Cemented paste backfill(CPB)is a key technology for green mining in metal mines,in which tailings thickening comprises the primary link of CPB technology.However,difficult flocculation and substandard concentrations o...Cemented paste backfill(CPB)is a key technology for green mining in metal mines,in which tailings thickening comprises the primary link of CPB technology.However,difficult flocculation and substandard concentrations of thickened tailings often occur.The rheological properties and concentration evolution in the thickened tailings remain unclear.Moreover,traditional indoor thickening experiments have yet to quantitatively characterize their rheological properties.An experiment of flocculation condition optimization based on the Box-Behnken design(BBD)was performed in the study,and the two response values were investigated:concentration and the mean weighted chord length(MWCL)of flocs.Thus,optimal flocculation conditions were obtained.In addition,the rheological properties and concentration evolution of different flocculant dosages and ultrafine tailing contents under shear,compression,and compression-shear coupling experimental conditions were tested and compared.The results show that the shear yield stress under compression and compression-shear coupling increases with the growth of compressive yield stress,while the shear yield stress increases slightly under shear.The order of shear yield stress from low to high under different thickening conditions is shear,compression,and compression-shear coupling.Under compression and compression-shear coupling,the concentration first rapidly increases with the growth of compressive yield stress and then slowly increases,while concentration increases slightly under shear.The order of concentration from low to high under different thickening conditions is shear,compression,and compression-shear coupling.Finally,the evolution mechanism of the flocs and drainage channels during the thickening of the thickened tailings under different experimental conditions was revealed.展开更多
The research on tight oil becomes another hotspot in the field of unconventional oil and gas after the boom of shale gas.The global recoverable resources of tight oil are estimated to be around 47.3×10^(9)t.In re...The research on tight oil becomes another hotspot in the field of unconventional oil and gas after the boom of shale gas.The global recoverable resources of tight oil are estimated to be around 47.3×10^(9)t.In recent years,significant progress has been made in the technologies of tight oil exploration and development in North America,thus stimulating the dramatic increase of tight oil production.Meanwhile,China has also acquired remarkable achievements in tight oil exploration.Mature assessment methods have been established for tight oil resources by the US,generally dominated by analogy and statistical methods with their own advantages and disadvantages as well as applicable conditions.In China,improvement of resource evaluation techniques becomes an urgent issue in increasing tight oil reserve and production.This study mainly discusses the resource evaluation methods and resource enrichment characteristics of tight oil.Seven kinds of assessment methods in three categories(i.e.,analogy,statistical and genetic method)and evaluation parameters have been preliminary established,and are specifically applied in the Sichuan,Ordos,Songliao,Junggar,Bohai Bay and other tight oil basins through the newly hierarchical resource abundance analogy method,the estimated ultimate recovery(EUR)analogy method and the small-cell volumetric method.The preliminary evaluation results reveal that China has great potential in tight oil resource,and the geological resources amount to 20×10^(9)t,providing a resource base for large-scale development.展开更多
Through test analysis of large amount of cores,rock fragments and crude oil samples,and in combination with dynamic data of production from 456 oil wells,hydrocarbon generation potentials of four major source rocks an...Through test analysis of large amount of cores,rock fragments and crude oil samples,and in combination with dynamic data of production from 456 oil wells,hydrocarbon generation potentials of four major source rocks and accumulation characteristics of three major pay layers in the Jurassic of Sichun Basin were well investigated.Results indicated that source rocks in the Lianggaoshan Formation,the Da'anzhai Member and the Dongyuemiao Member mainly generated oil,and those in the Zhenzhuchong Member dominantly generated gas;the organic-rich source rocks controlled distribution of sweet spots of tight oil,and most industrial oil wells were located at the area with high-quality source rocks(TOC>1.2%);and micron-sized pore throats were effective storage space,and fractures played a key role in initial high yield.Jurassic tight oil in the Sichuan Basin was characterized by light oil,high gas-oil ratio and abnormal high pressure,which were favorable for tight oil flow and output.Four methods(i.e.,small bin method,resource abundance analogy method,EUR analogy method and total organic carbon method)were used to estimate Jurassic oil in-place in the Sichuan Basin which ranged from 2×10^(9) to 3×10^(9) t.Through analysis of main controlling factors of resource enrichment,the grading criteria were established for the evaluation of oil in-place in the Sichuan Basin.Through the small bin method,the oil in-place of Type I,Type II and Type III was 1.611×10^(9)t,0.477×10^(9)t and 0.289×10^(9)t,respectively.It was predicted that the largest exploration potential of the Da'anzhai Member was in the Nanchong-Suining area and the east of Liangping area,the most favorable exploration area of the Lianggaoshan Formation was in the Guang'anNanchong-Suining-Yilong area,and the good exploration prospect of the Dongyuemiao Member was in the south of the Guang'an-Suining area.展开更多
