(Ti,Al,Zr)N/(Ti,Al,Zr,Cr)N bilayer films were deposited on cemented carbide (WC-8%Co) substrates by multi-arc ion plating (MAIP) using two Ti-AI-Zr alloy targets and one pure Cr target. To investigate the comp...(Ti,Al,Zr)N/(Ti,Al,Zr,Cr)N bilayer films were deposited on cemented carbide (WC-8%Co) substrates by multi-arc ion plating (MAIP) using two Ti-AI-Zr alloy targets and one pure Cr target. To investigate the composition, morphology, and crystalline structure of the bilayer films, a number of complementary methods of elemental and structural analysis were used, namely, scanning electron microscopy (SEM), energy disperse X-ray spectroscopy (EDS), and X-ray diffraction (XRD). Adhesive strength and mechanical properties of the films were evaluated by scratch testing and Vickers microindentation, respectively. It is shown that the resulting films have a TiN-type face-centered cubic (FCC) structure. The films exhibit fully dense, uniform, and columnar morphology. Furthermore, as the bias voltages vary from -50 to -200 V, the microhardness (max. Hv001 4100) and adhesive strength (max. 〉 200 N) of the bilayer films are superior to those of the (Ti,Al,Zr)N and (Ti,Al,Zr, Cr)N monolayer films.展开更多
CrN/(Ti,Al,Zr,Cr) N bilayer films were successfully deposited on cemented carbide( WC-8% Co) substrates by multi-arc ion plating process using two Ti-Al-Zr alloy targets and one pure Cr target. As a result of bila...CrN/(Ti,Al,Zr,Cr) N bilayer films were successfully deposited on cemented carbide( WC-8% Co) substrates by multi-arc ion plating process using two Ti-Al-Zr alloy targets and one pure Cr target. As a result of bilayered structure and addition of alloying elements( e. g. Al and Cr),the films exhibited excellent high temperature oxidation resistance under both short-term isothermal( up to 800 ℃) and long-term cyclic( up to 600 ℃) exposure conditions. Combined with pre-established outstanding tribological properties( e. g. maximum hardness of 4 000HV0. 01 and maximum adhesion strength over 200 N),these observations make such films quite a promising candidate to extend the cutting tool life span and boost the performance in high-productivity,high-speed and high-feed cutting or in dry machining conditions.展开更多
基金financially supported by the Foundation of Education Department of Liaoning Province(No.L2012430)the Foundation of Science and Technology Department of Liaoning Province(No.2011221007)the Open Foundation of Key Laboratory for Advanced Materials Preparation Technology of Liaoning Province,China(No.1120211406)
文摘(Ti,Al,Zr)N/(Ti,Al,Zr,Cr)N bilayer films were deposited on cemented carbide (WC-8%Co) substrates by multi-arc ion plating (MAIP) using two Ti-AI-Zr alloy targets and one pure Cr target. To investigate the composition, morphology, and crystalline structure of the bilayer films, a number of complementary methods of elemental and structural analysis were used, namely, scanning electron microscopy (SEM), energy disperse X-ray spectroscopy (EDS), and X-ray diffraction (XRD). Adhesive strength and mechanical properties of the films were evaluated by scratch testing and Vickers microindentation, respectively. It is shown that the resulting films have a TiN-type face-centered cubic (FCC) structure. The films exhibit fully dense, uniform, and columnar morphology. Furthermore, as the bias voltages vary from -50 to -200 V, the microhardness (max. Hv001 4100) and adhesive strength (max. 〉 200 N) of the bilayer films are superior to those of the (Ti,Al,Zr)N and (Ti,Al,Zr, Cr)N monolayer films.
基金financially supported by Natural Science Foundation of Liaoning Province of China(No.2014020096)Shenyang Science and Technology Plan Project of Liaoning Province of China(No.F14-231-119 )Shenyang Yongyuan Guanghui Machinery Factory Transverse Project of Liaoning Province of China(No.201521010100051)
文摘CrN/(Ti,Al,Zr,Cr) N bilayer films were successfully deposited on cemented carbide( WC-8% Co) substrates by multi-arc ion plating process using two Ti-Al-Zr alloy targets and one pure Cr target. As a result of bilayered structure and addition of alloying elements( e. g. Al and Cr),the films exhibited excellent high temperature oxidation resistance under both short-term isothermal( up to 800 ℃) and long-term cyclic( up to 600 ℃) exposure conditions. Combined with pre-established outstanding tribological properties( e. g. maximum hardness of 4 000HV0. 01 and maximum adhesion strength over 200 N),these observations make such films quite a promising candidate to extend the cutting tool life span and boost the performance in high-productivity,high-speed and high-feed cutting or in dry machining conditions.