Thermal stability and high-temperature mechanical properties of a 304 L austenitic oxide dispersion strengthened(ODS)alloy manufactured via laser powder bed fusion(LPBF)are examined in this work.Additively manufacture...Thermal stability and high-temperature mechanical properties of a 304 L austenitic oxide dispersion strengthened(ODS)alloy manufactured via laser powder bed fusion(LPBF)are examined in this work.Additively manufactured 304 L ODS alloy samples were aged at temperatures of 1000,1100,and 1200℃for 100 h in an argon atmosphere.Microstructure characterization of LPBF 304 L ODS alloy before and after the thermal stability experiments revealed that despite the annihilation of dislocations,induced cellular substructure by the LPBF process was partially retained in the ODS alloy even after aging at1200℃.The size of Y-Si-O nanoparticles after aging at 1200℃increased from 25 to 50 nm.EBSD analysis revealed that nanoparticles retained the microstructure of LPBF 304 L ODS and hindered recrystallization and further grain growth.At 600℃and 800℃,the yield stress of the 290 and 145 MPa were measured,respectively,which are substantially higher than 113 MPa,and 68 MPa for 304 L at the same temperatures.Furthermore,the creep properties of LPBF 304 L ODS alloy were evaluated at a temperature of 700℃under three applied stresses of 70,85,and 100 MPa yielding a stress exponent(n)of 7.7;the minimum creep rate at 100 MPa was found to be about two orders of magnitude lower than found in the literature for wrought 304 L stainless steel.展开更多
基金the funding of critical equipment provided by the Murdock Charitable Trust(No.2016231:MNL:5/18/2017)the RAPID Institute,the U.S.DOE(No.DE-EE0007888)the NSF Advanced Manufacturing Program(No.1856412)for the financial support。
文摘Thermal stability and high-temperature mechanical properties of a 304 L austenitic oxide dispersion strengthened(ODS)alloy manufactured via laser powder bed fusion(LPBF)are examined in this work.Additively manufactured 304 L ODS alloy samples were aged at temperatures of 1000,1100,and 1200℃for 100 h in an argon atmosphere.Microstructure characterization of LPBF 304 L ODS alloy before and after the thermal stability experiments revealed that despite the annihilation of dislocations,induced cellular substructure by the LPBF process was partially retained in the ODS alloy even after aging at1200℃.The size of Y-Si-O nanoparticles after aging at 1200℃increased from 25 to 50 nm.EBSD analysis revealed that nanoparticles retained the microstructure of LPBF 304 L ODS and hindered recrystallization and further grain growth.At 600℃and 800℃,the yield stress of the 290 and 145 MPa were measured,respectively,which are substantially higher than 113 MPa,and 68 MPa for 304 L at the same temperatures.Furthermore,the creep properties of LPBF 304 L ODS alloy were evaluated at a temperature of 700℃under three applied stresses of 70,85,and 100 MPa yielding a stress exponent(n)of 7.7;the minimum creep rate at 100 MPa was found to be about two orders of magnitude lower than found in the literature for wrought 304 L stainless steel.
