Effect of heating time on the structural,morphology,optical,and photocatalytic properties of graphitic carbon nitride(g-C3N4)nanosheets prepared at 550℃in Ar atmosphere is studied.The investigations are carried out b...Effect of heating time on the structural,morphology,optical,and photocatalytic properties of graphitic carbon nitride(g-C3N4)nanosheets prepared at 550℃in Ar atmosphere is studied.The investigations are carried out by using x-ray diffraction(XRD),scanning electron microscopy(SEM),Fourier-transform infrared spectroscopy(FTIR),UV-vis absorption,and photoluminescence(PL).At a heating temperature of 550℃,g-C3N4 nanocrystals are formed after 0.5 h and become more orderly as the heating time increases.The surface area of the g-C3N4 nanosheets significantly increases as the preparation time increases.The g-C3N4 prepared in 2.5 h shows the highest photocatalytic performance,decomposing completely 10 ppm RhB solution under xenon lamp irradiation for 2.0 h.展开更多
We investigate the effect of synthesized time on the structure, as well as optical properties in ZnWO4 nano rod prepared by hydrothermal method. The prepared rods were characterized by X-ray diffraction (XRD), scannin...We investigate the effect of synthesized time on the structure, as well as optical properties in ZnWO4 nano rod prepared by hydrothermal method. The prepared rods were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Raman scattering, absorption and photoluminescent (PL) spectra techniques. The size and morphology of ZnWO4 nano-rod can be controlled by adjusting the reaction time. The resultant sample is a pure phase of ZnWO4 without any impurities. The results showed that the optical property of ZnWO4 nanoparticles obviously relied on their rod sizes.展开更多
基金Project supported by the scientific and technological project at the level of Ministry of Education,Vietnam(Grant No.B2018-SPH-06-CTrVL).
文摘Effect of heating time on the structural,morphology,optical,and photocatalytic properties of graphitic carbon nitride(g-C3N4)nanosheets prepared at 550℃in Ar atmosphere is studied.The investigations are carried out by using x-ray diffraction(XRD),scanning electron microscopy(SEM),Fourier-transform infrared spectroscopy(FTIR),UV-vis absorption,and photoluminescence(PL).At a heating temperature of 550℃,g-C3N4 nanocrystals are formed after 0.5 h and become more orderly as the heating time increases.The surface area of the g-C3N4 nanosheets significantly increases as the preparation time increases.The g-C3N4 prepared in 2.5 h shows the highest photocatalytic performance,decomposing completely 10 ppm RhB solution under xenon lamp irradiation for 2.0 h.
文摘We investigate the effect of synthesized time on the structure, as well as optical properties in ZnWO4 nano rod prepared by hydrothermal method. The prepared rods were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Raman scattering, absorption and photoluminescent (PL) spectra techniques. The size and morphology of ZnWO4 nano-rod can be controlled by adjusting the reaction time. The resultant sample is a pure phase of ZnWO4 without any impurities. The results showed that the optical property of ZnWO4 nanoparticles obviously relied on their rod sizes.