and complex shape to droplet and spherical shape.From the XRD,XRF and EDX results,it has been determined that the structure comprises an a phase(Mg main matrix)and Mg17Al12 interphase,which isβphase,and very small amounts of MgO have been observed.The hardness of the produced powders increased based on the increase in gas pressure.The densities of the samples increased with both increasing pressing pressure and sintering temperature.It has been observed from the fractured surface SEM images that the number of pores formed in the samples decrease with an increase in the pressing pressure.It has been determined that the post-sintering structure exhibitsαtypical dendritic structure.In addition to theα-Mg matrix phase,β(Mg17Al12)intermetallic andα+βeutectic were formed in the structure.The microhardness values of the samples decreased depending on the sintering temperature;the highest hardness value was measured as 64,02 HV0.5 at a pressing pressure of 300 MPa and a sintering temperature of 500℃,whereas the lowest hardness value was measured as 54,86 HV0.5 at a pressing pressure of 600 MPa and a sintering temperature of 600℃.展开更多
文摘Iron powders were mixed with graphite powders by 1-15 wt pct to produce block samples using powder metallurgy technique. The powders were blended in a three dimensional blender for 20 min and compacted in a die under 500 MPa by using a one directional press. Sinterability and mechanical properties of the samples with different carbon content were investigated. Sintering process was carried out on a belt furnace with flame curtain in dissociated ammonia atmosphere. Block samples produced were suitable for ASTM B-312 transverse rupture strength test apparatus and were tested with 0.050 kN/s velocity in a press under 100 g load. It was found that graphite amount up to 2 wt pct increased the contact area of particles and acted as a lubricant to affect the sintering behaviour positively. The results indicated that the samples containing up to 5 wt pct showed good sintering behaviour and also good hardness due to an increase in pearlite amount. However, the samples containing higher amount of graphite （more than 5 wt pct） affected the sintering behaviour negatively due to the settlement of free graphite around the Fe powders, which resulted in a decrease in the hardness and transverse rupture strength.
文摘Friction-wear properties of the ZrSiO4 reinforced samples were measured and compared with those of plain bronze based ones. For this purpose, density, hardness, friction coefficient wear behaviour of the samples were tested. Microstructures of samples before and after sintering and worn surfaces were also investigated by scanning electron microscopy （SEM）, and the wear types were determined. The optimum friction-wear behaviour was obtained in the sample compacted at 500 MPa and sintered at 820℃. Density of the final samples decreased with increasing the amount of reinforcing elements （ZrSiO4） before pre-sintering. However after sintering, there is no change in density of the samples including reinforcing elements （ZrSiO4）. With increasing friction surface temperature, a reduction in the friction coefficient of the samples was observed. However, the highest reductions in the friction coefficients were observed in the as-received samples containing 0. 5% reinforced ZrSiO4. The SEM images of the sample indicated that while bronze-based break lining material without ZrSiO4 showed abrasive wear behaviour, increasing the amount of ZrSiO4 resulted a change in abrasive to adhesive wear mechanism. All samples exhibited friction-wear values, which were within the values shown in SAE-J661 standard. With increasing the amount of reinforcing ZrSiO4, wear resistance of the samples was increased. However samples reinforced with 5% and 6% ZrSiO4 showed the best results.
文摘This study intends to determine the pressability and sinterability of AZ91 powder production by gas atomisation method and that of the produced powder for partial production.Therefore,first,a gas atomisation unit has been designed and manufactured in the laboratories of the Karabiik University,Department of Manufacturing Engineering.Atomised powder production has been achieved at a temperature of 795℃,with nozzle diameters of 2 and 4 mm and four different gas pressures(5,15,25,35 bars).Argon gas has been used for atomisation and as a protective gas atmosphere.Scanning electron microscope(SEM)is used to determine the shape of the produced AZ91 powder,and a laser particle size analyzer is used to analyze the powder size.Additionally,a microhardness(HV0.025)measurement has been conducted to determine the hardness of the produced powders.To achieve a homogeneous distribution,the produced powders are mixed in a three-dimensional moving turbulator for 30 min.Mixed powders have been pressed at 300,400,500 and 600 MPa and have been sintered at 500℃,550℃and 600℃.Additionally,the density values have been determined before and after sintering of the materials.SEM images have been obtained from the fractured surfaces of the samples before and after sintering.XRD and EDX analyses have been performed to determine the chemical composition.Further,microhardness(HV0.5)is obtained from the pressure surfaces of the samples to determine the effects of the pressing pressure and the sintering temperature on the hardness.As a result of the experimental studies,it has been observed that the powder size decreases with the increase in gas pressure and that the powder shape generally changes from ligament and complex shape to droplet and spherical shape.From the XRD,XRF and EDX results,it has been determined that the structure comprises an a phase(Mg main matrix)and Mg17Al12 interphase,which isβphase,and very small amounts of MgO have been observed.The hardness of the produced powders increased based on the increase in gas pressure.The densities of the samples increased with both increasing pressing pressure and sintering temperature.It has been observed from the fractured surface SEM images that the number of pores formed in the samples decrease with an increase in the pressing pressure.It has been determined that the post-sintering structure exhibitsαtypical dendritic structure.In addition to theα-Mg matrix phase,β(Mg17Al12)intermetallic andα+βeutectic were formed in the structure.The microhardness values of the samples decreased depending on the sintering temperature;the highest hardness value was measured as 64,02 HV0.5 at a pressing pressure of 300 MPa and a sintering temperature of 500℃,whereas the lowest hardness value was measured as 54,86 HV0.5 at a pressing pressure of 600 MPa and a sintering temperature of 600℃.
