A 10.35-m-long sediment core from the Luobei depression in Lop-Nur,Xinjiang,Northwest China,provides detailed information about environmental changes during the Late Pleistocene.The samples taken every 5 cm of the cor...A 10.35-m-long sediment core from the Luobei depression in Lop-Nur,Xinjiang,Northwest China,provides detailed information about environmental changes during the Late Pleistocene.The samples taken every 5 cm of the core were analyzed for 10 environmental proxies,including magnetic susceptibility,granularity,chroma,carbonate and loss on ignition(LOI),and pH value.The chronology data are provided by the uranium/thorium disequi-librium dates.The sediments of the section were deposited during the last 32000 years.The results of analysis of 10 proxies were examined using multivariate statistical analysis,and the principal components were calculated.According to the results,the Late Pleistocene sequence contains four climatic and environmental stages appearing in the cycles of cold-wet and warm-dry changes.During 10-9 ka BP,it was the earliest warm episode in the Holocene.Environmental changes in this district were restricted by global change,as suggested by the analysis of glacial-interglacial cycles.But it was different from the mutative trend of a monsoon region in East China because of its own characteristics,which was the situation of cold-wet and warm-dry climate-environment change.The candidate reason may be the uplift of the Tibet Plateau and the westerly wind circulation.展开更多
samples of lava and pumice from the cone of Changbaishan Tianchi Volcano, Jiling, China, were dated by using high precision U-series TIMS method. We conclude that the bottom of the cone formed before 350 ka, the middl...samples of lava and pumice from the cone of Changbaishan Tianchi Volcano, Jiling, China, were dated by using high precision U-series TIMS method. We conclude that the bottom of the cone formed before 350 ka, the middle part in 70～80 ka, the upper during 20～1ka, and the top less than 1ka, and the age based periods of the volcano eruption since Late Pleistocene is given as follows: >350ka,70ka,18～25ka,10ka, 4C5ka, 1～0.75ka, which may offer the basis for the study of volcanic disaster in future. In addition, the principle of dating young volcanic rocks by using U-series TIMS method is introduced briefly. Differentiation characteristics of U and Th in different minerals of the volcanic rocks are discussed, and the ability producing isochrons, based on U and Th differentiation, are discussed. In the last part of the paper, the closure of samples to the elements U and Th, which is important for age results, is discussed by using ( 234 U/ 238 U) radioactivity ratio which can be used to monitor if the samples have been weathered or eroded or leached since the time they formed. In this study, all samples have ( 234 U/ 238 U) activity ratios within 1% of secular equilibrium (( 234 U/ 238 U) radioactivity ratios are unity), indicating no disturbance of the 234 U～ 238 U system. All of these discussions show that the TIMS method is good to date Tianchi volcanics and the results are reliable.展开更多
The microprobe EDXRF equipment was used for analysis of the major and trace elements in glaze layer-transitive layer-body layer of the celadon from the Altar Yao （Kiln） and Laohudong Yao in the Southern Song Dynasty...The microprobe EDXRF equipment was used for analysis of the major and trace elements in glaze layer-transitive layer-body layer of the celadon from the Altar Yao （Kiln） and Laohudong Yao in the Southern Song Dynasty （1127-1279 A.D.）, Zhejiang, China. The K values of the discriminant factor for the celadon wares are larger than 8, which means the celadon of the Altar Yao and Laohudong Yao are different from that of the Longquan Yao. The former two belong to the Guan Yao system （the Chinese imperial kilns）, but the latter to the Min Yao system （the Chinese popular kilns）. The principle component analysis shows their relationship between the Altar and Laohudong wares with provenance postulation. The thickness of the transitive layer in the Altar and Laohudong wares is obviously different, which reveals the microstructure characteristics of the celadon even though both kinds of wares belong to the imperial kiln system.展开更多
