High-intensity ultrasonic vibration was focused on the tip of conical steel specimens to induce severe plastic deformation at room temperature. We found, for the first time, that grain size smaller than 200 nm was obt...High-intensity ultrasonic vibration was focused on the tip of conical steel specimens to induce severe plastic deformation at room temperature. We found, for the first time, that grain size smaller than 200 nm was obtained. Furthermore, the sharp tip of the conical specimen became umbrella-shaped or disk-shaped. The tip size changed from 0.5 mm diameter to a disk about 5 mm diameter, representing a large amount of plastic deformation in the metal at the tip of the conical specimen.展开更多
The nano--crystal composite WO_3-TiO_2 photocatalyst was prepared by ultrasonic as-sisted sol--gel process. The effects of various factors, such as the crystal form, thesubstrates, the pH, the dissolved oxygen and the...The nano--crystal composite WO_3-TiO_2 photocatalyst was prepared by ultrasonic as-sisted sol--gel process. The effects of various factors, such as the crystal form, thesubstrates, the pH, the dissolved oxygen and the ultrasonic on the photocatalytic ac-tivity were investigated in view of the photodegradation of Rhodamine B. The resultsshow that the crystal form of WO_3-TiO_2 film with highest photocatalytic activity isrutile. The introduction of ultrasonic to the course of preparation can accelerate thedeposit time of the sol and increase the photocatalytic activity significantly in view ofthe highest photodegradation of Rhodamine B being 72.7% in 5 hours. The poroustitanium plate is the most suitable substrate in four kinds of investigated materials.Meanwhile the smaller the pH and the higher the concentration of the dissolved oxygenin the solution is, the higher the photodegradation is.展开更多
文摘High-intensity ultrasonic vibration was focused on the tip of conical steel specimens to induce severe plastic deformation at room temperature. We found, for the first time, that grain size smaller than 200 nm was obtained. Furthermore, the sharp tip of the conical specimen became umbrella-shaped or disk-shaped. The tip size changed from 0.5 mm diameter to a disk about 5 mm diameter, representing a large amount of plastic deformation in the metal at the tip of the conical specimen.
基金This work was supported by the National Natural Science Fundation of China(No.50105003).|
文摘The nano--crystal composite WO_3-TiO_2 photocatalyst was prepared by ultrasonic as-sisted sol--gel process. The effects of various factors, such as the crystal form, thesubstrates, the pH, the dissolved oxygen and the ultrasonic on the photocatalytic ac-tivity were investigated in view of the photodegradation of Rhodamine B. The resultsshow that the crystal form of WO_3-TiO_2 film with highest photocatalytic activity isrutile. The introduction of ultrasonic to the course of preparation can accelerate thedeposit time of the sol and increase the photocatalytic activity significantly in view ofthe highest photodegradation of Rhodamine B being 72.7% in 5 hours. The poroustitanium plate is the most suitable substrate in four kinds of investigated materials.Meanwhile the smaller the pH and the higher the concentration of the dissolved oxygenin the solution is, the higher the photodegradation is.