In this study,a KrF excimer laser was used to modify the biodegradable Mg-1Ca alloy and the time-evolution degradation behavior of the alloy before and after laser treatment was investigated in simulated body fluid(SB...In this study,a KrF excimer laser was used to modify the biodegradable Mg-1Ca alloy and the time-evolution degradation behavior of the alloy before and after laser treatment was investigated in simulated body fluid(SBF)solution using immersion tests and electrochemical impedance spectroscopy(EIS).A 5μm melted layer with a homogeneous microstructure and an MgO film on the surface were achieved by laser radiation.Corrosion observations(hydrogen evolution,morphology and corrosion products)and EIS results revealed an improvement of corrosion resistance after laser treatment for 48 h.It was found a two-layer structure developed after 2 h immersion on both the untreated and laser-treated alloys,but the sequence of forming the two layers was opposite and greatly influenced by the laser-treated layer.The time-evolution corrosion processes on the untreated and laser-treated alloys were discussed,providing a better understanding of corrosion behavior of biodegradable Mg alloys modified by excimer laser.展开更多
To investigate the influence of stress alone on the stray field signals of ferromagnetic materials,the static tensile tests of 0.45%C steel and 45CrNiMoVA steel flat-shaped specimens were performed on an MTS810 hydrau...To investigate the influence of stress alone on the stray field signals of ferromagnetic materials,the static tensile tests of 0.45%C steel and 45CrNiMoVA steel flat-shaped specimens were performed on an MTS810 hydraulic testing machine. Hp(y) signals,the normal component of spontaneous stray field,were measured during the testing process by an EMS-2003 metal magnetic memory diagnostic apparatus cooperated with a non-magnetic electric control displacement instrument. Fracture and microstructure were observed by a scanning electronic microscope and a transmission electron microscope,respectively. The relationships between axial applied stress or residual stress measured by X-ray diffraction method and Hp(y) were analyzed. The results indicate that some regular pattern of the magnetic curve is displayed only between applied stress and stray field signals. The magnetic ordering process stops due to dislocation pinning magnetic domain structure,and Hp(y) value unvaried nearly with applied load increasing in the plastic deformation stage.展开更多
This study attempts to investigate how the slippery surface of Nepenthes alata pitchers restricts the attachment ability of ant Camponotus japonicus Mayr, via climbing behavior observation and friction force measureme...This study attempts to investigate how the slippery surface of Nepenthes alata pitchers restricts the attachment ability of ant Camponotus japonicus Mayr, via climbing behavior observation and friction force measurement. Ants exhibited ineffective climbing behaviors and rather small friction forces when attached to upward-oriented slippery surfaces, but opposite phenomena were shown when on inverted surfaces. Friction forces of intact, claw tip-removed and pad-destroyed ants were measured on intact and de-waxed slippery surfaces, exploring the roles of wax crystals and lunate cells in restricting ant's attachment. On downward-directed slippery surfaces, greater forces were exhibited by intact and pad-destroyed ants; on the two slippery sur- faces, pad-destroyed ants presented slightly smaller forces and clawless ants generated considerably smaller forces. Somewhat different force was provided by clawless ants on upward and downward oriented slippery surfaces, and slightly higher force was shown when ants climbed on wax-removed surface. Results indicate that the lunate cells contribute greatly to decrease the friction force, whereas the wax crystals perform a supplementary role. Mechanical analysis suggests that the directionally growing lunate cells possess a sloped structure that effectively prevents the claw's mechanical interlock, reducing the ant's attachment ability considerably. Our conclusion supports a further interpretation of slippery surface's anti-attachment mecha- nism, also provides theoretical reference to develop biomimetic slippery plate to trap agricultural insect.展开更多
文摘In this study,a KrF excimer laser was used to modify the biodegradable Mg-1Ca alloy and the time-evolution degradation behavior of the alloy before and after laser treatment was investigated in simulated body fluid(SBF)solution using immersion tests and electrochemical impedance spectroscopy(EIS).A 5μm melted layer with a homogeneous microstructure and an MgO film on the surface were achieved by laser radiation.Corrosion observations(hydrogen evolution,morphology and corrosion products)and EIS results revealed an improvement of corrosion resistance after laser treatment for 48 h.It was found a two-layer structure developed after 2 h immersion on both the untreated and laser-treated alloys,but the sequence of forming the two layers was opposite and greatly influenced by the laser-treated layer.The time-evolution corrosion processes on the untreated and laser-treated alloys were discussed,providing a better understanding of corrosion behavior of biodegradable Mg alloys modified by excimer laser.
基金the National Natural Science Foundation of China (No 50235030 and No 50505052)
文摘To investigate the influence of stress alone on the stray field signals of ferromagnetic materials,the static tensile tests of 0.45%C steel and 45CrNiMoVA steel flat-shaped specimens were performed on an MTS810 hydraulic testing machine. Hp(y) signals,the normal component of spontaneous stray field,were measured during the testing process by an EMS-2003 metal magnetic memory diagnostic apparatus cooperated with a non-magnetic electric control displacement instrument. Fracture and microstructure were observed by a scanning electronic microscope and a transmission electron microscope,respectively. The relationships between axial applied stress or residual stress measured by X-ray diffraction method and Hp(y) were analyzed. The results indicate that some regular pattern of the magnetic curve is displayed only between applied stress and stray field signals. The magnetic ordering process stops due to dislocation pinning magnetic domain structure,and Hp(y) value unvaried nearly with applied load increasing in the plastic deformation stage.
基金We acknowledge Zhao Lei (The State Key Labo- ratory of Tribology, TsingHua University) for helping in the SWLI examinations. We sincerely thank the National Natural Science Foundation of China (No. 51205107), the Natural Science Foundation of Hebei province (No. E2014208056), and the Tribology Science Fund of State Key Laboratory of Tribology (No. SKLTKF13B05) for their financial supports.
文摘This study attempts to investigate how the slippery surface of Nepenthes alata pitchers restricts the attachment ability of ant Camponotus japonicus Mayr, via climbing behavior observation and friction force measurement. Ants exhibited ineffective climbing behaviors and rather small friction forces when attached to upward-oriented slippery surfaces, but opposite phenomena were shown when on inverted surfaces. Friction forces of intact, claw tip-removed and pad-destroyed ants were measured on intact and de-waxed slippery surfaces, exploring the roles of wax crystals and lunate cells in restricting ant's attachment. On downward-directed slippery surfaces, greater forces were exhibited by intact and pad-destroyed ants; on the two slippery sur- faces, pad-destroyed ants presented slightly smaller forces and clawless ants generated considerably smaller forces. Somewhat different force was provided by clawless ants on upward and downward oriented slippery surfaces, and slightly higher force was shown when ants climbed on wax-removed surface. Results indicate that the lunate cells contribute greatly to decrease the friction force, whereas the wax crystals perform a supplementary role. Mechanical analysis suggests that the directionally growing lunate cells possess a sloped structure that effectively prevents the claw's mechanical interlock, reducing the ant's attachment ability considerably. Our conclusion supports a further interpretation of slippery surface's anti-attachment mecha- nism, also provides theoretical reference to develop biomimetic slippery plate to trap agricultural insect.