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Synthesis of BaWOq/NRGO-g-C3N4 nanocomposites with excellent multifunctional catalytic performance via microwave approach 被引量:2
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作者 M. Mohamed Jaffer SADIQ u. sandhya shenoy D. Krishna BHAT 《Frontiers of Materials Science》 SCIE CSCD 2018年第3期247-263,共17页
Novel barium tungstate/nitrogen-doped reduced graphene oxide-graphi- tic carbon nitride (BaWO4/NRGO-g-C3N4) nanocomposite has been synthesized by a simple one-pot microwave technique. The synthesized nanocomposites ... Novel barium tungstate/nitrogen-doped reduced graphene oxide-graphi- tic carbon nitride (BaWO4/NRGO-g-C3N4) nanocomposite has been synthesized by a simple one-pot microwave technique. The synthesized nanocomposites are well characterized by diffraction, microscopic and spectroscopic techniques to study its crystal structure, elemental composition, morphological features and optical properties. The material prepared is tested for its performance as an electrocatalyst, photocatalyst and reduction catalyst. The nanocomposite catalyzed the photodegradation of methylene blue (MB) dye in 120 min, reduction of 4-nitro phenol (4-NP) to 4-amino phenol (4-AP) in 60 s, showed an impressive Tafel slope of 62 mV/dec for hydrogen evolution reaction (HER). The observed results suggest that the nanocomposite acts as an efficient multifunctional catalyst. The reported approach provides fundamental insights which can be extended to other metal tungstate-based ternary composites for applications in the field of clean energy and environment in the future. 展开更多
关键词 BaWO4/NRGO-g-C3N4 nanocomposites microwave irradiation hydrogen evolution reaction PHOTOCATALYST reduction
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A simple single-step approach towards synthesis of nanofluids containing cuboctahedral cuprous oxide particles using glucose reduction 被引量:1
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作者 u. sandhya shenoy A. Nityananda SHETTY 《Frontiers of Materials Science》 SCIE CSCD 2018年第1期74-82,共9页
Enhancement of thermal properties of conventional heat transfer fluids has become one of the important technical challenges. Since nanofluids offer a promising help in this regard, development of simpler and hassle fr... Enhancement of thermal properties of conventional heat transfer fluids has become one of the important technical challenges. Since nanofluids offer a promising help in this regard, development of simpler and hassle free routes for their synthesis is of utmost importance. Synthesis of nanofluids using a hassle free route with greener chemicals has been reported. The single-step chemical approach reported here overcomes the drawbacks of the two-step procedures in the synthesis of nanofluids. The resulting Newtonian nanofluids prepared contained cuboctahedral particles of cuprous oxide and exhibited a thermal conductivity of 2.852 W- m-1. K-1. Polyvinylpyrro- lidone (PVP) used during the synthesis acted as a stabilizing agent rendering the nanofluid a stability of 9 weeks. 展开更多
关键词 cuprous oxide nanofluids thermal conductivity VISCOSITY
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