Through analysis of the connotation of unconventional hydrocarbons,the source-reservoir assemblages of unconventional hydrocarbons are divided into three types,i.e.,source-reservoir neighboring type,source-reservoir i...Through analysis of the connotation of unconventional hydrocarbons,the source-reservoir assemblages of unconventional hydrocarbons are divided into three types,i.e.,source-reservoir neighboring type,source-reservoir integration type,and source-reservoir separation type.The source-reservoir neighboring type resources mainly include tight oil and tight gas with the following formation conditions and characteristics:(1)efficient near-source accumulation close to high-quality source rocks with the pressure difference between source and reservoir as the dynamic force;(2)large-area tight reservoirs with certain porosity,dominated by micro-nanopores of inorganic origin;(3)distributed in depressions and slopes with large hydrocarbon-bearing area and great resource quantity,low abundance and local development of“sweet spots”;(4)weak tectonism.The source-reservoir integration type resources mainly include coalbed methane,shale gas,shale oil and oil shale.The formation conditions and characteristics are:(1)high abundance of organic matter,different types of organic matter and thermal evolution grades leading to formation of different resources types;(2)organic-rich sections are distributed continuously in the reservoiring space which is dominated by nanometer organic pores,interparticle pores and microfissures;(3)hydrocarbons mainly occur in free or adsorbed state,varying much with resource type;(4)the resources are self-conserved,and enriched in depressions and slopes,the conservation conditions are controlled by tectonics,temperature and pressure;(5)the production per well can be enhanced by volume fracturing,which increases the permeability of the reservoirs.The source-reservoir separation type resources are more special,mainly including(1)transformed conventional resources such as oil sand and heavy oil;(2)unsteady resources formed under special conditions of temperature and pressure,among which natural gas hydrate is a representative.These three types of resources in China are different in both development prospect and current situation:(1)the source-reservoir neighboring type is most practical and will develop fast in the next 5 years;(2)the source-reservoir integration type needs continuous exploration and technical breakthrough,and is expected to develop rapidly in the coming decade;(3)in the source-reservoir separation type resources,natural gas hydrates have the greatest development potential,on which technical tests are being conducted.展开更多
基金financially supported by the National Natural Science Foundation of China(Nos.52130404 and 52304121)the Fundamental Research Funds for the Central Universities(No.FRF-TP-22-112A1)+4 种基金the Guangdong Basic and Applied Basic Research Foundation(No.2021A 1515110161)the ANID(Chile)through Fondecyt project 1210610the Centro de Modelamiento Matemático(BASAL funds for Centers of Excellence FB210005)the CRHIAM project ANID/FONDAP/15130015 and ANID/FONDAP/1523A0001the Anillo project ANID/ACT210030。
文摘Cemented paste backfill(CPB)is a key technology for green mining in metal mines,in which tailings thickening comprises the primary link of CPB technology.However,difficult flocculation and substandard concentrations of thickened tailings often occur.The rheological properties and concentration evolution in the thickened tailings remain unclear.Moreover,traditional indoor thickening experiments have yet to quantitatively characterize their rheological properties.An experiment of flocculation condition optimization based on the Box-Behnken design(BBD)was performed in the study,and the two response values were investigated:concentration and the mean weighted chord length(MWCL)of flocs.Thus,optimal flocculation conditions were obtained.In addition,the rheological properties and concentration evolution of different flocculant dosages and ultrafine tailing contents under shear,compression,and compression-shear coupling experimental conditions were tested and compared.The results show that the shear yield stress under compression and compression-shear coupling increases with the growth of compressive yield stress,while the shear yield stress increases slightly under shear.The order of shear yield stress from low to high under different thickening conditions is shear,compression,and compression-shear coupling.Under compression and compression-shear coupling,the concentration first rapidly increases with the growth of compressive yield stress and then slowly increases,while concentration increases slightly under shear.The order of concentration from low to high under different thickening conditions is shear,compression,and compression-shear coupling.Finally,the evolution mechanism of the flocs and drainage channels during the thickening of the thickened tailings under different experimental conditions was revealed.
基金This work was funded by Major Scientific and Technological Project of PetroChina(Grant No.2014E-050202).
