Graphene/Inconel 718 composites were innovatively synthesized through selective laser melting,and the mechanical and tribological performances of the grapheme-reinforced Inconel 718 matrix composites were evaluated.Th...Graphene/Inconel 718 composites were innovatively synthesized through selective laser melting,and the mechanical and tribological performances of the grapheme-reinforced Inconel 718 matrix composites were evaluated.The composite microstructures were characterized by XRD,SEM and Raman spectroscopy.The results show that selective laser melting is a viable method to fabricate Inconel 718 matrix composite and the addition of graphene nanoplatelets leads to a significant strengthening of Inconel 718 alloy,as well as the improvement of tribological performance.The yield strength and ultimate tensile strength of 1.0%graphene/Inconel 718 composites(mass fraction)are 42%and 53%higher than those of pure material,and the friction coefficient and wear rate are 22.4%and 66.8%lower than those of pure material.The decrease of fraction coefficient and wear rate is attributed to the improved hardness of composites and the formation of graphene nanoplatelet protective layer on the worn surfaces.展开更多
The influence of the boriding conditions on the boride layers was examined by boriding Ti−6Al−2Zr−1Mo−1V alloy in the temperature range of 920−1120℃.The experimental results show that the boride layers were composed ...The influence of the boriding conditions on the boride layers was examined by boriding Ti−6Al−2Zr−1Mo−1V alloy in the temperature range of 920−1120℃.The experimental results show that the boride layers were composed of a continuous thin outer layer of TiB_(2) and a thick inner layer of TiB with whiskers or needle-like morphologies that extended into the substrate.Thick and compact boride layers were obtained when the boriding temperatures were 1000−1080℃,and the treatment time exceeded 8 h.The boride layer depth increased with the boriding temperature and time,and the growth kinetics of the boride layers was characterized by a parabolic curve.The growth kinetics of the boride layers,including both TiB_(2) and TiB layers,were predicted by establishing a diffusion model,which presented satisfactory consistency with the experimental data.As a result,the activation energies of boron in the TiB_(2) and TiB layers were estimated to be 223.1 and 246.9 kJ/mol,respectively.展开更多
Isothermal β heat treatments of Ti-6.5 Al-3.5 Mo-1.5 Zr-0.3 Si alloy were performed at the temperature of1040-1240 ℃ to examine the influence of heating conditions on grain growth of the alloy. The results show that...Isothermal β heat treatments of Ti-6.5 Al-3.5 Mo-1.5 Zr-0.3 Si alloy were performed at the temperature of1040-1240 ℃ to examine the influence of heating conditions on grain growth of the alloy. The results show that the grain size increases with heating temperature and holding time increasing. Rapid β grain growth of the alloy takes place at the temperature of over 1140 ℃. The grain growth kinetics for the alloy follows the classical isothermal grain growth law.The growth time exponent(n) of 0.5651 and activation energy(Q) of 129.6 kJ mol-1 are determined. Finally, in order to determine the grain size under different heating conditions,the grain growth model of the alloy was established.展开更多
The isothermal compression test for Ti-6Al-7Nb alloy was conducted by using Gleeble-3800 thermal simulator.The hot deformation behavior of Ti-6Al-7Nb alloy was investigated in the deformation temperature ranges of 940...The isothermal compression test for Ti-6Al-7Nb alloy was conducted by using Gleeble-3800 thermal simulator.The hot deformation behavior of Ti-6Al-7Nb alloy was investigated in the deformation temperature ranges of 940-1030℃and the strain rate ranges of 0.001-10 s^(-1).Meanwhile,the activation energy of thermal deformation was computed.The results show that the flow stress of Ti-6Al-7Nb alloy increases with increasing the strain rate and decreasing the deformation temperature.The activation energy of thermal deformation for Ti-6Al-7Nb alloy is much greater than that for self-diffusion ofα-Ti andβ-Ti.Considering the influence of strain on flow stress,the strain-compensated Arrhenius constitutive model of Ti-6Al-7Nb alloy was established.The error analysis shows that the model has higher accuracy,and the correlation coefficient r and average absolute relative error are 0.9879 and 4.11%,respectively.The processing map(PM)of Ti-6Al-7Nb alloy was constructed by the dynamic materials model and Prasad instability criterion.According to PM and microstructural observation,it is found that the main form of instability zone is local flow,and the deformation mechanisms of the stable zone are mainly superplasticity and dynamic recrystallization.The optimal processing parameters of Ti-6Al-7Nb alloy are determined as follows:960-995℃/0.01-0.18 s^(-1)and 1000-1030℃/0.001-0.01 s^(-1).展开更多
The hot deformation behavior of Ti 5.6Al-4.8Sn-2.0Zr-1.0Mo 0.35Si 0.85Nd alloy in β/quasi-β forging process was studied using isothermal compression tests over temperature range from 1040℃ to 1 100 ℃ and strain ra...The hot deformation behavior of Ti 5.6Al-4.8Sn-2.0Zr-1.0Mo 0.35Si 0.85Nd alloy in β/quasi-β forging process was studied using isothermal compression tests over temperature range from 1040℃ to 1 100 ℃ and strain rates form 0. 001 s-1 to 70 s -1. The results show that the flow stress and mierostrueture are sensitive to thermomechanical parameters. The processing maps based on the dynamic materials model at strain of 0.3 and 0.7 were established. The optimum deformation thermomechanical parameters at a strain of 0.7 have two regions that exhibit the peak of power dissipation efficiency. One is the region of 1062-1100 ℃ and 10- 3 10-1.5 s -1 ; and another which represents dynamic recrystallization is 1040-1045 ℃ and 10-1.8 10- 0.5 s -1. The instable region is located where the strain rate is larger than 1 s 1 which corresponds to the mechanical instability.展开更多
基金Project supported by the Ganpo 555 Program for Leading Talents of Jiangxi Province,China
文摘Graphene/Inconel 718 composites were innovatively synthesized through selective laser melting,and the mechanical and tribological performances of the grapheme-reinforced Inconel 718 matrix composites were evaluated.The composite microstructures were characterized by XRD,SEM and Raman spectroscopy.The results show that selective laser melting is a viable method to fabricate Inconel 718 matrix composite and the addition of graphene nanoplatelets leads to a significant strengthening of Inconel 718 alloy,as well as the improvement of tribological performance.The yield strength and ultimate tensile strength of 1.0%graphene/Inconel 718 composites(mass fraction)are 42%and 53%higher than those of pure material,and the friction coefficient and wear rate are 22.4%and 66.8%lower than those of pure material.The decrease of fraction coefficient and wear rate is attributed to the improved hardness of composites and the formation of graphene nanoplatelet protective layer on the worn surfaces.
