Vertically aligned carbon nanotubes (VACNTs) array with high density have been synthesized from a mixture of ferrocene and ethanol using ultrasonic nebulizer techniques. Using scanning electron microscopy (SEM) and tr...Vertically aligned carbon nanotubes (VACNTs) array with high density have been synthesized from a mixture of ferrocene and ethanol using ultrasonic nebulizer techniques. Using scanning electron microscopy (SEM) and transmission electron microscopy (TEM) as well as Raman spectroscopy, investigations reveal that the vertically aligned CNTs are multi-wall CNTs with well-ordered graphene sheets and are about 20 - 50 nm in diameter. We found that high density vertically aligned CNTs can be synthesized at 750℃ - 850℃ and that the length and density of vertically aligned CNTs increase with increasing growth temperatures. In addition, the single-walls CNTs have well-ordered graphene sheet and are about 2 nm in diameter on silicon substrates at 650℃.展开更多
ZnO nanostructures were prepared on corning glass substrate by flow coating process with different annealing temperature from 100?C to 600?C. Fresh and two days aged solutions were used to investigate the growth behav...ZnO nanostructures were prepared on corning glass substrate by flow coating process with different annealing temperature from 100?C to 600?C. Fresh and two days aged solutions were used to investigate the growth behavior and to evaluate the nanostructure of ZnO. The effect of preparation conditions on the deposition of ZnO nanostructure was investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), Raman, and photoluminescence spectroscopy (PL). The results indicated that the solution aging condition and annealing temperature have a strong influence on the morphology and structural properties of the ZnO nanostructure. The solution aged after two days shows the different morphologies compared with the freshly prepared solution.展开更多
文摘Vertically aligned carbon nanotubes (VACNTs) array with high density have been synthesized from a mixture of ferrocene and ethanol using ultrasonic nebulizer techniques. Using scanning electron microscopy (SEM) and transmission electron microscopy (TEM) as well as Raman spectroscopy, investigations reveal that the vertically aligned CNTs are multi-wall CNTs with well-ordered graphene sheets and are about 20 - 50 nm in diameter. We found that high density vertically aligned CNTs can be synthesized at 750℃ - 850℃ and that the length and density of vertically aligned CNTs increase with increasing growth temperatures. In addition, the single-walls CNTs have well-ordered graphene sheet and are about 2 nm in diameter on silicon substrates at 650℃.
文摘ZnO nanostructures were prepared on corning glass substrate by flow coating process with different annealing temperature from 100?C to 600?C. Fresh and two days aged solutions were used to investigate the growth behavior and to evaluate the nanostructure of ZnO. The effect of preparation conditions on the deposition of ZnO nanostructure was investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), Raman, and photoluminescence spectroscopy (PL). The results indicated that the solution aging condition and annealing temperature have a strong influence on the morphology and structural properties of the ZnO nanostructure. The solution aged after two days shows the different morphologies compared with the freshly prepared solution.
