Colloidal silver nanoparticles (Ag-NPs) were obtained through γ-irradiation of aqueous solutions containing AgNO3 and gelatin as a silver source and stabilizer, respectively. The absorbed dose of γ-irradiation inf...Colloidal silver nanoparticles (Ag-NPs) were obtained through γ-irradiation of aqueous solutions containing AgNO3 and gelatin as a silver source and stabilizer, respectively. The absorbed dose of γ-irradiation influences the particle diameter of the Ag-NPs, as evidenced from surface plasmon resonance (SPR) and transmission electron microscopy (TEM) images. When the γ-irradiation dose was increased (from 2 to 50 kGy), the mean particle size was decreased continuously as a result of γ-induced Ag-NPs fragmentation. The antibacterial properties of the Ag-NPs were tested against Methicillinresistant Staphylococcus aureus (MRSA) (Gram-positive) and Pseudomonas aeruginosa (P.a) (Gram-negative) bacteria. This approach reveals that the γ-irradiation-mediated method is a promising simple route for synthesizing highly stable Ag-NPs in aqueous solutions with good antibacterial properties for different applications.展开更多
A laser ablation technique is applied for synthesis of silver nanoparticles in different concentrations of polyvinyl alcohol (PVA) aqueous solution. The ablation of high pure silver plate in the solution is carried ...A laser ablation technique is applied for synthesis of silver nanoparticles in different concentrations of polyvinyl alcohol (PVA) aqueous solution. The ablation of high pure silver plate in the solution is carried out by a nanosecond Q-switched Nd:YAG pulsed laser. X-ray diffraction and transmission electron microscopy are implemented to explore the particles sizes. The effects of PYA concentrations on the absorbance of the silver nanoparticles are studied as well, by using a UV-vis spectrophotometer. The preparation process is carried out for deionized water as a reference sample. The comparison of the obtained results with the reference sample shows that the formation efficiency of nanoparticles in PYA is much higher and the sizes of particles are also smaller.展开更多
Er-doped Y_(2)O_(3),Bi_(2)O_(3)and Sb_(2)O_(3)nanoparticles are synthesized using pulsed laser ablation in a liquid.Ceramic targets of Y_(2)O_(3):Er^(3+),Bi_(2)O_(3):Er^(3+)and Sb_(2)O_(3):Er^(3+)for ablation process ...Er-doped Y_(2)O_(3),Bi_(2)O_(3)and Sb_(2)O_(3)nanoparticles are synthesized using pulsed laser ablation in a liquid.Ceramic targets of Y_(2)O_(3):Er^(3+),Bi_(2)O_(3):Er^(3+)and Sb_(2)O_(3):Er^(3+)for ablation process are prepared by standard solid-state reaction technique and ablation is carried out in 5-ml distilled water using nanosecond Q-switched Nd:YAG laser.The morphology and size of the fabricated nanoparticles are evaluated by transmission electron microscopy and the luminescence emission properties of the prepared samples are investigated under different excitation wavelengths.展开更多
文摘Colloidal silver nanoparticles (Ag-NPs) were obtained through γ-irradiation of aqueous solutions containing AgNO3 and gelatin as a silver source and stabilizer, respectively. The absorbed dose of γ-irradiation influences the particle diameter of the Ag-NPs, as evidenced from surface plasmon resonance (SPR) and transmission electron microscopy (TEM) images. When the γ-irradiation dose was increased (from 2 to 50 kGy), the mean particle size was decreased continuously as a result of γ-induced Ag-NPs fragmentation. The antibacterial properties of the Ag-NPs were tested against Methicillinresistant Staphylococcus aureus (MRSA) (Gram-positive) and Pseudomonas aeruginosa (P.a) (Gram-negative) bacteria. This approach reveals that the γ-irradiation-mediated method is a promising simple route for synthesizing highly stable Ag-NPs in aqueous solutions with good antibacterial properties for different applications.
文摘A laser ablation technique is applied for synthesis of silver nanoparticles in different concentrations of polyvinyl alcohol (PVA) aqueous solution. The ablation of high pure silver plate in the solution is carried out by a nanosecond Q-switched Nd:YAG pulsed laser. X-ray diffraction and transmission electron microscopy are implemented to explore the particles sizes. The effects of PYA concentrations on the absorbance of the silver nanoparticles are studied as well, by using a UV-vis spectrophotometer. The preparation process is carried out for deionized water as a reference sample. The comparison of the obtained results with the reference sample shows that the formation efficiency of nanoparticles in PYA is much higher and the sizes of particles are also smaller.
基金Supported by University Putra Malaysia and FCT(Fundação para a Ciência e a Tecnologia)for Post-Doctoral Research under Grant No SFRH/BPD/76185/2011the Research University Grant Scheme of Higher Education Malaysia(No 05-01-09-0754RU).
文摘Er-doped Y_(2)O_(3),Bi_(2)O_(3)and Sb_(2)O_(3)nanoparticles are synthesized using pulsed laser ablation in a liquid.Ceramic targets of Y_(2)O_(3):Er^(3+),Bi_(2)O_(3):Er^(3+)and Sb_(2)O_(3):Er^(3+)for ablation process are prepared by standard solid-state reaction technique and ablation is carried out in 5-ml distilled water using nanosecond Q-switched Nd:YAG laser.The morphology and size of the fabricated nanoparticles are evaluated by transmission electron microscopy and the luminescence emission properties of the prepared samples are investigated under different excitation wavelengths.