基金The authors are grateful for the financial supports from the National Natural Science Foundation of China(Nos.51761029,51864035)the Natural Science Foundation of Jiangxi Province,China(Nos.2020BABL204011 and 2020BABL204007)Key Laboratory for Microstructural Control of Metallic Materials of Jiangxi Province(Nanchang Hangkong University),China(Nos.EJ201701513 and EJ201901454).
文摘The influence of the boriding conditions on the boride layers was examined by boriding Ti−6Al−2Zr−1Mo−1V alloy in the temperature range of 920−1120℃.The experimental results show that the boride layers were composed of a continuous thin outer layer of TiB_(2) and a thick inner layer of TiB with whiskers or needle-like morphologies that extended into the substrate.Thick and compact boride layers were obtained when the boriding temperatures were 1000−1080℃,and the treatment time exceeded 8 h.The boride layer depth increased with the boriding temperature and time,and the growth kinetics of the boride layers was characterized by a parabolic curve.The growth kinetics of the boride layers,including both TiB_(2) and TiB layers,were predicted by establishing a diffusion model,which presented satisfactory consistency with the experimental data.As a result,the activation energies of boron in the TiB_(2) and TiB layers were estimated to be 223.1 and 246.9 kJ/mol,respectively.
基金financially supported by the National Natural Science Foundation of China (No. 51261020)the Aeronautical Science Foundation of China(No. 2014ZE56015)the Educational Committee of Jiangxi Province of China(No. GJJ14505)
文摘Isothermal β heat treatments of Ti-6.5 Al-3.5 Mo-1.5 Zr-0.3 Si alloy were performed at the temperature of1040-1240 ℃ to examine the influence of heating conditions on grain growth of the alloy. The results show that the grain size increases with heating temperature and holding time increasing. Rapid β grain growth of the alloy takes place at the temperature of over 1140 ℃. The grain growth kinetics for the alloy follows the classical isothermal grain growth law.The growth time exponent(n) of 0.5651 and activation energy(Q) of 129.6 kJ mol-1 are determined. Finally, in order to determine the grain size under different heating conditions,the grain growth model of the alloy was established.
基金the National Natural Science Foundation of China(Grant No.51464035).
文摘The isothermal compression test for Ti-6Al-7Nb alloy was conducted by using Gleeble-3800 thermal simulator.The hot deformation behavior of Ti-6Al-7Nb alloy was investigated in the deformation temperature ranges of 940-1030℃and the strain rate ranges of 0.001-10 s^(-1).Meanwhile,the activation energy of thermal deformation was computed.The results show that the flow stress of Ti-6Al-7Nb alloy increases with increasing the strain rate and decreasing the deformation temperature.The activation energy of thermal deformation for Ti-6Al-7Nb alloy is much greater than that for self-diffusion ofα-Ti andβ-Ti.Considering the influence of strain on flow stress,the strain-compensated Arrhenius constitutive model of Ti-6Al-7Nb alloy was established.The error analysis shows that the model has higher accuracy,and the correlation coefficient r and average absolute relative error are 0.9879 and 4.11%,respectively.The processing map(PM)of Ti-6Al-7Nb alloy was constructed by the dynamic materials model and Prasad instability criterion.According to PM and microstructural observation,it is found that the main form of instability zone is local flow,and the deformation mechanisms of the stable zone are mainly superplasticity and dynamic recrystallization.The optimal processing parameters of Ti-6Al-7Nb alloy are determined as follows:960-995℃/0.01-0.18 s^(-1)and 1000-1030℃/0.001-0.01 s^(-1).
基金Item Sponsored by National Natural Science Foundation of China(51164030,51261020)Education Commission Foundation of Jiangxi Province of China(GJJ13501)
文摘The hot deformation behavior of Ti 5.6Al-4.8Sn-2.0Zr-1.0Mo 0.35Si 0.85Nd alloy in β/quasi-β forging process was studied using isothermal compression tests over temperature range from 1040℃ to 1 100 ℃ and strain rates form 0. 001 s-1 to 70 s -1. The results show that the flow stress and mierostrueture are sensitive to thermomechanical parameters. The processing maps based on the dynamic materials model at strain of 0.3 and 0.7 were established. The optimum deformation thermomechanical parameters at a strain of 0.7 have two regions that exhibit the peak of power dissipation efficiency. One is the region of 1062-1100 ℃ and 10- 3 10-1.5 s -1 ; and another which represents dynamic recrystallization is 1040-1045 ℃ and 10-1.8 10- 0.5 s -1. The instable region is located where the strain rate is larger than 1 s 1 which corresponds to the mechanical instability.