文摘The research on tight oil becomes another hotspot in the field of unconventional oil and gas after the boom of shale gas.The global recoverable resources of tight oil are estimated to be around 47.3×10^(9)t.In recent years,significant progress has been made in the technologies of tight oil exploration and development in North America,thus stimulating the dramatic increase of tight oil production.Meanwhile,China has also acquired remarkable achievements in tight oil exploration.Mature assessment methods have been established for tight oil resources by the US,generally dominated by analogy and statistical methods with their own advantages and disadvantages as well as applicable conditions.In China,improvement of resource evaluation techniques becomes an urgent issue in increasing tight oil reserve and production.This study mainly discusses the resource evaluation methods and resource enrichment characteristics of tight oil.Seven kinds of assessment methods in three categories(i.e.,analogy,statistical and genetic method)and evaluation parameters have been preliminary established,and are specifically applied in the Sichuan,Ordos,Songliao,Junggar,Bohai Bay and other tight oil basins through the newly hierarchical resource abundance analogy method,the estimated ultimate recovery(EUR)analogy method and the small-cell volumetric method.The preliminary evaluation results reveal that China has great potential in tight oil resource,and the geological resources amount to 20×10^(9)t,providing a resource base for large-scale development.
基金supported by the Major Science and Technology Project of the Ministry of Land and Resources of China(2015YQKYQ01)Petro China Major Science and Technology Project(2012E-2601,2013E-0502).
文摘Through test analysis of large amount of cores,rock fragments and crude oil samples,and in combination with dynamic data of production from 456 oil wells,hydrocarbon generation potentials of four major source rocks and accumulation characteristics of three major pay layers in the Jurassic of Sichun Basin were well investigated.Results indicated that source rocks in the Lianggaoshan Formation,the Da'anzhai Member and the Dongyuemiao Member mainly generated oil,and those in the Zhenzhuchong Member dominantly generated gas;the organic-rich source rocks controlled distribution of sweet spots of tight oil,and most industrial oil wells were located at the area with high-quality source rocks(TOC>1.2%);and micron-sized pore throats were effective storage space,and fractures played a key role in initial high yield.Jurassic tight oil in the Sichuan Basin was characterized by light oil,high gas-oil ratio and abnormal high pressure,which were favorable for tight oil flow and output.Four methods(i.e.,small bin method,resource abundance analogy method,EUR analogy method and total organic carbon method)were used to estimate Jurassic oil in-place in the Sichuan Basin which ranged from 2×10^(9) to 3×10^(9) t.Through analysis of main controlling factors of resource enrichment,the grading criteria were established for the evaluation of oil in-place in the Sichuan Basin.Through the small bin method,the oil in-place of Type I,Type II and Type III was 1.611×10^(9)t,0.477×10^(9)t and 0.289×10^(9)t,respectively.It was predicted that the largest exploration potential of the Da'anzhai Member was in the Nanchong-Suining area and the east of Liangping area,the most favorable exploration area of the Lianggaoshan Formation was in the Guang'anNanchong-Suining-Yilong area,and the good exploration prospect of the Dongyuemiao Member was in the south of the Guang'an-Suining area.
基金This work was funded by National Science and Technology Major Project of China(Grant No.2011ZX05043)Major Science and Technology Special Project of China National Petroleum Corporation(Grant No:2013E-0502)。
文摘Through analysis of the connotation of unconventional hydrocarbons,the source-reservoir assemblages of unconventional hydrocarbons are divided into three types,i.e.,source-reservoir neighboring type,source-reservoir integration type,and source-reservoir separation type.The source-reservoir neighboring type resources mainly include tight oil and tight gas with the following formation conditions and characteristics:(1)efficient near-source accumulation close to high-quality source rocks with the pressure difference between source and reservoir as the dynamic force;(2)large-area tight reservoirs with certain porosity,dominated by micro-nanopores of inorganic origin;(3)distributed in depressions and slopes with large hydrocarbon-bearing area and great resource quantity,low abundance and local development of“sweet spots”;(4)weak tectonism.The source-reservoir integration type resources mainly include coalbed methane,shale gas,shale oil and oil shale.The formation conditions and characteristics are:(1)high abundance of organic matter,different types of organic matter and thermal evolution grades leading to formation of different resources types;(2)organic-rich sections are distributed continuously in the reservoiring space which is dominated by nanometer organic pores,interparticle pores and microfissures;(3)hydrocarbons mainly occur in free or adsorbed state,varying much with resource type;(4)the resources are self-conserved,and enriched in depressions and slopes,the conservation conditions are controlled by tectonics,temperature and pressure;(5)the production per well can be enhanced by volume fracturing,which increases the permeability of the reservoirs.The source-reservoir separation type resources are more special,mainly including(1)transformed conventional resources such as oil sand and heavy oil;(2)unsteady resources formed under special conditions of temperature and pressure,among which natural gas hydrate is a representative.These three types of resources in China are different in both development prospect and current situation:(1)the source-reservoir neighboring type is most practical and will develop fast in the next 5 years;(2)the source-reservoir integration type needs continuous exploration and technical breakthrough,and is expected to develop rapidly in the coming decade;(3)in the source-reservoir separation type resources,natural gas hydrates have the greatest development potential,on which technical tests are being conducted.