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基于锥面衍射实现高效率双光栅光谱合成
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作者 吴娟 李建民 +4 位作者 尹新启 曾理江 邱克强 李朝明 颜宏 《强激光与粒子束》 EI CAS CSCD 北大核心 2020年第12期83-87,共5页
分析了基于锥面衍射的双光栅光谱合成系统的可行性,设计了激光入射角为Littrow角附近的双多层介质膜(MLD)光栅光谱合成系统,开展了两路合成实验。当入射极角等于自准直入射角,入射方位角为6°时,光栅衍射效率近似等于光束自准直入... 分析了基于锥面衍射的双光栅光谱合成系统的可行性,设计了激光入射角为Littrow角附近的双多层介质膜(MLD)光栅光谱合成系统,开展了两路合成实验。当入射极角等于自准直入射角,入射方位角为6°时,光栅衍射效率近似等于光束自准直入射时的衍射效率。基于锥面衍射原理,对中心波长为1050.24 nm和1064.33 nm的两束光纤激光子束进行合成,入射极角为43.99°,测得合成效率为92.9%,较基于非锥面衍射的双光栅光谱合成系统的合成效率提高了8.8%;测得合成光斑光束质量Mx 2=1.204,My 2=1.467,与基于非锥面衍射的双光栅光谱合成系统输出光斑光束质量基本一致。 展开更多
关键词 锥面衍射 非锥面衍射 双MLD光栅 光谱合成 合成效率
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高硬度Mg-5Al-2Sn-5Ca镁合金在铸态与热处理后的蠕变行为 被引量:4
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作者 热焱 邱克强 +4 位作者 李东和 丁韧 王梅 徐慧 徐颖 《材料导报》 EI CAS CSCD 北大核心 2020年第12期12076-12082,共7页
本工作借鉴MRI230D合金的设计思路,通过添加Al、Ca、Sn等元素,采用普通铸造工艺制备了一种新型的Mg-5Al-2Sn-5Ca镁合金。使用XRD衍射仪、扫描电子显微镜对样品进行表征,采用图像处理显微维氏硬度计和蠕变试验机测试合金在铸态与热处理... 本工作借鉴MRI230D合金的设计思路,通过添加Al、Ca、Sn等元素,采用普通铸造工艺制备了一种新型的Mg-5Al-2Sn-5Ca镁合金。使用XRD衍射仪、扫描电子显微镜对样品进行表征,采用图像处理显微维氏硬度计和蠕变试验机测试合金在铸态与热处理后的力学性能。研究结果表明:该合金由α-Mg、Al 2Ca、Mg 2Ca、CaMgSn相组成;铸态及经热处理后(热处理态)的合金晶界处均分布着连续的骨架状相,具有较高的维氏硬度,且热处理态合金的晶粒内部有微小颗粒状相析出;在520℃,该合金才发生相变,说明合金具有较高的耐热性能。分别在50 MPa/200℃下对铸态合金和热处理态合金进行蠕变试验,结果发现,相比于铸态合金,经热处理后合金的总蠕变时间延长至540 h,蠕变总量降低了0.001%,但在100 h时的蠕变量减少了0.030%。对比其他研究者的蠕变数据可知,在相同条件下,该铸态合金的蠕变性能远优于MRI153镁合金;热处理后的合金在50 MPa/200℃的蠕变断裂时间也长于A380铝合金。 展开更多
关键词 铸态 热处理 镁合金 骨架状相 显微维氏硬度 蠕变时间
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Application of digital pattern-less molding technology to produce art casting 被引量:5
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作者 Chen Li Zhang Wei +4 位作者 Wu Chenhong Jia Baochang Xiang Qingchun qiu keqiang Li Rongde 《China Foundry》 SCIE CAS 2014年第6期487-492,共6页
Compared with the conventional casting process, digital pattern-less casting technology has many advantages such as good machining accuracy, a short processing cycle, and low production cost. It is a new rapid manufac... Compared with the conventional casting process, digital pattern-less casting technology has many advantages such as good machining accuracy, a short processing cycle, and low production cost. It is a new rapid manufacturing technology for castings, integrated with CAD/CAM, casting, CNC machining and many other advanced technologies. With this digital casting technology, no pattern is needed for making molds; it is precise, f lexible, and green. Usually, art castings have complex structures and are made in small batches or even made in a single-piece, especially for large-sized art castings. So it has the shortcomings of high cost, low eff iciency and long time for making a pattern to produce art castings with the conventional casting processes. However, the digital pattern-less casting technology can be applied to fabricate art castings, since it can greatly shorten the manufacturing cycle and lower the production cost, thus having a very good prospect. In this study, based on the digital pattern-less casting technology, a plaque casting with artistic Chinese characters(a Chinese poem) was designed and manufactured, and the production process was demonstrated in detail. 展开更多
