This work outlines the characterization of epoxy resin[Bisphenol A-(epichlorhydrin):epoxy]and hardener[N(3-dimethylaminopropyl)-1,3-propylenediamine]with various inorganic nano-fillers.Dielectric characterizations of ...This work outlines the characterization of epoxy resin[Bisphenol A-(epichlorhydrin):epoxy]and hardener[N(3-dimethylaminopropyl)-1,3-propylenediamine]with various inorganic nano-fillers.Dielectric characterizations of epoxy,hardener,neat epoxy(epoxy+hardener)and nano-epoxy(nano-filler+neat epoxy)composites loaded with 1 wt.%of inorganic nano-fillers(SiO_(2),Al_(2)O_(3),TiO_(2)and ZnO)were carried out using precision LCR meter,over the frequency range of 1 kHz-2 MHz at a constant temperature of 300.15 K.The structural information of nano-fillers,neat epoxy and nano-epoxy composites was understood by Fourier transform infrared spectroscopy and by XRD.Moreover,hardness and shear strength(shear punch)were also determined in order to gain additional information about the mechanical properties of epoxy composite.Influence of inorganic nano-fillers on the dielectric properties,structural chemistry and mechanical properties of neat epoxy composite is discussed thoroughly in this study.展开更多
基金Authors are thankful to the funding agency DST,New Delhi for providing financial assistance,through the DST-FIST Projects(SR/FST/PSI-001/2006 and SR/FST/PSI-198/2014)Funding provided by UGC,New Delhi through DRSSAP Program Grants[Nos.F.530/10/DRS/2010(SAP-1)and F.530/17/DRS-II/2018(SAP-1)]is also gratefully acknowledged.Authors are also thankful to Prof.P.N.Gajjar,Head,Department of Physics,University School of Sciences,Gujarat University,Ahmedabad for his constant encouragement.
文摘This work outlines the characterization of epoxy resin[Bisphenol A-(epichlorhydrin):epoxy]and hardener[N(3-dimethylaminopropyl)-1,3-propylenediamine]with various inorganic nano-fillers.Dielectric characterizations of epoxy,hardener,neat epoxy(epoxy+hardener)and nano-epoxy(nano-filler+neat epoxy)composites loaded with 1 wt.%of inorganic nano-fillers(SiO_(2),Al_(2)O_(3),TiO_(2)and ZnO)were carried out using precision LCR meter,over the frequency range of 1 kHz-2 MHz at a constant temperature of 300.15 K.The structural information of nano-fillers,neat epoxy and nano-epoxy composites was understood by Fourier transform infrared spectroscopy and by XRD.Moreover,hardness and shear strength(shear punch)were also determined in order to gain additional information about the mechanical properties of epoxy composite.Influence of inorganic nano-fillers on the dielectric properties,structural chemistry and mechanical properties of neat epoxy composite is discussed thoroughly in this study.