This paper presents a study of the major and trace element compositions of fresh mantle-derived spinel lherzolite and harzburgite inclusions from Cenozoic alkaline basalt in Mount Lianshan and Mount Panshi, Liuhe Coun...This paper presents a study of the major and trace element compositions of fresh mantle-derived spinel lherzolite and harzburgite inclusions from Cenozoic alkaline basalt in Mount Lianshan and Mount Panshi, Liuhe County, Jiangsu Province. An estimation is made of the contents of the major elements and some of the trace elements in the primitive mantle source region of the area, from which the authors have obtained MgO/Al2O3= 7.86. The contents of MgO and Al2O3 are also obtained as 37.58% and 4.78% respectively based on the correlation of MgO-Al2O3. Then, the contents of various elements in the primitive mantle are calculated using their regression equations with MgO, and the compositon of the primitive mantle, a basic issue in geochemistry study, is discussed on that basis.展开更多
Dating techniques including gypsum dissolution in water, iron hydroxide co-precipitation with uranium and thorium and mass spectrometric determination have been investigated in this note. The ages of the gypsum sample...Dating techniques including gypsum dissolution in water, iron hydroxide co-precipitation with uranium and thorium and mass spectrometric determination have been investigated in this note. The ages of the gypsum samples in a CK core from Luobubo lacustrine sediments are in the range of (12.85±0.21) kaBP (4 m distance from the top core) to (153.2 ± 7.2) kaBP (49 m distance from the top core) with the relative errors of ( 1.6%-±4.7%. It indicates that the sedimental environment of the CK core was situated in the middle-late Pleistocene and Holocene periods, corresponding to 1-6 stages of oxygen isotopes in the abyssal sediments and included much information from last inter-glacial to Holocene warm periods.展开更多
A high precision thermal ionization mass spectrometric (HP-TIMS) technique is used to determine 238U,234U,232Th,230Th concentrations and their ratios in whole rocks and minerals separated from Ouaternary Maanshan, Day...A high precision thermal ionization mass spectrometric (HP-TIMS) technique is used to determine 238U,234U,232Th,230Th concentrations and their ratios in whole rocks and minerals separated from Ouaternary Maanshan, Dayingshan and Heikongshan volcanic rocks of Tengchong volcanic field .Yunnan Province, China. The 238U-230Th isochrons are given, yielding four age values (227 ? 20) ka (D-1, Dayingshan), (79.6 ±5.5) ka (D-7, Dayingshan), (21.9 ± 3.0) ka (h-1, Heikongshan), and (7.5 ± 1.0) ka (M-1, Maanshan). The result is not only consistent with but also preciser than those measured by the K-Ar method and the alpha spectrometry U-series method, indicating that the HP-TIMS method is reliable and has high precision. Besides, a procedure of HP-TIMS analysis of young volcanic rocks in China is set up preliminarily.展开更多
Ages of small aragonite samples retrieved from sediments from the Daihai Lake are determined by using the Thermal Ionization Mass Spectrometry (TIMS) technique. The ages of the samples range from (8740±601) to (1...Ages of small aragonite samples retrieved from sediments from the Daihai Lake are determined by using the Thermal Ionization Mass Spectrometry (TIMS) technique. The ages of the samples range from (8740±601) to (10446±489) a, with a precision of 2%-3% for non-corrected dating ages and 4.7%-9.8% for corrected ages respectively, and are consistent within the deviation range. At about 10.5 ka BP, the grain-size of the sediments coarsens sharply, the frequency curves of grain-size distribution show coarse grain dominated single-double kurtosis, indicating cooling, decreased hydrodynamic conditions and increased wind influence procedure. This is in good agreement with previous results obtained from the Daihai Lake, which suggests that the climate was cold and the lake surface was shrinking. The TIMS ages of the sediments are therefore believed to be credible.展开更多
Two national stalagmite standard （GBW04412, GBW04413） and one international coral standard （RKM4） have been determined by using thermal ionization mass spectrometry （TIMS） method. The values of （ 234 U/ 238 U）...Two national stalagmite standard （GBW04412, GBW04413） and one international coral standard （RKM4） have been determined by using thermal ionization mass spectrometry （TIMS） method. The values of （ 234 U/ 238 U） act , （ 230 Th/ 234 U） act and age are all consistent in error range with the standard values obtained by using α spectrometry.展开更多
基金supported by the NKBRSF Project Fund(2004CB720208)the National Natural Science Foundation of China(Nos.40599424 and 40473006)Institutions of Higher Learning Doctorate Foundation(No.20050358006).