关键词 DIGITAL pattern-less casting art castings
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Efects of minor amounts of scandium on microstructure and mechanical properties of ZA27 alloy 被引量:1
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作者 Xiang Qingchun Zhang Wei +2 位作者 Wang Ruichun qiu keqiang Li Rongde 《China Foundry》 SCIE CAS 2013年第5期294-298,共5页
The influences of minor amounts of scandium on the microstructure and mechanical properties of as-cast ZA27 alloy have been experimentally investigated.The experimental results show that as far as the Sc addition is i... The influences of minor amounts of scandium on the microstructure and mechanical properties of as-cast ZA27 alloy have been experimentally investigated.The experimental results show that as far as the Sc addition is individually concerned,the refinement result of the as-cast ZA27 alloy with 0.5wt.%Sc addition is comparatively better.After alloying with minor amounts of Sc,the coarse dendrites of the ZA27 alloy are refined and transformed into the uniform and small equiaxed grain microstructure;also the eutectics among the grain boundaries become finer.The test results of mechanical properties show that the tensile strength and hardness of the as-cast ZA27 alloy containing 0.5wt.%Sc approach 495 MPa and 120.2 HB,increase by28.5%and 33.1%,respectively,compared with those of the ZA27 alloy with no addition of Sc element,while the elongation of the alloy is improved to 7.6%from 2.7%.The SEM,EDAX and XRD analyses show that in the ZA27 alloy,the trace element Sc combines with Al to form the square Al3Sc phase particles,which serve as heterogeneous nuclei,facilitating the refinement of the microstructure and the improvement of the mechanical properties of the alloy. 展开更多
关键词 ZA27 alloy SCANDIUM MICROSTRUCTURE mechanical properties heterogeneous nuclei
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激光选区熔化甲烷水蒸气催化重整器的结构与催化效率研究
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作者 王文旋 刘敏 +4 位作者 邱克强 董东东 刘太楷 李艳辉 闫星辰 《材料导报》 EI CAS CSCD 北大核心 2022年第S01期43-48,共6页
氢气是新一代清洁能源的代表,甲烷重整制氢是获得氢气的重要技术。激光选区熔化技术可实现重整器的结构功能一体化,简化制备流程,因此本工作通过计算机辅助软件进行设计并建模得到具有极小曲面结构的蜂窝式催化重整器模型,采用激光选区... 氢气是新一代清洁能源的代表,甲烷重整制氢是获得氢气的重要技术。激光选区熔化技术可实现重整器的结构功能一体化,简化制备流程,因此本工作通过计算机辅助软件进行设计并建模得到具有极小曲面结构的蜂窝式催化重整器模型,采用激光选区熔化技术制备了具有不同壁厚及不同孔径的催化重整器,研究了负载催化剂前后重整器表面宏观、微观形貌及物相组成的变化,并结合甲烷水蒸气催化重整机理研究分析得出重整器壁厚、孔径、比表面积及催化温度对氢气转化率的影响规律及机理。结果表明:重整器壁厚对氢气转化效率的影响并不显著;反应温度的升高可提高氢气转化率,当温度为900℃时,氢气转化率最高;同时,当孔径过小时,由于反应过程中产生积碳、流速过快导致氢气转化率降低,适当地增大孔径可使转化率提升,在此适当的孔径前提下,氢气的转化率随着重整器的比表面积增大而提高。 展开更多
关键词 甲烷 水蒸气 催化重整器 催化剂 氢气浓度
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Microstructures and formation mechanism of hypoeutectic white cast iron by isothermal electromagnetic rheocast process
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作者 Zhang Wanning Song Dan +3 位作者 Zhang Hongbing Li Deyuan Yuan Xiaoguang qiu keqiang 《China Foundry》 SCIE CAS 2010年第2期113-116,共4页
