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聚乙烯亚胺修饰磁性纳米材料固相萃取-火焰原子吸收光谱法测定水样中痕量Mo(Ⅵ) 被引量:3
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作者 彭俊标 马晓国 陈圆 《分析测试学报》 CAS CSCD 北大核心 2021年第6期960-964,共5页
以聚乙烯亚胺(PEI)和二氧化硅包覆四氧化三铁(SiO_(2)-Fe_(3)O_(4))为原料,通过加热搅拌,制备了聚乙烯亚胺修饰磁性纳米材料(PEI-SiO_(2)-Fe_(3)O_(4))。利用红外光谱、扫描电镜和振动样品磁强计对PEI-SiO_(2)-Fe_(3)O_(4)进行了表征。... 以聚乙烯亚胺(PEI)和二氧化硅包覆四氧化三铁(SiO_(2)-Fe_(3)O_(4))为原料,通过加热搅拌,制备了聚乙烯亚胺修饰磁性纳米材料(PEI-SiO_(2)-Fe_(3)O_(4))。利用红外光谱、扫描电镜和振动样品磁强计对PEI-SiO_(2)-Fe_(3)O_(4)进行了表征。将PEI-SiO_(2)-Fe_(3)O_(4)作为吸附剂应用于Mo(Ⅵ)的磁固相萃取,结合火焰原子吸收光谱,建立了一种检测水样中痕量Mo(Ⅵ)的新方法。该方法对Mo(Ⅵ)的线性范围为10~200μg/L,检出限(LOD,S/N=3)为1.3μg·L^(-1),定量下限(LOD,S/N=10)为4.3μg/L,富集因子达172。应用建立的方法分析了环境水样、饮用水和工业废水中的Mo(Ⅵ),加标回收率为91.0%~110%,相对标准偏差(RSD)为0.90%~6.1%。该方法具有前处理速度快、灵敏、准确等特点,适用于各种水样中痕量Mo(Ⅵ)的检测。 展开更多
关键词 Mo(Ⅵ) 聚乙烯亚胺 磁固相萃取 火焰原子吸收光谱法
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A Novel Oligomer Poly (Phenylene Vinylene) Derivative Containing Oxadiazole Segment
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作者 YANG Xiao-Hui YIN Shou-Gen +5 位作者 WANG Zhen-Jia HOU Yan-Bing XU Zheng XU Xu-Rong peng jun-biao LI Wen-Lian 《Chinese Physics Letters》 SCIE CAS CSCD 2000年第1期58-60,共3页
A novel oligomer PPV derivative(OPPV)is reported,which is designed to contain the oxadiazole function segment in the main chain.Photoluminescence of the OPPV thin Him originates from aggregated states.In a double laye... A novel oligomer PPV derivative(OPPV)is reported,which is designed to contain the oxadiazole function segment in the main chain.Photoluminescence of the OPPV thin Him originates from aggregated states.In a double layer device consisting of poly phenylene vinylene(PPV)and OPPV,emission only from PPV layer was observed and the efficiency of the device was improved by about one order of magnitude compared with the single layer PPV device,this indicates the electron transport characteristic of OPPV.In the OPPV/Tb complex device^OPPV functions as the hole transport layer.A possible explanation is proposed. 展开更多
关键词 states. layer. layer
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Stimulated Emission in Blue Wavelength Region from a Copolymer
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作者 LIU Xing-yuan WANG Shu-mei +11 位作者 FENG Ji-meng LIANG Chun-jun ZHAO Dong-xu HONG Zi-ruo LI Wen-lian peng jun-biao YU Jia-qi ZHAO Jia-min WANG Li-jun WANG Li-xiang JING Xia-bin WANG Fo-song 《Chinese Physics Letters》 SCIE CAS CSCD 1999年第6期455-457,共3页
A dye laser based on the soluble conjugated polymer,Poly[1,8-octanedioxy-2,6-dimethoxy-1,4-phenylene-1,2-ethenylene-1,4-phenylene-1,2-ethenylene-3,5-dimethoxy-1,4-phenylene],has been fabricated.The laser was pumped by... A dye laser based on the soluble conjugated polymer,Poly[1,8-octanedioxy-2,6-dimethoxy-1,4-phenylene-1,2-ethenylene-1,4-phenylene-1,2-ethenylene-3,5-dimethoxy-1,4-phenylene],has been fabricated.The laser was pumped by light pulses from the third harmonic radiation of an Nd:YAG laser.The lasing was observed in the blue wavelength region with the peak at 450 nm.The threshold energy is about 19μJ.The energy conversion yield of the laser is about 3.4%.The maximum peak power of the laser output pulse arrives at about 20kW. 展开更多
关键词 ND:YAG laser PUMPED
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