文摘A 10.35-m-long sediment core from the Luobei depression in Lop-Nur,Xinjiang,Northwest China,provides detailed information about environmental changes during the Late Pleistocene.The samples taken every 5 cm of the core were analyzed for 10 environmental proxies,including magnetic susceptibility,granularity,chroma,carbonate and loss on ignition(LOI),and pH value.The chronology data are provided by the uranium/thorium disequi-librium dates.The sediments of the section were deposited during the last 32000 years.The results of analysis of 10 proxies were examined using multivariate statistical analysis,and the principal components were calculated.According to the results,the Late Pleistocene sequence contains four climatic and environmental stages appearing in the cycles of cold-wet and warm-dry changes.During 10-9 ka BP,it was the earliest warm episode in the Holocene.Environmental changes in this district were restricted by global change,as suggested by the analysis of glacial-interglacial cycles.But it was different from the mutative trend of a monsoon region in East China because of its own characteristics,which was the situation of cold-wet and warm-dry climate-environment change.The candidate reason may be the uplift of the Tibet Plateau and the westerly wind circulation.
文摘samples of lava and pumice from the cone of Changbaishan Tianchi Volcano, Jiling, China, were dated by using high precision U-series TIMS method. We conclude that the bottom of the cone formed before 350 ka, the middle part in 70～80 ka, the upper during 20～1ka, and the top less than 1ka, and the age based periods of the volcano eruption since Late Pleistocene is given as follows: >350ka,70ka,18～25ka,10ka, 4C5ka, 1～0.75ka, which may offer the basis for the study of volcanic disaster in future. In addition, the principle of dating young volcanic rocks by using U-series TIMS method is introduced briefly. Differentiation characteristics of U and Th in different minerals of the volcanic rocks are discussed, and the ability producing isochrons, based on U and Th differentiation, are discussed. In the last part of the paper, the closure of samples to the elements U and Th, which is important for age results, is discussed by using ( 234 U/ 238 U) radioactivity ratio which can be used to monitor if the samples have been weathered or eroded or leached since the time they formed. In this study, all samples have ( 234 U/ 238 U) activity ratios within 1% of secular equilibrium (( 234 U/ 238 U) radioactivity ratios are unity), indicating no disturbance of the 234 U～ 238 U system. All of these discussions show that the TIMS method is good to date Tianchi volcanics and the results are reliable.
文摘The microprobe EDXRF equipment was used for analysis of the major and trace elements in glaze layer-transitive layer-body layer of the celadon from the Altar Yao （Kiln） and Laohudong Yao in the Southern Song Dynasty （1127-1279 A.D.）, Zhejiang, China. The K values of the discriminant factor for the celadon wares are larger than 8, which means the celadon of the Altar Yao and Laohudong Yao are different from that of the Longquan Yao. The former two belong to the Guan Yao system （the Chinese imperial kilns）, but the latter to the Min Yao system （the Chinese popular kilns）. The principle component analysis shows their relationship between the Altar and Laohudong wares with provenance postulation. The thickness of the transitive layer in the Altar and Laohudong wares is obviously different, which reveals the microstructure characteristics of the celadon even though both kinds of wares belong to the imperial kiln system.
基金This study was supported by the National Natural Science Foundation of China Grants 49573173 and 49673186.
