A new hapten, aldicarb oxime succinic ester (AOSE), was synthesized for immunoassay of aldicarb. It was conjugated to proteins by active ester method. Polyclonal antibody was raised against AOSE-BSA (bovine serum a...A new hapten, aldicarb oxime succinic ester (AOSE), was synthesized for immunoassay of aldicarb. It was conjugated to proteins by active ester method. Polyclonal antibody was raised against AOSE-BSA (bovine serum albumin) conjugate. Enzyme-linked immunosorbent assays (ELISAs) showed that this antiserum had high affinity to aldicarb and can be used for sensitive and selective immunoassay of aldicarb.展开更多
In the synthesis of HMS, Soxhlet extraction as a new method to remove neutral template was studied. HREM image, X-ray diffraction patterns and nitrogen adsorption-desorption results verified that this method can not o...In the synthesis of HMS, Soxhlet extraction as a new method to remove neutral template was studied. HREM image, X-ray diffraction patterns and nitrogen adsorption-desorption results verified that this method can not only efficiently remove and recover the template, but also benefit the maintenance of the mesoporous framework structure.展开更多
The hexagonal liquid crystal mediated synthesis of nanostructured PbS was studied. Thioacetamide and lead acetate were used as the sulfide and lead source, respectively. It was found that the nanohole structure of PdS...The hexagonal liquid crystal mediated synthesis of nanostructured PbS was studied. Thioacetamide and lead acetate were used as the sulfide and lead source, respectively. It was found that the nanohole structure of PdS was formed in this system.展开更多
文摘A new hapten, aldicarb oxime succinic ester (AOSE), was synthesized for immunoassay of aldicarb. It was conjugated to proteins by active ester method. Polyclonal antibody was raised against AOSE-BSA (bovine serum albumin) conjugate. Enzyme-linked immunosorbent assays (ELISAs) showed that this antiserum had high affinity to aldicarb and can be used for sensitive and selective immunoassay of aldicarb.
基金financially supported by the National High Technology Research and Development Program of China(No.2007AA03Z532)the National Natural Science Foundation of China(No.20774015)the China National Petroleum Corporation Innovation Fund(No.07E1034)
基金the foundation support from the National Natural Science Foundation (Project No. 29890210) and the Research Fund for the Doctora
文摘In the synthesis of HMS, Soxhlet extraction as a new method to remove neutral template was studied. HREM image, X-ray diffraction patterns and nitrogen adsorption-desorption results verified that this method can not only efficiently remove and recover the template, but also benefit the maintenance of the mesoporous framework structure.
基金The authors would like to thank NNSFC ado. 29890210) and RFDP (No. 9800if8) for fund support.
文摘The hexagonal liquid crystal mediated synthesis of nanostructured PbS was studied. Thioacetamide and lead acetate were used as the sulfide and lead source, respectively. It was found that the nanohole structure of PdS was formed in this system.