Ni-Al2O3 nano-composite coatings were fabricated by sediment co-deposition (SCD) from Watt’s type electrolyte containing nano-Al2O3 particles without any additives. For comparison, Ni-Al2O3 nano-composite coatings we...Ni-Al2O3 nano-composite coatings were fabricated by sediment co-deposition (SCD) from Watt’s type electrolyte containing nano-Al2O3 particles without any additives. For comparison, Ni-Al2O3 nano-composite coatings were prepared by conventional electro-plating (CEP) under experimental conditions. Effects of process parameters, such as nano-Al2O3 concentration in plating solution, current density, stirring rate, and bath temperature, on nano-Al2O3 content in composite coatings were investigated. The distribution of elements in deposit, and the bonding strength between coating and substrate was analyzed by electron probe microanalyzer (EPMA) and auto-scratch apparatus, respectively. It is found that the nano-Al2O3 concentration in plating solution, current density and stirring rate are three main factors affecting the particles content in deposit, and played a key role in the formation of composite coatings. The nano-Al2O3 content in composite coatings increased with increasing of nano-Al2O3 concentration in plating solution, current density and stirring rate to reach a maximum value, and then reduced slightly. The contents of nano-Al2O3 particles in composite coatings by the SCD technique were higher than that by the CEP technique. The co-deposited nano-Al2O3 particles embedded uniformly in the Ni matrix. The coating was well adhesion with substrate. It is demonstrated that the SCD technique is an efficient approach for improving the nano-Al2O3 content in Ni-Al2O3 composite coatings.展开更多
The Yutian earthquake with M_S7.3 happened on February 12,2014. The precursor monitoring ability is weak in that area. We found tendency anomalies and middle- and short-term anomalies from metal pendulum tilt measurem...The Yutian earthquake with M_S7.3 happened on February 12,2014. The precursor monitoring ability is weak in that area. We found tendency anomalies and middle- and short-term anomalies from metal pendulum tilt measurements in Hotan seismic station before the earthquake. And we also compared the anomalies with that of the M_S7.3 Yutian earthquake on March 21,2008. The tendency anomalies measured by the metal pendulum tiltmeter appeared since 2012 as tilting eastward. While the middle- and short-term anomalies were characterized by acceleration,pause and rapid change of tilt rate in two directions. The tendency anomalies of metal pendulum tilt records are the same before the two earthquakes. They both happened in the east direction. However,there are differences in duration,characteristic and earthquake intervals for the middle- and short-term anomalies.展开更多
基金Supported by the National Natural Science Foundation of China (Grant No 50234020 and 50474055) and the of Northeastern University
文摘Ni-Al2O3 nano-composite coatings were fabricated by sediment co-deposition (SCD) from Watt’s type electrolyte containing nano-Al2O3 particles without any additives. For comparison, Ni-Al2O3 nano-composite coatings were prepared by conventional electro-plating (CEP) under experimental conditions. Effects of process parameters, such as nano-Al2O3 concentration in plating solution, current density, stirring rate, and bath temperature, on nano-Al2O3 content in composite coatings were investigated. The distribution of elements in deposit, and the bonding strength between coating and substrate was analyzed by electron probe microanalyzer (EPMA) and auto-scratch apparatus, respectively. It is found that the nano-Al2O3 concentration in plating solution, current density and stirring rate are three main factors affecting the particles content in deposit, and played a key role in the formation of composite coatings. The nano-Al2O3 content in composite coatings increased with increasing of nano-Al2O3 concentration in plating solution, current density and stirring rate to reach a maximum value, and then reduced slightly. The contents of nano-Al2O3 particles in composite coatings by the SCD technique were higher than that by the CEP technique. The co-deposited nano-Al2O3 particles embedded uniformly in the Ni matrix. The coating was well adhesion with substrate. It is demonstrated that the SCD technique is an efficient approach for improving the nano-Al2O3 content in Ni-Al2O3 composite coatings.
基金sponsored by the Earthquake Science Foundation of Xinjiang,China(201302)
文摘The Yutian earthquake with M_S7.3 happened on February 12,2014. The precursor monitoring ability is weak in that area. We found tendency anomalies and middle- and short-term anomalies from metal pendulum tilt measurements in Hotan seismic station before the earthquake. And we also compared the anomalies with that of the M_S7.3 Yutian earthquake on March 21,2008. The tendency anomalies measured by the metal pendulum tiltmeter appeared since 2012 as tilting eastward. While the middle- and short-term anomalies were characterized by acceleration,pause and rapid change of tilt rate in two directions. The tendency anomalies of metal pendulum tilt records are the same before the two earthquakes. They both happened in the east direction. However,there are differences in duration,characteristic and earthquake intervals for the middle- and short-term anomalies.