文摘This paper presents a study of the major and trace element compositions of fresh mantle-derived spinel lherzolite and harzburgite inclusions from Cenozoic alkaline basalt in Mount Lianshan and Mount Panshi, Liuhe County, Jiangsu Province. An estimation is made of the contents of the major elements and some of the trace elements in the primitive mantle source region of the area, from which the authors have obtained MgO/Al2O3= 7.86. The contents of MgO and Al2O3 are also obtained as 37.58% and 4.78% respectively based on the correlation of MgO-Al2O3. Then, the contents of various elements in the primitive mantle are calculated using their regression equations with MgO, and the compositon of the primitive mantle, a basic issue in geochemistry study, is discussed on that basis.
基金This work was supported by the National Key Basis Research Project (Grant No. G19990434) the Innovative Project of the Chinese Academy of Sciences (Grant No. KZCX 1-y 05) and the Resources and Environment Basis Project of the University of Science an
文摘Dating techniques including gypsum dissolution in water, iron hydroxide co-precipitation with uranium and thorium and mass spectrometric determination have been investigated in this note. The ages of the gypsum samples in a CK core from Luobubo lacustrine sediments are in the range of (12.85±0.21) kaBP (4 m distance from the top core) to (153.2 ± 7.2) kaBP (49 m distance from the top core) with the relative errors of ( 1.6%-±4.7%. It indicates that the sedimental environment of the CK core was situated in the middle-late Pleistocene and Holocene periods, corresponding to 1-6 stages of oxygen isotopes in the abyssal sediments and included much information from last inter-glacial to Holocene warm periods.
文摘A high precision thermal ionization mass spectrometric (HP-TIMS) technique is used to determine 238U,234U,232Th,230Th concentrations and their ratios in whole rocks and minerals separated from Ouaternary Maanshan, Dayingshan and Heikongshan volcanic rocks of Tengchong volcanic field .Yunnan Province, China. The 238U-230Th isochrons are given, yielding four age values (227 ? 20) ka (D-1, Dayingshan), (79.6 ±5.5) ka (D-7, Dayingshan), (21.9 ± 3.0) ka (h-1, Heikongshan), and (7.5 ± 1.0) ka (M-1, Maanshan). The result is not only consistent with but also preciser than those measured by the K-Ar method and the alpha spectrometry U-series method, indicating that the HP-TIMS method is reliable and has high precision. Besides, a procedure of HP-TIMS analysis of young volcanic rocks in China is set up preliminarily.
基金the National Key BasicResearch Development Project (Grant No. 1999043401) the Key Project of Knowledge Innovation of the CAS (Grant No. KZCX1-Y-05)+1 种基金 the Key Project of the CAS (Grant Nos. KZ952-J1-015 and KZ-951-A1-402) and the National Outstandin
文摘Ages of small aragonite samples retrieved from sediments from the Daihai Lake are determined by using the Thermal Ionization Mass Spectrometry (TIMS) technique. The ages of the samples range from (8740±601) to (10446±489) a, with a precision of 2%-3% for non-corrected dating ages and 4.7%-9.8% for corrected ages respectively, and are consistent within the deviation range. At about 10.5 ka BP, the grain-size of the sediments coarsens sharply, the frequency curves of grain-size distribution show coarse grain dominated single-double kurtosis, indicating cooling, decreased hydrodynamic conditions and increased wind influence procedure. This is in good agreement with previous results obtained from the Daihai Lake, which suggests that the climate was cold and the lake surface was shrinking. The TIMS ages of the sediments are therefore believed to be credible.
文摘Two national stalagmite standard （GBW04412, GBW04413） and one international coral standard （RKM4） have been determined by using thermal ionization mass spectrometry （TIMS） method. The values of （ 234 U/ 238 U） act , （ 230 Th/ 234 U） act and age are all consistent in error range with the standard values obtained by using α spectrometry.