An investigation was made on the evolution of microstructures of hypoeutectic white cast iron slurry containing 2.5wt.%C and 1.8wt.%Si produced by rheocasting in which the solidifying alloy was vigorously agitated by ... An investigation was made on the evolution of microstructures of hypoeutectic white cast iron slurry containing 2.5wt.%C and 1.8wt.%Si produced by rheocasting in which the solidifying alloy was vigorously agitated by electromagnetic stirrer during isothermal cooling processes.The results indicated that under the proper agitating temperatures and speeds applied,the dendrite structures in white cast iron slurry were gradually evolved into spherical structures during a certain agitating time.It also revealed that the bent dendrites were formed by either convection force or by the growth of the dendrites themselves in the bending direction;then,as they were in solidifying,they were gradually being alternated into separated particles and into more spherical structures at the end of the isothermal cooling process.Especially,the dendrites were granulated as the bending process proceeding,which suggested that they were caused by unwanted elements such as sulfur and phosphor usually contained in engineering cast iron.Convective-ow of the melt caused corrosion on the dendritic segments where they were weaker in strength and lower in melting temperature because of higher concentration of sulfur or phosphor.And the granulation process for such dendrites formed in the melt became possible under the condition.Certainly,dendrite fragments are another factors considerable to function for spherical particles formation.A new mechanism,regarding to the rheocast structure formation of white cast iron,was suggested based on the structural evolution observed in the study. 展开更多
关键词 电磁搅拌器 微观结构 等温过程 白口铸铁 亚共晶 机制 弯曲过程 球形微粒
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Morphology and microstructure of rapidly solidified tin-lead alloy powders
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作者 Xiang Qingchun Zhang Wei +2 位作者 qiu keqiang Qu Yingdong Li Rongde 《China Foundry》 SCIE CAS 2014年第5期428-434,共7页
Sn60Pb40 alloy powders were fabricated using the planar flow casting(PFC) atomization process. By using OM, SEM and EPMA, the characteristics of the morphologies and microstructures of the powders have been investigat... Sn60Pb40 alloy powders were fabricated using the planar flow casting(PFC) atomization process. By using OM, SEM and EPMA, the characteristics of the morphologies and microstructures of the powders have been investigated. It is observed that the environment of ambient gas in the atomization box has great effects on the morphology of the alloy powders. The microstructures of Sn60Pb40 alloy powders produced by the PFC atomization process are completely composed of eutectic, which is made up of both oversaturated α solid solution and β solid solution. The microstructures of small size powders are extraordinarily undeveloped dendritic eutectic, in which the large majority of the α phase appears nearly spherical, evidently since the cooling rate is higher and the under-cooling is larger. As for the large size powders, since the cooling rate and undercooling are relatively low, lamellar α phase apparently increases in the eutectic microstructures of these powders, and there is even typical lamellar eutectic structure clearly observed in some micro-areas. After remelting tests by DTA, the microstructures of small size powders are transformed, which become composed of large crumby α phase and eutectic(α+β), while those of large size powders change into classical tin-lead structures of primary α phase plus lamellar eutectic(α+β). By studying the microstructures of tin-lead alloy powders, a model has been proposed to predict the microstructure formation of Sn60Pb40 alloy powders. 展开更多
关键词 rapid solidification planar flow casting tin-lead alloy metal powders MICROSTRUCTURE
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激光熔覆高耐磨无裂纹双层Fe基非晶复合涂层
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作者 张新宇 吕威闫 +1 位作者 邱克强 曲迎东 《特种铸造及有色合金》 CAS 北大核心 2024年第5期692-698,共7页
在40Cr钢表面采用SAM2X5非晶合金粉末分别进行了单层和不同扫描速度的双层激光熔覆,制备了无裂纹Fe基非晶复合涂层。分析了双层熔覆工艺对Fe基非晶复合涂层的微观组织、元素分布、硬度及耐磨性的影响。结果表明,双层熔覆Fe基非晶合金复... 在40Cr钢表面采用SAM2X5非晶合金粉末分别进行了单层和不同扫描速度的双层激光熔覆,制备了无裂纹Fe基非晶复合涂层。分析了双层熔覆工艺对Fe基非晶复合涂层的微观组织、元素分布、硬度及耐磨性的影响。结果表明,双层熔覆Fe基非晶合金复合涂层能够提升涂层的硬度和耐磨性。另外,随第2层激光扫描速度增加,基体对涂层的成分稀释作用减小且涂层的硬度和耐磨性随之提升。第2层激光扫描速度为1 m/min时涂层硬度最高,平均硬度(HV0.1)达到852,约为基体的3倍。涂层耐磨性远高于基体,在第2层扫描速度为1 m/min时涂层耐磨性达到最优,磨损体积仅为基体的28%。 展开更多
关键词 激光熔覆 无裂纹 FE基非晶 硬度 耐磨性
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用长程面形仪对变线距光栅的线密度进行拼接测量
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作者 韦怀坤 宦述虎 +4 位作者 刘颖 陈火耀 邱克强 刘正坤 洪义麟 《光学学报》 EI CAS CSCD 北大核心 2023年第3期124-131,共8页
随着同步辐射光源中光束线的分辨率不断提高,衍射光栅成为影响分辨率的关键因素,因此,在将光栅安装到光束线之前,需要进行准确的测试。用长程面形仪测量合肥光源光电子能谱线所需的变线距光栅的线密度,光栅衍射角变化范围超出长程面形... 随着同步辐射光源中光束线的分辨率不断提高,衍射光栅成为影响分辨率的关键因素,因此,在将光栅安装到光束线之前,需要进行准确的测试。用长程面形仪测量合肥光源光电子能谱线所需的变线距光栅的线密度,光栅衍射角变化范围超出长程面形仪的测量范围,因此采用拼接测量。用数据重叠测试及数据处理方法,消除了转台定位误差,有效抑制了随机误差,使光栅周期测量的重复性有较大提高。不同重叠率的测试结果显示,测量一致性优于1.13×10-6(RMS),满足了变线距光栅的测试需求。 展开更多
关键词 测量 衍射测量 变线距光栅 拼接测量 长程面形仪
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用于检测光栅线密度的长程面形仪系统 被引量:4
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作者 吴新朴 韦怀坤 +3 位作者 刘正坤 邱克强 徐向东 洪义麟 《光学学报》 EI CAS CSCD 北大核心 2021年第6期140-148,共9页
衍射光栅已被广泛应用于同步辐射光源软X射线与真空紫外光栅单色器中,光栅线密度偏差会直接影响单色器的性能。为了检测光栅线密度的偏差,本文在合肥先进光源预研过程中搭建了长程面形仪(LTP)系统。使用自准直仪对LTP检测光栅系统在26μ... 衍射光栅已被广泛应用于同步辐射光源软X射线与真空紫外光栅单色器中,光栅线密度偏差会直接影响单色器的性能。为了检测光栅线密度的偏差,本文在合肥先进光源预研过程中搭建了长程面形仪(LTP)系统。使用自准直仪对LTP检测光栅系统在26μrad内的检测精度进行了标定。利用LTP对自主研制的760 line/mm与2400 line/mm等间距光栅进行线密度均匀性检测,使用干涉仪对760 line/mm光栅进行0级与1级衍射波前检测,并将检测结果与LTP测量结果进行比较。结果表明:系统标定的均方根误差为30 nrad,与干涉仪检测结果相比,两者同位置处的高度轮廓曲线具有较好的一致性。这说明搭建的LTP系统具有较高精度的检测光栅线密度的能力,为检测同步辐射光栅线密度的变化提供了平台。 展开更多
关键词 测量 长程面形仪 等间距光栅 线密度均匀性
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光谱巡天科学级紫外光栅的研制 被引量:1
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作者 陈力斯 胡中文 +1 位作者 邱克强 姜海娇 《中国激光》 EI CAS CSCD 北大核心 2022年第6期147-158,共12页
不同于国际上其他空间项目采用光栅切换的光谱获取方式,中国空间巡天望远镜采用近焦面拼接光栅的方式获取大视场、宽波段无缝光谱,波长覆盖范围为250~1000nm,光谱分辨率R≥200。国内紫外透射衍射光栅的天文应用尚在起步阶段,制作难度高... 不同于国际上其他空间项目采用光栅切换的光谱获取方式,中国空间巡天望远镜采用近焦面拼接光栅的方式获取大视场、宽波段无缝光谱,波长覆盖范围为250~1000nm,光谱分辨率R≥200。国内紫外透射衍射光栅的天文应用尚在起步阶段,制作难度高,且不能从国外获得。经过多年努力,光栅性能在近期获得了较大提升。本文针对紫外光栅的科学应用性能和使用条件,分析了衍射光栅制作参数的优化,给出了衍射效率随入射角、入射光偏振态以及光栅槽形结构参数的变化规律。相关数据对在轨流量定标具有借鉴价值。通过选用不同的光栅结构参数对衍射效率特性进行分析,发现了紫外光栅峰值波长与顶角投影在每个周期上的比值之间的近似线性表达关系。本文讨论了满足科学需求的参数许可域,并将其用于控制光栅制作参数。多次试验后,光栅槽形结构参数和形状得到了精确控制,获得了性能优异的衍射光栅。制作的光栅线密度为333line/mm,闪耀角为12.51°,峰值效率波长控制在315nm,紫外波段实测峰值衍射效率为72.3%,平均效率为65.1%。该光栅的槽形、波前质量等均控制在较高水平,衍射波前质量均方根(RMS)达到0.06λ,峰谷值(PV值)达到了0.33λ。采用该光栅可获得良好的成像质量。 展开更多
关键词 光栅 光谱巡天 衍射效率 衍射波前 像质
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